ATE107272T1 - Reinigung von alkylglyoxylate. - Google Patents

Reinigung von alkylglyoxylate.

Info

Publication number: ATE107272T1
Authority: AT; Austria
Prior art keywords: purification; streams; alkyl glyoxylate; oxidation; acid
Prior art date: 1988-07-25

Application number

AT89870115T

Other languages

English (en)

Inventor

Dario Ricardo Cova

John Michael Thorman

Original Assignee

Monsanto Co

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1988-07-25

Filing date

1989-07-24

Publication date

1994-07-15

1989-07-24 Application filed by Monsanto Co filed Critical Monsanto Co

1994-07-15 Application granted granted Critical

1994-07-15 Publication of ATE107272T1 publication Critical patent/ATE107272T1/de

Links

HHLFWLYXYJOTON-UHFFFAOYSA-N glyoxylic acid Chemical compound OC(=O)C=O HHLFWLYXYJOTON-UHFFFAOYSA-N 0.000 title abstract 3
238000000746 purification Methods 0.000 title 1
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 abstract 3
AEMRFAOFKBGASW-UHFFFAOYSA-N Glycolic acid Chemical compound OCC(O)=O AEMRFAOFKBGASW-UHFFFAOYSA-N 0.000 abstract 2
238000007254 oxidation reaction Methods 0.000 abstract 2
AEMRFAOFKBGASW-UHFFFAOYSA-M Glycolate Chemical compound OCC([O-])=O AEMRFAOFKBGASW-UHFFFAOYSA-M 0.000 abstract 1
239000002253 acid Substances 0.000 abstract 1
150000007513 acids Chemical class 0.000 abstract 1
125000005907 alkyl ester group Chemical group 0.000 abstract 1
239000006227 byproduct Substances 0.000 abstract 1
238000004821 distillation Methods 0.000 abstract 1
238000004519 manufacturing process Methods 0.000 abstract 1
238000000034 method Methods 0.000 abstract 1
230000003647 oxidation Effects 0.000 abstract 1

Classifications

- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/22—Evaporating by bringing a thin layer of the liquid into contact with a heated surface
- B01D1/222—In rotating vessels; vessels with movable parts
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
- B01D3/146—Multiple effect distillation
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
- B01D3/36—Azeotropic distillation
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
- B01D5/0078—Condensation of vapours; Recovering volatile solvents by condensation characterised by auxiliary systems or arrangements
- B01D5/0093—Removing and treatment of non condensable gases
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
- C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S203/00—Distillation: processes, separatory
- Y10S203/20—Power plant
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S203/00—Distillation: processes, separatory
- Y10S203/90—Particular type of heating

Landscapes

Chemical & Material Sciences (AREA)
Chemical Kinetics & Catalysis (AREA)
Organic Chemistry (AREA)
Crystallography & Structural Chemistry (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Polysaccharides And Polysaccharide Derivatives (AREA)

AT89870115T 1988-07-25 1989-07-24 Reinigung von alkylglyoxylate. ATE107272T1 (de)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
US07/224,045 US4867849A (en)	1988-07-25	1988-07-25	Purification of alkyl glyoxylate

Publications (1)

Publication Number	Publication Date
ATE107272T1 true ATE107272T1 (de)	1994-07-15

Family

ID=22839075

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
AT89870115T ATE107272T1 (de)	1988-07-25	1989-07-24	Reinigung von alkylglyoxylate.

