UA98372C2 - Способ получения трифтористого титана - Google Patents
Способ получения трифтористого титанаInfo
- Publication number
- UA98372C2 UA98372C2 UAA201010137A UAA201010137A UA98372C2 UA 98372 C2 UA98372 C2 UA 98372C2 UA A201010137 A UAA201010137 A UA A201010137A UA A201010137 A UAA201010137 A UA A201010137A UA 98372 C2 UA98372 C2 UA 98372C2
- Authority
- UA
- Ukraine
- Prior art keywords
- titanium
- transition metal
- titanium trifluoride
- precipitate
- solution
- Prior art date
Links
- NLPMQGKZYAYAFE-UHFFFAOYSA-K titanium(iii) fluoride Chemical compound F[Ti](F)F NLPMQGKZYAYAFE-UHFFFAOYSA-K 0.000 title abstract 3
- 239000010936 titanium Substances 0.000 abstract 5
- 229910052723 transition metal Inorganic materials 0.000 abstract 3
- 150000003624 transition metals Chemical class 0.000 abstract 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 abstract 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 abstract 2
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 abstract 2
- 239000000463 material Substances 0.000 abstract 2
- 239000002244 precipitate Substances 0.000 abstract 2
- 229910052719 titanium Inorganic materials 0.000 abstract 2
- DDFHBQSCUXNBSA-UHFFFAOYSA-N 5-(5-carboxythiophen-2-yl)thiophene-2-carboxylic acid Chemical compound S1C(C(=O)O)=CC=C1C1=CC=C(C(O)=O)S1 DDFHBQSCUXNBSA-UHFFFAOYSA-N 0.000 abstract 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 abstract 1
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 abstract 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 abstract 1
- 239000000956 alloy Substances 0.000 abstract 1
- 229910045601 alloy Inorganic materials 0.000 abstract 1
- 229910021529 ammonia Inorganic materials 0.000 abstract 1
- 229910017052 cobalt Inorganic materials 0.000 abstract 1
- 239000010941 cobalt Substances 0.000 abstract 1
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 abstract 1
- 229910052742 iron Inorganic materials 0.000 abstract 1
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 abstract 1
- 229910052759 nickel Inorganic materials 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- 229910052725 zinc Inorganic materials 0.000 abstract 1
- 239000011701 zinc Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
- C01G23/02—Halides of titanium
- C01G23/028—Titanium fluoride
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
- C22B34/1204—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 preliminary treatment of ores or scrap to eliminate non- titanium constituents, e.g. iron, without attacking the titanium constituent
- C22B34/1213—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 preliminary treatment of ores or scrap to eliminate non- titanium constituents, e.g. iron, without attacking the titanium constituent by wet processes, e.g. using leaching methods or flotation techniques
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
- C22B34/1236—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining titanium or titanium compounds from ores or scrap by wet processes, e.g. by leaching
- C22B34/124—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining titanium or titanium compounds from ores or scrap by wet processes, e.g. by leaching using acidic solutions or liquors
- C22B34/1245—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining titanium or titanium compounds from ores or scrap by wet processes, e.g. by leaching using acidic solutions or liquors containing a halogen ion as active agent
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
- C22B34/1236—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining titanium or titanium compounds from ores or scrap by wet processes, e.g. by leaching
