UA73471C2 - A process for producing pectin products separated into fractions - Google Patents

A process for producing pectin products separated into fractions Download PDF

Info

Publication number: UA73471C2
Authority: UA; Ukraine
Prior art keywords: calcium; pectin; minimum; value; maximum
Prior art date: 1998-12-28

Application number

UA2000095566A

Other languages

English (en)

Ukrainian (uk)

Original Assignee

Hercules Inc

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1998-12-28

Filing date

1999-11-29

Publication date

2005-08-15

1999-11-29 Application filed by Hercules Inc filed Critical Hercules Inc

2005-08-15 Publication of UA73471C2 publication Critical patent/UA73471C2/uk

Links

238000000034 method Methods 0.000 title claims abstract description 181
239000001814 pectin Substances 0.000 title claims abstract description 167
229920001277 pectin Polymers 0.000 title claims abstract description 167
235000010987 pectin Nutrition 0.000 title claims abstract description 167
230000008569 process Effects 0.000 title claims abstract description 20
238000000605 extraction Methods 0.000 claims abstract description 108
OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims abstract description 87
239000011575 calcium Substances 0.000 claims abstract description 87
229910052791 calcium Inorganic materials 0.000 claims abstract description 87
239000000243 solution Substances 0.000 claims abstract description 45
239000002253 acid Substances 0.000 claims abstract description 32
239000003929 acidic solution Substances 0.000 claims abstract description 23
239000007858 starting material Substances 0.000 claims abstract description 10
235000013311 vegetables Nutrition 0.000 claims abstract description 8
235000011389 fruit/vegetable juice Nutrition 0.000 claims abstract 4
229960005069 calcium Drugs 0.000 claims description 85
239000000463 material Substances 0.000 claims description 49
241000196324 Embryophyta Species 0.000 claims description 36
239000000203 mixture Substances 0.000 claims description 36
150000001768 cations Chemical class 0.000 claims description 33
230000035945 sensitivity Effects 0.000 claims description 31
239000007788 liquid Substances 0.000 claims description 27
238000005886 esterification reaction Methods 0.000 claims description 22
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 20
230000032050 esterification Effects 0.000 claims description 20
VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 16
235000020971 citrus fruits Nutrition 0.000 claims description 16
230000002378 acidificating effect Effects 0.000 claims description 15
238000000926 separation method Methods 0.000 claims description 13
BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 claims description 12
229910001424 calcium ion Inorganic materials 0.000 claims description 12
XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 10
159000000007 calcium salts Chemical class 0.000 claims description 10
238000012545 processing Methods 0.000 claims description 9
150000003839 salts Chemical class 0.000 claims description 9
229910000019 calcium carbonate Inorganic materials 0.000 claims description 8
229960003563 calcium carbonate Drugs 0.000 claims description 8
ZCCIPPOKBCJFDN-UHFFFAOYSA-N calcium nitrate Chemical compound [Ca+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O ZCCIPPOKBCJFDN-UHFFFAOYSA-N 0.000 claims description 8
230000003993 interaction Effects 0.000 claims description 7
241000207199 Citrus Species 0.000 claims description 6
239000002994 raw material Substances 0.000 claims description 6
RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 5
FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims description 5
GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 5
229910052782 aluminium Inorganic materials 0.000 claims description 5
239000007864 aqueous solution Substances 0.000 claims description 5
229910052802 copper Inorganic materials 0.000 claims description 5
239000010949 copper Substances 0.000 claims description 5