Country Status (7)

Country	Link
US (1)	US4867849A (de)
EP (1)	EP0353215B1 (de)
JP (1)	JPH0745435B2 (de)
AT (1)	ATE107272T1 (de)
CA (1)	CA1324103C (de)
DE (1)	DE68916123T2 (de)
ES (1)	ES2013588T3 (de)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
AT392638B (de) *	1989-06-05	1991-05-10	Chemie Linz Gmbh	Verfahren zur kontinuierlichen herstellung einer konzentrierten waessrigen loesung von glyoxylsaeure
US5217582A (en) *	1990-06-20	1993-06-08	E. I. Du Pont De Nemours And Company	Process for the isolation of alkyl glyoxylate
JP3150909B2 (ja) *	1996-09-05	2001-03-26	株式会社日本触媒	グリオキシル酸エステル類の精製方法
US6286335B1 (en) *	1999-09-03	2001-09-11	Air Products And Chemicals, Inc.	Processes for multicomponent separation
NL1013682C2 (nl) *	1999-11-26	2001-05-30	Purac Biochem Bv	Werkwijze en inrichting voor het zuiveren van een waterige oplossing van melkzuur.
US9114328B2 (en)	2012-05-16	2015-08-25	Eastman Chemical Company	Reactive distillation of a carboxylic acid and a glycol
US9040748B2 (en)	2012-06-08	2015-05-26	Eastman Chemical Company	Hydrocarboxylation of aqueous formaldehyde using a dehydrating recycle stream to decrease water concentration
DE102013222343A1 (de)	2013-11-04	2015-05-07	Matthias Enzenhofer	Vorrichtung und Verfahren für den Kontakt einer Gasphase mit einem flüssigen Medium

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US1627091A (en) *	1923-03-05	1927-05-03	Boehringer Sohn Ingelheim	Making keto and aldo aliphatic carboxylic acids
US3476656A (en) *	1968-06-07	1969-11-04	Universal Oil Prod Co	Fractional distillation and recovery of styrene containing sulfur with subsequent bottoms separation
FR2383911A1 (fr) *	1977-03-17	1978-10-13	Hoechst France	Procede permettant d'augmenter les rendements en hemiacetal-esters de l'acide glyoxylique au cours de leur obtention ou leurs taux de recuperation dans les milieux les contenant
US4144226A (en) *	1977-08-22	1979-03-13	Monsanto Company	Polymeric acetal carboxylates
US4234739A (en) *	1978-12-05	1980-11-18	Stauffer Chemical Company	Method for preparing glyoxylic acids and derivatives thereof
DE2904775C2 (de) *	1979-02-08	1985-03-21	Hoechst Ag, 6230 Frankfurt	Verfahren zur Herstellung von Glyoxylsäureestern
JPS57176929A (en) *	1981-04-24	1982-10-30	Nippon Synthetic Chem Ind Co Ltd:The	Preparation of glyoxylic ester
DE3323372A1 (de) *	1983-06-29	1985-01-10	Hoechst Ag, 6230 Frankfurt	Verfahren zur herstellung eines glyoxylsaeureesters
US4502923A (en) *	1983-10-06	1985-03-05	Monsanto Company	Production of high purity alkyl glyoxylate by plural stage distillation
JPS61109221A (ja) *	1984-10-31	1986-05-27	田中貴金属工業株式会社	孔あき型クラツドボタン接点の製造方法
DE3446528A1 (de) *	1984-12-20	1986-06-26	Hoechst Ag, 6230 Frankfurt	Verfahren zur herstellung von glyoxylsaeurehemiacetalestern
DE3602274A1 (de) *	1986-01-25	1987-07-30	Hoechst Ag	Halbacetale von glyoxylsaeureestern sowie verfahren zur isolierung von glyoxylsaeureestern

1988
- 1988-07-25 US US07/224,045 patent/US4867849A/en not_active Expired - Lifetime
1989
- 1989-07-24 AT AT89870115T patent/ATE107272T1/de not_active IP Right Cessation
- 1989-07-24 ES ES89870115T patent/ES2013588T3/es not_active Expired - Lifetime
- 1989-07-24 JP JP1189028A patent/JPH0745435B2/ja not_active Expired - Lifetime
- 1989-07-24 EP EP89870115A patent/EP0353215B1/de not_active Expired - Lifetime
- 1989-07-24 CA CA000606487A patent/CA1324103C/en not_active Expired - Fee Related
- 1989-07-24 DE DE68916123T patent/DE68916123T2/de not_active Expired - Fee Related

