PL442807A1 - A new β-ketoimine derivative, method of its preparation and its application - Google Patents

A new β-ketoimine derivative, method of its preparation and its application

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Publication number
PL442807A1
PL442807A1 PL442807A PL44280722A PL442807A1 PL 442807 A1 PL442807 A1 PL 442807A1 PL 442807 A PL442807 A PL 442807A PL 44280722 A PL44280722 A PL 44280722A PL 442807 A1 PL442807 A1 PL 442807A1
Authority
PL
Poland
Prior art keywords
application
ethyl
derivative
new
preparation
Prior art date
Application number
PL442807A
Other languages
Polish (pl)
Other versions
PL247622B1 (en
Inventor
Katarzyna WITT
Original Assignee
Politechnika Bydgoska Im. Jana I Jędrzeja Śniadeckich
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Politechnika Bydgoska Im. Jana I Jędrzeja Śniadeckich filed Critical Politechnika Bydgoska Im. Jana I Jędrzeja Śniadeckich
Priority to PL442807A priority Critical patent/PL247622B1/en
Publication of PL442807A1 publication Critical patent/PL442807A1/en
Publication of PL247622B1 publication Critical patent/PL247622B1/en

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/18—Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F15/00—Compounds containing elements of Groups 8, 9, 10 or 18 of the Periodic Table

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)

Abstract

Przedmiotem zgłoszenia jest nowa pochodna β-ketoiminy, którą stanowi 4-(3-trietoksysililopropyloimino)-3-etylo-pentan-2-on o wzorze strukturalnym 1. Przedmiotem zgłoszenia jest również sposób otrzymywania tej pochodnej obejmujący poddawanie reakcji 3-etylo-pentano-2,4-dionu oraz 3-aminopropylotrietoksysilanu w proporcji molowej reagentów wynoszącej 1:1, następnie przeprowadzano eliminację cząsteczek wody z uzyskanego produktu pośredniego poprzez ogrzewanie mieszaniny przy stałym mieszaniu w temperaturze od temperatury wrzenia 3-etylo-pentano-2,4-dionu do 100°C przez 1 — 2 godzin, a uzyskany produkt rekrystalizowano znanym sposobem. Ujawniono również zastosowanie nowej pochodnej lub związku otrzymanego sposobem wg zgłoszenia.The subject of the application is a new derivative of β-ketoimine, which is 4-(3-triethoxysilylpropylimino)-3-ethyl-pentan-2-one with the structural formula 1. The subject of the application is also a method of obtaining this derivative, including reacting 3-ethyl-pentan- 2,4-dione and 3-aminopropyltriethoxysilane in a molar proportion of the reactants of 1:1, then the elimination of water molecules from the obtained intermediate product was carried out by heating the mixture with constant stirring at a temperature from the boiling point of 3-ethyl-pentane-2,4-dione to 100°C for 1 - 2 hours, and the obtained product was recrystallized by a known method. The use of a new derivative or compound obtained by the method according to the application is also disclosed.

PL442807A 2022-11-15 2022-11-15 β-ketoimine derivative, method of its preparation and its use PL247622B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PL442807A PL247622B1 (en) 2022-11-15 2022-11-15 β-ketoimine derivative, method of its preparation and its use

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PL442807A PL247622B1 (en) 2022-11-15 2022-11-15 β-ketoimine derivative, method of its preparation and its use

Publications (2)

Publication Number Publication Date
PL442807A1 true PL442807A1 (en) 2024-05-20
PL247622B1 PL247622B1 (en) 2025-08-04

Family

ID=91128883

Family Applications (1)

Application Number Title Priority Date Filing Date
PL442807A PL247622B1 (en) 2022-11-15 2022-11-15 β-ketoimine derivative, method of its preparation and its use

Country Status (1)

Country Link
PL (1) PL247622B1 (en)

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
PL196528B1 (en) * 2003-12-23 2008-01-31 Univ Adama Mickiewicza New agent for complexing metal ions and method of its obtaining
JP2020196681A (en) * 2019-06-03 2020-12-10 信越化学工業株式会社 Production method of imino group-containing organoxysilane compound
KR20210047254A (en) * 2019-10-21 2021-04-29 신에쓰 가가꾸 고교 가부시끼가이샤 Method for producing imino group-containing organoxysilane compound
RU2751696C1 (en) * 2020-09-15 2021-07-15 Федеральное государственное бюджетное образовательное учреждение высшего образования "Чувашский государственный университет имени И.Н. Ульянова" Method for production of aminosilanes

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
PL196528B1 (en) * 2003-12-23 2008-01-31 Univ Adama Mickiewicza New agent for complexing metal ions and method of its obtaining
JP2020196681A (en) * 2019-06-03 2020-12-10 信越化学工業株式会社 Production method of imino group-containing organoxysilane compound
KR20210047254A (en) * 2019-10-21 2021-04-29 신에쓰 가가꾸 고교 가부시끼가이샤 Method for producing imino group-containing organoxysilane compound
RU2751696C1 (en) * 2020-09-15 2021-07-15 Федеральное государственное бюджетное образовательное учреждение высшего образования "Чувашский государственный университет имени И.Н. Ульянова" Method for production of aminosilanes

Also Published As

Publication number Publication date
PL247622B1 (en) 2025-08-04

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