229910052742 iron Inorganic materials 0.000 claims description 5
239000011777 magnesium Substances 0.000 claims description 5
229910052749 magnesium Inorganic materials 0.000 claims description 5
238000004519 manufacturing process Methods 0.000 claims description 5
229910017604 nitric acid Inorganic materials 0.000 claims description 5
BCZXFFBUYPCTSJ-UHFFFAOYSA-L Calcium propionate Chemical compound [Ca+2].CCC([O-])=O.CCC([O-])=O BCZXFFBUYPCTSJ-UHFFFAOYSA-L 0.000 claims description 4
235000003222 Helianthus annuus Nutrition 0.000 claims description 4
XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 4
235000021016 apples Nutrition 0.000 claims description 4
239000006227 byproduct Substances 0.000 claims description 4
VSGNNIFQASZAOI-UHFFFAOYSA-L calcium acetate Chemical compound [Ca+2].CC([O-])=O.CC([O-])=O VSGNNIFQASZAOI-UHFFFAOYSA-L 0.000 claims description 4
239000001639 calcium acetate Substances 0.000 claims description 4
235000011092 calcium acetate Nutrition 0.000 claims description 4
229960005147 calcium acetate Drugs 0.000 claims description 4
AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 claims description 4
239000004227 calcium gluconate Substances 0.000 claims description 4
235000013927 calcium gluconate Nutrition 0.000 claims description 4
229960004494 calcium gluconate Drugs 0.000 claims description 4
239000000920 calcium hydroxide Substances 0.000 claims description 4
229910001861 calcium hydroxide Inorganic materials 0.000 claims description 4
235000011116 calcium hydroxide Nutrition 0.000 claims description 4
MKJXYGKVIBWPFZ-UHFFFAOYSA-L calcium lactate Chemical compound [Ca+2].CC(O)C([O-])=O.CC(O)C([O-])=O MKJXYGKVIBWPFZ-UHFFFAOYSA-L 0.000 claims description 4
239000001527 calcium lactate Substances 0.000 claims description 4
229960002401 calcium lactate Drugs 0.000 claims description 4
235000011086 calcium lactate Nutrition 0.000 claims description 4
BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 claims description 4
239000000292 calcium oxide Substances 0.000 claims description 4
ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 claims description 4
235000012255 calcium oxide Nutrition 0.000 claims description 4
235000010331 calcium propionate Nutrition 0.000 claims description 4
239000004330 calcium propionate Substances 0.000 claims description 4
NEEHYRZPVYRGPP-UHFFFAOYSA-L calcium;2,3,4,5,6-pentahydroxyhexanoate Chemical compound [Ca+2].OCC(O)C(O)C(O)C(O)C([O-])=O.OCC(O)C(O)C(O)C(O)C([O-])=O NEEHYRZPVYRGPP-UHFFFAOYSA-L 0.000 claims description 4
150000007522 mineralic acids Chemical class 0.000 claims description 4
239000008346 aqueous phase Substances 0.000 claims description 3
230000015572 biosynthetic process Effects 0.000 claims description 3
244000020551 Helianthus annuus Species 0.000 claims description 2
241000219310 Beta vulgaris subsp. vulgaris Species 0.000 claims 3
241000220225 Malus Species 0.000 claims 3
235000021536 Sugar beet Nutrition 0.000 claims 3
235000010216 calcium carbonate Nutrition 0.000 claims 3
229940087373 calcium oxide Drugs 0.000 claims 3
241000208818 Helianthus Species 0.000 claims 2
229940095643 calcium hydroxide Drugs 0.000 claims 2
238000012876 topography Methods 0.000 claims 1
239000000284 extract Substances 0.000 abstract description 13
239000005418 vegetable material Substances 0.000 abstract 1
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 32
239000000047 product Substances 0.000 description 31
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 15
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 15
238000002474 experimental method Methods 0.000 description 15
239000013049 sediment Substances 0.000 description 9
239000002904 solvent Substances 0.000 description 9
238000012360 testing method Methods 0.000 description 9
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 8
IAJILQKETJEXLJ-RSJOWCBRSA-N aldehydo-D-galacturonic acid Chemical compound O=C[C@H](O)[C@@H](O)[C@@H](O)[C@H](O)C(O)=O IAJILQKETJEXLJ-RSJOWCBRSA-N 0.000 description 7
239000000126 substance Substances 0.000 description 7