- C22B34/1259—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining titanium or titanium compounds from ores or scrap by wet processes, e.g. by leaching treatment or purification of titanium containing solutions or liquors or slurries
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
- C22B34/1263—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction
- C22B34/1268—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction using alkali or alkaline-earth metals or amalgams
- C22B34/1272—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction using alkali or alkaline-earth metals or amalgams reduction of titanium halides, e.g. Kroll process
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
- C22B34/129—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds by dissociation, e.g. thermic dissociation of titanium tetraiodide, or by electrolysis or with the use of an electric arc
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
- C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/80—Compositional purity
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Mechanical Engineering (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Manufacturing & Machinery (AREA)
- Inorganic Chemistry (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Catalysts (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Manufacture Of Metal Powder And Suspensions Thereof (AREA)
Abstract
Способ получения трифтористого титана из материала, содержащего титан, включает стадии получения фтористого раствора Ti (IV) из материала, содержащего титан, и восстановление Ti (IV) в растворе переходным металлом или сплавом переходного металла. Переходный металл выбран из марганца, железа, кобальта, никеля и цинка, при этом соль, содержащую аммоний, и аммиак или фторид аммония, добавляют в полученный раствор, содержащий Ti (III), для получения осадка, после чего данный осадок пиролизуют для получения трифтористого титана.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| ZA200800404 | 2008-01-14 | ||
| PCT/IB2008/055559 WO2009090513A1 (en) | 2008-01-14 | 2008-12-29 | The production of titanium trifluoride |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| UA98372C2 true UA98372C2 (ru) | 2012-05-10 |
Family
ID=40673692
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| UAA201010137A UA98372C2 (ru) | 2008-01-14 | 2008-12-29 | Способ получения трифтористого титана |
Country Status (22)
| Country | Link |
|---|---|
| US (1) | US20100278685A1 (ru) |
| EP (1) | EP2244980B1 (ru) |
| JP (1) | JP5370692B2 (ru) |
| KR (1) | KR20100125237A (ru) |
| CN (1) | CN101918319B (ru) |
| AR (1) | AR070155A1 (ru) |
| AT (1) | ATE526289T1 (ru) |
| AU (1) | AU2008348005B2 (ru) |
| BR (1) | BRPI0822138A2 (ru) |
| CA (1) | CA2712116C (ru) |
| CL (1) | CL2009000046A1 (ru) |
| EA (1) | EA017080B1 (ru) |
| EG (1) | EG26459A (ru) |
| ES (1) | ES2375236T3 (ru) |
| MX (1) | MX2010007653A (ru) |
| MY (1) | MY147802A (ru) |
| NZ (1) | NZ586672A (ru) |
| PL (1) | PL2244980T3 (ru) |
| PT (1) | PT2244980E (ru) |
| UA (1) | UA98372C2 (ru) |
| WO (1) | WO2009090513A1 (ru) |
| ZA (1) | ZA201005616B (ru) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101245323B1 (ko) * | 2010-12-28 | 2013-03-19 | 재단법인 포항산업과학연구원 | 망간단괴로부터의 유가금속 침출방법 |
| CN102153128A (zh) * | 2011-05-26 | 2011-08-17 | 中国地质科学院矿产综合利用研究所 | 一种制备氟化钪的方法 |
| CN102616836B (zh) * | 2012-03-31 | 2014-07-02 | 攀枝花东方钛业有限公司 | 三价钛溶液的制备方法 |
| RU2717418C1 (ru) * | 2019-10-04 | 2020-03-23 | Федеральное государственное бюджетное учреждение науки Институт химии Дальневосточного отделения Российской академии наук (ИХ ДВО РАН) | Способ переработки титансодержащего минерального сырья |
| CN110817947B (zh) * | 2019-11-15 | 2020-11-20 | 北京理工大学 | 一种低温离子液体中制备三氯化钛粉体的装置及方法 |