Also Published As

Publication number	Publication date
US4867849A (en)	1989-09-19
DE68916123T2 (de)	1994-12-01
JPH0745435B2 (ja)	1995-05-17
EP0353215A3 (en)	1990-08-08
ES2013588A4 (es)	1990-05-16
JPH0273040A (ja)	1990-03-13
EP0353215A2 (de)	1990-01-31
CA1324103C (en)	1993-11-09
DE68916123D1 (de)	1994-07-21
EP0353215B1 (de)	1994-06-15
ES2013588T3 (es)	1994-08-01

Legal Events

Date	Code	Title
1995-02-15	UEP	Publication of translation of european patent specification
2000-12-15	EEIH	Change in the person of patent owner
2002-11-15	EEIH	Change in the person of patent owner
2003-04-15	REN	Ceased due to non-payment of the annual fee

Publication	Publication Date	Title
DE69327085D1 (de)	1999-12-30	Herstellung von Polysuccinimid durch thermische Polymerisation von Maleamicsäure
ATE166044T1 (de)	1998-05-15	Verfahren zur herstellung von halomethyl-estern von alifatischer carbonsäure
ATE94531T1 (de)	1993-10-15	Verfahren zur kontinuierlichen herstellung von leichten acrylaten.
ATE107272T1 (de)	1994-07-15	Reinigung von alkylglyoxylate.
FR2523961B1 (fr)	1985-08-30	Procede de preparation d'un alpha-amino-acide libre l
ATE25264T1 (de)	1987-02-15	Verfahren zur herstellung von fettsaeurealkylestern mit verbesserter verarbeitbarkeit.
JPS5498718A (en)	1979-08-03	Recovery of acrylic acid
EP0307472A4 (de)	1989-06-27	Immunogenes produkt, erhalten durch expression in einer rekombinanten hefe, und verfahren zu seiner reinigung.
NO903726L (no)	1991-03-13	Rensing av 1,1-diklor-1-fluoretan.
ATE45346T1 (de)	1989-08-15	Herstellungsverfahren von tetrahydro-1,1,2,2perfluoralkanolen und ihren estern.
KR960017611A (ko)	1996-06-17	미정제 (메트) 아크릴산의 정제 방법
ATE161583T1 (de)	1998-01-15	Verfahren zur herstellung von optisch aktiven glycidat-estern
ATE133160T1 (de)	1996-02-15	Verfahren zur herstellung von einer alpha- aminosäure, und dem entsprechenden ester und amid
ATE118779T1 (de)	1995-03-15	Diastereoselektive herstellung von phosphinsäureestern.
DE68906097D1 (de)	1993-05-27	Verfahren zur herstellung von ethercarbonsaeuren.
MX166774B (es)	1993-02-03	Metodo mejorado para producir acrilato de etilo
ATE73756T1 (de)	1992-04-15	Verfahren zur reinigung von alpha-substituierten essigsaeuren.
DE69204983D1 (de)	1995-10-26	Verfahren zur Herstellung von Cyclopropylmethylketon.
DE3778821D1 (de)	1992-06-11	Verfahren zur herstellung von 6-hydroxy-2-naphtonen.
ATE65490T1 (de)	1991-08-15	Herstellungsverfahren von optisch aktiven milchsaeureestern.
ATE12391T1 (de)	1985-04-15	Verfahren zur herstellung von tetronsaeure.
FR2429613A1 (fr)	1980-01-25	Procede pour purifier des gaz de recyclage contenant de l'oxygene et provenant d'une ozonisation
NO170756C (no)	1992-12-02	Fremgangsmaate for separering av karboksylsyrer
GB1467936A (en)	1977-03-23	Process for purifying the waste water from the production of polybasic carboxylic acid esters
ATA135689A (de)	1990-09-15	Verfahren zur herstellung lagerstabiler laevulinsaeure