235000013618 yogurt Nutrition 0.000 description 7
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
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238000005516 engineering process Methods 0.000 description 6
239000002245 particle Substances 0.000 description 6
IAJILQKETJEXLJ-UHFFFAOYSA-N Galacturonsaeure Natural products O=CC(O)C(O)C(O)C(O)C(O)=O IAJILQKETJEXLJ-UHFFFAOYSA-N 0.000 description 5
238000004458 analytical method Methods 0.000 description 5
238000006243 chemical reaction Methods 0.000 description 5
239000000499 gel Substances 0.000 description 5
230000000087 stabilizing effect Effects 0.000 description 5
238000003756 stirring Methods 0.000 description 5
241000283690 Bos taurus Species 0.000 description 4
238000009835 boiling Methods 0.000 description 4
229910000389 calcium phosphate Inorganic materials 0.000 description 4
238000001035 drying Methods 0.000 description 4
238000001914 filtration Methods 0.000 description 4
239000012530 fluid Substances 0.000 description 4
235000013305 food Nutrition 0.000 description 4
238000010438 heat treatment Methods 0.000 description 4
238000005325 percolation Methods 0.000 description 4
KJFMBFZCATUALV-UHFFFAOYSA-N phenolphthalein Chemical compound C1=CC(O)=CC=C1C1(C=2C=CC(O)=CC=2)C2=CC=CC=C2C(=O)O1 KJFMBFZCATUALV-UHFFFAOYSA-N 0.000 description 4
UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 3
LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 3
235000012970 cakes Nutrition 0.000 description 3
125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 3
238000005119 centrifugation Methods 0.000 description 3
239000013256 coordination polymer Substances 0.000 description 3
238000013461 design Methods 0.000 description 3
239000012153 distilled water Substances 0.000 description 3
239000000945 filler Substances 0.000 description 3
230000006870 function Effects 0.000 description 3
238000002156 mixing Methods 0.000 description 3
235000019691 monocalcium phosphate Nutrition 0.000 description 3
235000015108 pies Nutrition 0.000 description 3
239000007787 solid Substances 0.000 description 3
235000000346 sugar Nutrition 0.000 description 3
150000008163 sugars Chemical class 0.000 description 3
NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 description 2
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
244000089742 Citrus aurantifolia Species 0.000 description 2
235000008733 Citrus aurantifolia Nutrition 0.000 description 2
235000005979 Citrus limon Nutrition 0.000 description 2
244000131522 Citrus pyriformis Species 0.000 description 2
SHZGCJCMOBCMKK-JFNONXLTSA-N L-rhamnopyranose Chemical compound C[C@@H]1OC(O)[C@H](O)[C@H](O)[C@H]1O SHZGCJCMOBCMKK-JFNONXLTSA-N 0.000 description 2
244000141359 Malus pumila Species 0.000 description 2
229920002230 Pectic acid Polymers 0.000 description 2
235000011941 Tilia x europaea Nutrition 0.000 description 2
150000007513 acids Chemical class 0.000 description 2
230000009471 action Effects 0.000 description 2
230000009435 amidation Effects 0.000 description 2
238000007112 amidation reaction Methods 0.000 description 2
229910052788 barium Inorganic materials 0.000 description 2
DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 description 2
239000001110 calcium chloride Substances 0.000 description 2
229910001628 calcium chloride Inorganic materials 0.000 description 2
FUFJGUQYACFECW-UHFFFAOYSA-L calcium hydrogenphosphate Chemical compound [Ca+2].OP([O-])([O-])=O FUFJGUQYACFECW-UHFFFAOYSA-L 0.000 description 2
239000001913 cellulose Substances 0.000 description 2
229920002678 cellulose Polymers 0.000 description 2
235000009508 confectionery Nutrition 0.000 description 2
239000006071 cream Substances 0.000 description 2
235000013365 dairy product Nutrition 0.000 description 2
238000010586 diagram Methods 0.000 description 2
238000009826 distribution Methods 0.000 description 2
230000000694 effects Effects 0.000 description 2
239000004744 fabric Substances 0.000 description 2
239000011521 glass Substances 0.000 description 2