| EP4474498A3 (en) * | 2020-07-10 | 2025-04-02 | NSGI Non-Ferrous Metals Inc. | Processing of titaniferous ores and minerals |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1985000160A1 (en) * | 1983-06-27 | 1985-01-17 | Occidental Research Corporation | Process for making titanium metal from titanium ore |
| JPH01252531A (ja) * | 1987-12-04 | 1989-10-09 | Nkk Corp | フッ化チタンの製造方法 |
| US4917872A (en) * | 1987-12-04 | 1990-04-17 | Nkk Corporation | Method for producing titanium fluoride |
| JPH062917B2 (ja) * | 1988-05-18 | 1994-01-12 | 日本鋼管株式会社 | 金属チタンの製造方法 |
| NZ231769A (en) * | 1988-12-20 | 1991-01-29 | Univ Melbourne | Production of tif 4 from ore containing tio 2 |
| WO1992014851A1 (en) * | 1991-02-21 | 1992-09-03 | The University Of Melbourne | Process for the production of metallic titanium and intermediates useful in the processing of ilmenite and related minerals |
| JP4257467B2 (ja) * | 1999-03-18 | 2009-04-22 | 住友金属工業株式会社 | チタンの回収方法 |
| JP3800122B2 (ja) * | 2002-04-04 | 2006-07-26 | 住友金属工業株式会社 | チタンのフッ化物イオンを含む水溶液中の不純物金属イオンの除去方法 |
| CN100507032C (zh) * | 2005-01-27 | 2009-07-01 | 派鲁克（私人）有限公司 | 制备钛的方法 |
| CN101016167A (zh) * | 2006-02-09 | 2007-08-15 | 朱作远 | 预热氯气低温氯化法高纯TiCl4生产技术 |
-
2008
- 2008-12-29 BR BRPI0822138-3A patent/BRPI0822138A2/pt not_active IP Right Cessation
- 2008-12-29 PT PT08871063T patent/PT2244980E/pt unknown
- 2008-12-29 JP JP2010541857A patent/JP5370692B2/ja not_active Expired - Fee Related
- 2008-12-29 NZ NZ586672A patent/NZ586672A/en not_active IP Right Cessation
- 2008-12-29 CN CN2008801247216A patent/CN101918319B/zh not_active Expired - Fee Related
- 2008-12-29 ES ES08871063T patent/ES2375236T3/es active Active
- 2008-12-29 US US12/811,981 patent/US20100278685A1/en not_active Abandoned
- 2008-12-29 EA EA201001160A patent/EA017080B1/ru not_active IP Right Cessation
- 2008-12-29 AU AU2008348005A patent/AU2008348005B2/en not_active Ceased
- 2008-12-29 WO PCT/IB2008/055559 patent/WO2009090513A1/en not_active Ceased
- 2008-12-29 MX MX2010007653A patent/MX2010007653A/es active IP Right Grant
- 2008-12-29 PL PL08871063T patent/PL2244980T3/pl unknown
- 2008-12-29 MY MYPI2010004095A patent/MY147802A/en unknown
- 2008-12-29 KR KR1020107017065A patent/KR20100125237A/ko not_active Ceased
- 2008-12-29 AT AT08871063T patent/ATE526289T1/de not_active IP Right Cessation
- 2008-12-29 CA CA2712116A patent/CA2712116C/en not_active Expired - Fee Related
- 2008-12-29 UA UAA201010137A patent/UA98372C2/ru unknown
- 2008-12-29 EP EP08871063A patent/EP2244980B1/en not_active Not-in-force
-
2009
- 2009-01-12 AR ARP090100091A patent/AR070155A1/es not_active Application Discontinuation
- 2009-01-12 CL CL2009000046A patent/CL2009000046A1/es unknown
-
2010
- 2010-07-13 EG EG2010071182A patent/EG26459A/en active
- 2010-08-05 ZA ZA2010/05616A patent/ZA201005616B/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| AU2008348005B2 (en) | 2012-11-01 |
| EA017080B1 (ru) | 2012-09-28 |
| JP5370692B2 (ja) | 2013-12-18 |
| EG26459A (en) | 2013-11-13 |
| CA2712116A1 (en) | 2009-07-23 |
| EP2244980B1 (en) | 2011-09-28 |
| BRPI0822138A2 (pt) | 2015-06-23 |
| AU2008348005A1 (en) | 2009-07-23 |
| EA201001160A1 (ru) | 2011-02-28 |
| KR20100125237A (ko) | 2010-11-30 |
| CN101918319B (zh) | 2013-01-09 |
| ZA201005616B (en) | 2011-04-28 |
| AR070155A1 (es) | 2010-03-17 |
| PL2244980T3 (pl) | 2012-02-29 |
| MY147802A (en) | 2013-01-31 |
| ES2375236T3 (es) | 2012-02-28 |
| NZ586672A (en) | 2011-06-30 |
| ATE526289T1 (de) | 2011-10-15 |
| CA2712116C (en) | 2013-06-25 |
| PT2244980E (pt) | 2011-12-21 |
| EP2244980A1 (en) | 2010-11-03 |
| CN101918319A (zh) | 2010-12-15 |
| JP2011509905A (ja) | 2011-03-31 |
| WO2009090513A1 (en) | 2009-07-23 |
| US20100278685A1 (en) | 2010-11-04 |
| MX2010007653A (es) | 2011-02-23 |
| CL2009000046A1 (es) | 2009-12-18 |
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