238000000227 grinding Methods 0.000 description 2
229910052500 inorganic mineral Inorganic materials 0.000 description 2
238000005342 ion exchange Methods 0.000 description 2
150000002500 ions Chemical class 0.000 description 2
235000015110 jellies Nutrition 0.000 description 2
239000004571 lime Substances 0.000 description 2
239000011572 manganese Substances 0.000 description 2
239000011707 mineral Substances 0.000 description 2
235000010755 mineral Nutrition 0.000 description 2
-1 nitric Chemical class 0.000 description 2
150000007524 organic acids Chemical class 0.000 description 2
235000005985 organic acids Nutrition 0.000 description 2
239000010318 polygalacturonic acid Substances 0.000 description 2
239000002244 precipitate Substances 0.000 description 2
102000004169 proteins and genes Human genes 0.000 description 2
108090000623 proteins and genes Proteins 0.000 description 2
239000002683 reaction inhibitor Substances 0.000 description 2
230000001105 regulatory effect Effects 0.000 description 2
235000020183 skimmed milk Nutrition 0.000 description 2
239000003381 stabilizer Substances 0.000 description 2
210000004243 sweat Anatomy 0.000 description 2
QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 description 2
HIQIXEFWDLTDED-UHFFFAOYSA-N 4-hydroxy-1-piperidin-4-ylpyrrolidin-2-one Chemical compound O=C1CC(O)CN1C1CCNCC1 HIQIXEFWDLTDED-UHFFFAOYSA-N 0.000 description 1
QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 1
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244000105624 Arachis hypogaea Species 0.000 description 1
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208000035985 Body Odor Diseases 0.000 description 1
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239000001736 Calcium glycerylphosphate Substances 0.000 description 1
UNMYWSMUMWPJLR-UHFFFAOYSA-L Calcium iodide Chemical group [Ca+2].[I-].[I-] UNMYWSMUMWPJLR-UHFFFAOYSA-L 0.000 description 1
240000000560 Citrus x paradisi Species 0.000 description 1
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IMQLKJBTEOYOSI-GPIVLXJGSA-N Inositol-hexakisphosphate Chemical compound OP(O)(=O)O[C@H]1[C@H](OP(O)(O)=O)[C@@H](OP(O)(O)=O)[C@H](OP(O)(O)=O)[C@H](OP(O)(O)=O)[C@@H]1OP(O)(O)=O IMQLKJBTEOYOSI-GPIVLXJGSA-N 0.000 description 1
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KNVPMEZIMFVWMD-UHFFFAOYSA-N Menthyl pyrrolidone carboxylate Chemical compound CC(C)C1CCC(C)CC1OC(=O)N1C(=O)CCC1 KNVPMEZIMFVWMD-UHFFFAOYSA-N 0.000 description 1
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UJNOLBSYLSYIBM-WISYIIOYSA-N [(1r,2s,5r)-5-methyl-2-propan-2-ylcyclohexyl] (2r)-2-hydroxypropanoate Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@H]1OC(=O)[C@@H](C)O UJNOLBSYLSYIBM-WISYIIOYSA-N 0.000 description 1
YDHWWBZFRZWVHO-UHFFFAOYSA-H [oxido-[oxido(phosphonatooxy)phosphoryl]oxyphosphoryl] phosphate Chemical compound [O-]P([O-])(=O)OP([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O YDHWWBZFRZWVHO-UHFFFAOYSA-H 0.000 description 1
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235000015197 apple juice Nutrition 0.000 description 1
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JUNWLZAGQLJVLR-UHFFFAOYSA-J calcium diphosphate Chemical compound [Ca+2].[Ca+2].[O-]P([O-])(=O)OP([O-])([O-])=O JUNWLZAGQLJVLR-UHFFFAOYSA-J 0.000 description 1
235000019255 calcium formate Nutrition 0.000 description 1
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UHHRFSOMMCWGSO-UHFFFAOYSA-L calcium glycerophosphate Chemical compound [Ca+2].OCC(CO)OP([O-])([O-])=O UHHRFSOMMCWGSO-UHFFFAOYSA-L 0.000 description 1
235000019299 calcium glycerylphosphate Nutrition 0.000 description 1
229940046413 calcium iodide Drugs 0.000 description 1
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ZFXVRMSLJDYJCH-UHFFFAOYSA-N calcium magnesium Chemical group [Mg].[Ca] ZFXVRMSLJDYJCH-UHFFFAOYSA-N 0.000 description 1
QXDMQSPYEZFLGF-UHFFFAOYSA-L calcium oxalate Chemical compound [Ca+2].[O-]C(=O)C([O-])=O QXDMQSPYEZFLGF-UHFFFAOYSA-L 0.000 description 1
239000001506 calcium phosphate Substances 0.000 description 1
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235000010261 calcium sulphite Nutrition 0.000 description 1
UMVAYAXXQSFULN-QHTZZOMLSA-L calcium;(2s)-2-aminopentanedioate;hydron Chemical compound [Ca+2].[O-]C(=O)[C@@H](N)CCC(O)=O.[O-]C(=O)[C@@H](N)CCC(O)=O UMVAYAXXQSFULN-QHTZZOMLSA-L 0.000 description 1
VPWAVWZPVGDNMN-UHFFFAOYSA-L calcium;2,3-dihydroxypropanoate Chemical compound [Ca+2].OCC(O)C([O-])=O.OCC(O)C([O-])=O VPWAVWZPVGDNMN-UHFFFAOYSA-L 0.000 description 1
OFNJDDJDXNMTHZ-UHFFFAOYSA-L calcium;2-aminoacetate Chemical compound [Ca+2].NCC([O-])=O.NCC([O-])=O OFNJDDJDXNMTHZ-UHFFFAOYSA-L 0.000 description 1
LLEWEKKNPYGRTD-UHFFFAOYSA-L calcium;2-hydroxypropanoyl phosphate Chemical group [Ca+2].CC(O)C(=O)OP([O-])([O-])=O LLEWEKKNPYGRTD-UHFFFAOYSA-L 0.000 description 1
PBUBJNYXWIDFMU-UHFFFAOYSA-L calcium;butanedioate Chemical compound [Ca+2].[O-]C(=O)CCC([O-])=O PBUBJNYXWIDFMU-UHFFFAOYSA-L 0.000 description 1
HHSPVTKDOHQBKF-UHFFFAOYSA-J calcium;magnesium;dicarbonate Chemical group [Mg+2].[Ca+2].[O-]C([O-])=O.[O-]C([O-])=O HHSPVTKDOHQBKF-UHFFFAOYSA-J 0.000 description 1
238000004364 calculation method Methods 0.000 description 1
239000001569 carbon dioxide Substances 0.000 description 1
229910002092 carbon dioxide Inorganic materials 0.000 description 1
239000000969 carrier Substances 0.000 description 1
210000000170 cell membrane Anatomy 0.000 description 1
235000013351 cheese Nutrition 0.000 description 1
230000001055 chewing effect Effects 0.000 description 1
150000001805 chlorine compounds Chemical class 0.000 description 1
235000019987 cider Nutrition 0.000 description 1
150000001875 compounds Chemical class 0.000 description 1
238000010924 continuous production Methods 0.000 description 1
235000014510 cooky Nutrition 0.000 description 1
238000001816 cooling Methods 0.000 description 1
239000002537 cosmetic Substances 0.000 description 1
235000012495 crackers Nutrition 0.000 description 1
235000015140 cultured milk Nutrition 0.000 description 1
230000007423 decrease Effects 0.000 description 1
239000008367 deionised water Substances 0.000 description 1
229910021641 deionized water Inorganic materials 0.000 description 1
239000002781 deodorant agent Substances 0.000 description 1
238000011161 development Methods 0.000 description 1
239000008121 dextrose Substances 0.000 description 1
235000019821 dicalcium diphosphate Nutrition 0.000 description 1
238000007865 diluting Methods 0.000 description 1
239000003085 diluting agent Substances 0.000 description 1
238000010790 dilution Methods 0.000 description 1
239000012895 dilution Substances 0.000 description 1
238000004821 distillation Methods 0.000 description 1
235000012489 doughnuts Nutrition 0.000 description 1
229910052571 earthenware Inorganic materials 0.000 description 1
235000013399 edible fruits Nutrition 0.000 description 1
230000002500 effect on skin Effects 0.000 description 1
239000003974 emollient agent Substances 0.000 description 1
235000013341 fat substitute Nutrition 0.000 description 1
239000003778 fat substitute Substances 0.000 description 1
239000000835 fiber Substances 0.000 description 1
239000000706 filtrate Substances 0.000 description 1
239000012467 final product Substances 0.000 description 1
235000013332 fish product Nutrition 0.000 description 1
235000019541 flavored milk drink Nutrition 0.000 description 1
238000005187 foaming Methods 0.000 description 1
239000003205 fragrance Substances 0.000 description 1
235000013569 fruit product Nutrition 0.000 description 1
239000007789 gas Substances 0.000 description 1
238000007429 general method Methods 0.000 description 1
238000000265 homogenisation Methods 0.000 description 1
239000010903 husk Substances 0.000 description 1
235000015243 ice cream Nutrition 0.000 description 1
239000012535 impurity Substances 0.000 description 1
238000009434 installation Methods 0.000 description 1
238000002955 isolation Methods 0.000 description 1
239000006210 lotion Substances 0.000 description 1
235000004213 low-fat Nutrition 0.000 description 1
239000000314 lubricant Substances 0.000 description 1
229910052748 manganese Inorganic materials 0.000 description 1
239000008268 mayonnaise Substances 0.000 description 1
235000010746 mayonnaise Nutrition 0.000 description 1
235000013372 meat Nutrition 0.000 description 1
229940041616 menthol Drugs 0.000 description 1
CEQFOVLGLXCDCX-WUKNDPDISA-N methyl red Chemical compound C1=CC(N(C)C)=CC=C1\N=N\C1=CC=CC=C1C(O)=O CEQFOVLGLXCDCX-WUKNDPDISA-N 0.000 description 1
230000011987 methylation Effects 0.000 description 1
238000007069 methylation reaction Methods 0.000 description 1
244000005706 microflora Species 0.000 description 1
235000013336 milk Nutrition 0.000 description 1
239000008267 milk Substances 0.000 description 1
210000004080 milk Anatomy 0.000 description 1
239000002480 mineral oil Substances 0.000 description 1
230000007935 neutral effect Effects 0.000 description 1
150000002823 nitrates Chemical class 0.000 description 1
229910052757 nitrogen Inorganic materials 0.000 description 1
230000009972 noncorrosive effect Effects 0.000 description 1
239000003921 oil Substances 0.000 description 1
235000019198 oils Nutrition 0.000 description 1
238000012856 packing Methods 0.000 description 1
235000015927 pasta Nutrition 0.000 description 1
235000011837 pasties Nutrition 0.000 description 1
235000020232 peanut Nutrition 0.000 description 1
239000002304 perfume Substances 0.000 description 1
230000000737 periodic effect Effects 0.000 description 1
229940068041 phytic acid Drugs 0.000 description 1
229920001296 polysiloxane Polymers 0.000 description 1
235000012015 potatoes Nutrition 0.000 description 1
244000144977 poultry Species 0.000 description 1
235000013594 poultry meat Nutrition 0.000 description 1
239000000843 powder Substances 0.000 description 1
238000002360 preparation method Methods 0.000 description 1
235000012434 pretzels Nutrition 0.000 description 1
235000011962 puddings Nutrition 0.000 description 1
238000010926 purge Methods 0.000 description 1
238000000746 purification Methods 0.000 description 1
239000012429 reaction media Substances 0.000 description 1
230000003134 recirculating effect Effects 0.000 description 1
238000005070 sampling Methods 0.000 description 1
238000007127 saponification reaction Methods 0.000 description 1
235000015067 sauces Nutrition 0.000 description 1
230000028327 secretion Effects 0.000 description 1
230000035807 sensation Effects 0.000 description 1
239000011343 solid material Substances 0.000 description 1
238000005063 solubilization Methods 0.000 description 1
230000007928 solubilization Effects 0.000 description 1
235000014347 soups Nutrition 0.000 description 1
235000021262 sour milk Nutrition 0.000 description 1
239000012086 standard solution Substances 0.000 description 1
238000012546 transfer Methods 0.000 description 1
235000013337 tricalcium citrate Nutrition 0.000 description 1
229910000391 tricalcium phosphate Inorganic materials 0.000 description 1
238000003828 vacuum filtration Methods 0.000 description 1
235000015112 vegetable and seed oil Nutrition 0.000 description 1
239000008158 vegetable oil Substances 0.000 description 1
239000002699 waste material Substances 0.000 description 1
239000002025 wood fiber Substances 0.000 description 1
239000011701 zinc Substances 0.000 description 1
229910052725 zinc Inorganic materials 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B37/00—Preparation of polysaccharides not provided for in groups C08B1/00 - C08B35/00; Derivatives thereof
- C08B37/0006—Homoglycans, i.e. polysaccharides having a main chain consisting of one single sugar, e.g. colominic acid
- C08B37/0045—Homoglycans, i.e. polysaccharides having a main chain consisting of one single sugar, e.g. colominic acid alpha-D-Galacturonans, e.g. methyl ester of (alpha-1,4)-linked D-galacturonic acid units, i.e. pectin, or hydrolysis product of methyl ester of alpha-1,4-linked D-galacturonic acid units, i.e. pectinic acid; Derivatives thereof
- C08B37/0048—Processes of extraction from organic materials

Landscapes

Chemical & Material Sciences (AREA)
Life Sciences & Earth Sciences (AREA)
Health & Medical Sciences (AREA)
Biochemistry (AREA)
Molecular Biology (AREA)
Engineering & Computer Science (AREA)
General Health & Medical Sciences (AREA)
Materials Engineering (AREA)
Chemical Kinetics & Catalysis (AREA)
Medicinal Chemistry (AREA)
Polymers & Plastics (AREA)
Organic Chemistry (AREA)
Polysaccharides And Polysaccharide Derivatives (AREA)
Jellies, Jams, And Syrups (AREA)

UA2000095566A 1998-12-28 1999-11-29 A process for producing pectin products separated into fractions UA73471C2 (en)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
US22411698A	1998-12-28	1998-12-28
PCT/US1999/027908 WO2000039168A1 (en)	1998-12-28	1999-11-29	Process for producing fractionated pectin products

Publications (1)

Publication Number	Publication Date
UA73471C2 true UA73471C2 (en)	2005-08-15

Family

ID=22839341

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
UA2000095566A UA73471C2 (en)	1998-12-28	1999-11-29	A process for producing pectin products separated into fractions

Country Status (11)

Country	Link
EP (1)	EP1058693A1 (pl)
JP (1)	JP2002533533A (pl)
KR (1)	KR20010041405A (pl)
CN (1)	CN100381470C (pl)
AU (1)	AU3103500A (pl)
ID (1)	ID26580A (pl)
IL (1)	IL138106A0 (pl)
PL (1)	PL201281B1 (pl)
RU (1)	RU2272812C2 (pl)
UA (1)	UA73471C2 (pl)
WO (1)	WO2000039168A1 (pl)

Families Citing this family (16)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JP3941772B2 (ja) *	1999-01-19	2007-07-04	不二製油株式会社	根菜類由来ペクチンを含む安定剤、並びにそれを使用した酸性蛋白食品及びその製造法
JP3511952B2 (ja) *	1999-01-19	2004-03-29	不二製油株式会社	ペクチン及びその製造法並びにそれを使用した酸性蛋白食品及びその製造法
DE60122522T2 (de) *	2000-06-09	2007-04-05	Cp Kelco Aps	Pektine mit niedrigem methoxylgrad, verfahren zu deren herstellung und stabilisierte, wässrige systeme, die diese pektine enthalten
US6699977B1 (en)	2000-06-09	2004-03-02	Cp Kelco Aps	Low methoxyl pectins, processes thereof, and stabilized aqueous systems comprising the same
US20060099302A1 (en) *	2002-09-02	2006-05-11	Cp Kelco Aps	Process for treating pectin containing plant material
KR100754658B1 (ko)	2004-03-12	2007-09-03	삼성전자주식회사	통신 시스템에서 복합 재전송 운용 방법
MY159105A (en)	2009-10-30	2016-12-15	Cj Cheiljedang Corp	Process for economically manufacturing xylose from hydrolysate using electrodialysis and direct recovery method
EP2628396B1 (en)	2010-10-13	2019-11-20	Cargill, Incorporated	Powder mix
CN102033050B (zh) *	2011-01-13	2012-07-04	广东中烟工业有限责任公司	植物样品中果胶含量的测定方法
US8592575B2 (en)	2011-06-06	2013-11-26	Cp Kelco Aps	Process for extraction of pectin
IN2015KN00377A (pl)	2012-07-13	2015-07-10	Yakult Honsha Kk
RU2527296C2 (ru) *	2012-12-21	2014-08-27	Федеральное государственное бюджетное образовательное учреждение Высшего профессионального образования КАБАРДИНО-БАЛКАРСКАЯ ГОСУДАРСТВЕННАЯ СЕЛЬСКОХОЗЯЙСТВЕННАЯ АКАДЕМИЯ ИМЕНИ В.М. КОКОВА	Способ получения пектина из створок зеленого гороха
GB201322454D0 (en) *	2013-12-18	2014-02-05	Dupont Nutrition Biosci Aps	Process
NZ757054A (en) *	2017-02-15	2023-04-28	Cp Kelco Aps	Activated pectin-containing biomass compositions, products, and methods of producing
CN109306026B (zh) *	2018-07-24	2021-04-09	江西莱檬生物科技有限责任公司	柑橘类果胶的分级提取方法及应用
BR112022022711A2 (pt) *	2020-05-14	2023-03-28	Dupont Nutrition Biosci Aps	Processo de extração de pectina

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US2020572A (en) *	1929-07-29	1935-11-12	Fruit Growers Exchange Ca	Method of extracting pectin
JPH0649724B2 (ja) *	1984-09-21	1994-06-29	三菱レイヨン株式会社	ペクチンの製造方法
JPS6178501A (ja) *	1984-09-27	1986-04-22	Kawasaki Steel Corp	Ｈ形鋼の製造方法
FR2608017B1 (fr) *	1986-12-11	1989-03-31	Etude Rech Dev	Produit alimentaire reconstitue, procede et melangeur pour sa preparation
RU2033056C1 (ru) *	1990-08-10	1995-04-20	Научно-исследовательский, конструкторско-технологический институт пищевой промышленности	Способ получения пектина из фруктовых выжимок
US6143346A (en) *	1993-12-02	2000-11-07	Hercules Incorporated	Pectin process and composition
US5627269A (en) *	1994-06-22	1997-05-06	Hercules Incorporated	Process for the extraction of soluble polysaccharides
AU741977B2 (en) *	1997-06-23	2001-12-13	Dupont Nutrition Biosciences Aps	Methods of obtaining selected pectin fractions, such fractions and their use

1999
- 1999-11-29 RU RU2000124866/04A patent/RU2272812C2/ru not_active IP Right Cessation
- 1999-11-29 CN CNB998053546A patent/CN100381470C/zh not_active Expired - Fee Related
- 1999-11-29 IL IL13810699A patent/IL138106A0/xx unknown
- 1999-11-29 PL PL342496A patent/PL201281B1/pl not_active IP Right Cessation
- 1999-11-29 EP EP99965032A patent/EP1058693A1/en not_active Withdrawn
- 1999-11-29 UA UA2000095566A patent/UA73471C2/uk unknown
- 1999-11-29 KR KR1020007009538A patent/KR20010041405A/ko not_active Ceased
- 1999-11-29 AU AU31035/00A patent/AU3103500A/en not_active Abandoned
- 1999-11-29 ID IDW20001918A patent/ID26580A/id unknown
- 1999-11-29 WO PCT/US1999/027908 patent/WO2000039168A1/en not_active Ceased
- 1999-11-29 JP JP2000591079A patent/JP2002533533A/ja active Pending

Also Published As

Publication number	Publication date
WO2000039168A1 (en)	2000-07-06
KR20010041405A (ko)	2001-05-15
IL138106A0 (en)	2001-10-31
AU3103500A (en)	2000-07-31
EP1058693A1 (en)	2000-12-13
RU2272812C2 (ru)	2006-03-27
ID26580A (id)	2001-01-18
PL342496A1 (en)	2001-06-04
CN1298413A (zh)	2001-06-06
JP2002533533A (ja)	2002-10-08
PL201281B1 (pl)	2009-03-31
CN100381470C (zh)	2008-04-16

Publication	Publication Date	Title
UA73471C2 (en)	2005-08-15	A process for producing pectin products separated into fractions
Joye et al.	2000	Process for selective extraction of pectins from plant material by differential pH
Alamineh	2018	Extraction of pectin from orange peels and characterizing its physical and chemical properties
US20090202705A1 (en)	2009-08-13	Inulin of very high chain length
EP0664300A1 (en)	1995-07-26	Pectin process and composition
JP2004503666A5 (pl)	2008-07-24
Quintas et al.	2010	Sucrose in the concentrated solution or the supercooled “state”: a review of caramelisation reactions and physical behaviour
US2232555A (en)	1941-02-18	Processing corn
JP7812194B2 (ja)	2026-02-09	高タンパク質の乳原料の製造方法
Ruzibayev et al.	2025	Developing a healthier chocolate spread: Using persimmons to reduce sugar content
Reitz	2016	Investigating the chemical basis of functionality differences between beet and cane sugar sources in model egg white foams and other products
WO2020085517A1 (ja)	2020-04-30	高タンパク質の乳原料の製造方法
CZ20003129A3 (cs)	2001-05-16	Způsob výroby frakcionovaných pektinových produk
MXPA00008339A (en)	2001-12-04	Process for producing fractionated pectin products
US2355098A (en)	1944-08-08	Processing corn
US829254A (en)	1906-08-21	Method of manufacturing food products.
Francio et al.	2025	PHYSICOCHEMICAL CHARACTERIZATION OF THE SEED FLOUR AND THE PULP OF UNRIPE AND RIPE ARATICUM, A BRAZILIAN NATIVE FRUIT
RU2175204C1 (ru)	2001-10-27	Способ производства плодово-ягодного десерта
RU2175494C1 (ru)	2001-11-10	Способ производства плодово-ягодного десерта
RU2183084C2 (ru)	2002-06-10	Способ производства плодово-ягодного десерта
RU2174340C1 (ru)	2001-10-10	Способ производства плодово-ягодного десерта
WO2022005413A2 (en)	2022-01-06	Honey powder having high honey and antioxidant content and production of it
RU2174339C1 (ru)	2001-10-10	Способ производства плодово-ягодного десерта
RU2175500C1 (ru)	2001-11-10	Способ производства плодово-ягодного десерта
JP2729642B2 (ja)	1998-03-18	食品組成物及びその製法