ATE120742T1 - Verfahren zur herstellung von e-caprolacton. - Google Patents

Verfahren zur herstellung von e-caprolacton.

Info

Publication number: ATE120742T1
Authority: AT; Austria
Prior art keywords: mole; caprolactone; cyclohexanone; hydrogen peroxide; less
Prior art date: 1990-04-25

Application number

AT91303594T

Other languages

English (en)

Inventor

Yukio C O Ube Chemical F Inaba

Kogushi

Yohsuke C O Ube Chemical Ueno

Takafumi C O Ube Chem Hirakawa

Kogushi Oaza

Suzuo C O Ube Chemic Takiguchi

Original Assignee

Atochem Elf Sa

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1990-04-25

Filing date

1991-04-22

Publication date

1995-04-15

1991-04-22 Application filed by Atochem Elf Sa filed Critical Atochem Elf Sa

1995-04-15 Application granted granted Critical

1995-04-15 Publication of ATE120742T1 publication Critical patent/ATE120742T1/de

Links

PAPBSGBWRJIAAV-UHFFFAOYSA-N ε-Caprolactone Chemical compound O=C1CCCCCO1 PAPBSGBWRJIAAV-UHFFFAOYSA-N 0.000 title abstract 3
238000004519 manufacturing process Methods 0.000 title abstract 2
JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 abstract 6
MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 abstract 4
SCKXCAADGDQQCS-UHFFFAOYSA-N Performic acid Chemical compound OOC=O SCKXCAADGDQQCS-UHFFFAOYSA-N 0.000 abstract 3
KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 abstract 2
239000004327 boric acid Substances 0.000 abstract 2
239000003054 catalyst Substances 0.000 abstract 2
150000001732 carboxylic acid derivatives Chemical class 0.000 abstract 1
239000003960 organic solvent Substances 0.000 abstract 1
230000001590 oxidative effect Effects 0.000 abstract 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D315/00—Heterocyclic compounds containing rings having one oxygen atom as the only ring hetero atom according to more than one of groups C07D303/00 - C07D313/00
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C407/00—Preparation of peroxy compounds
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C407/00—Preparation of peroxy compounds
- C07C407/003—Separation; Purification; Stabilisation; Use of additives
- C07C407/006—Stabilisation; Use of additives

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Pyrane Compounds (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)

AT91303594T 1990-04-25 1991-04-22 Verfahren zur herstellung von e-caprolacton. ATE120742T1 (de)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP2107674A JPH0798816B2 (ja)	1990-04-25	1990-04-25	ε―カプロラクトンの製造法

Publications (1)

Publication Number	Publication Date
ATE120742T1 true ATE120742T1 (de)	1995-04-15

Family

ID=14465118

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
AT91303594T ATE120742T1 (de)	1990-04-25	1991-04-22	Verfahren zur herstellung von e-caprolacton.

Country Status (7)

Country	Link
US (1)	US5250707A (de)
EP (1)	EP0454397B1 (de)
JP (1)	JPH0798816B2 (de)
CN (1)	CN1035379C (de)
AT (1)	ATE120742T1 (de)
CA (1)	CA2040270A1 (de)
DE (1)	DE69108600T2 (de)

Families Citing this family (30)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
WO1999014190A1 (fr) *	1997-09-16	1999-03-25	Daicel Chemical Industries, Ltd.	Procede de preparation de peroxyacide d'equilibre et procede de production de lactone
JP2004143047A (ja) *	2002-10-22	2004-05-20	Daicel Chem Ind Ltd	ε−カプロラクトンの製造方法
JP2005139110A (ja) *	2003-11-06	2005-06-02	Ecology Maximum Co Ltd	ε−カプロラクトンの製造方法、並びに、ε−カプロラクトンを用いたポリカプロラクトンの製造方法
JP4297152B2 (ja)	2006-10-06	2009-07-15	トヨタ自動車株式会社	車両前部構造
US8809392B2 (en)	2008-03-28	2014-08-19	Ecolab Usa Inc.	Sulfoperoxycarboxylic acids, their preparation and methods of use as bleaching and antimicrobial agents
CA2715175C (en)	2008-03-28	2017-11-21	Ecolab Inc.	Sulfoperoxycarboxylic acids, their preparation and methods of use as bleaching and antimicrobial agents
US12203056B2 (en)	2008-03-28	2025-01-21	Ecolab Usa Inc.	Sulfoperoxycarboxylic acids, their preparation and methods of use as bleaching and antimicrobial agents
US8871807B2 (en)	2008-03-28	2014-10-28	Ecolab Usa Inc.	Detergents capable of cleaning, bleaching, sanitizing and/or disinfecting textiles including sulfoperoxycarboxylic acids
CN102584775B (zh) *	2011-01-12	2015-04-22	中国石油化工集团公司	制备ε-己内酯的方法
CN102584776A (zh) *	2011-01-12	2012-07-18	中国石油化工集团公司	一种制备ε-己内酯的方法
CN102304117A (zh) *	2011-09-19	2012-01-04	武汉理工大学	一种合成ε-己内酯的方法
US9321664B2 (en)	2011-12-20	2016-04-26	Ecolab Usa Inc.	Stable percarboxylic acid compositions and uses thereof
CN106396037B (zh)	2012-03-30	2019-10-15	艺康美国股份有限公司	过乙酸/过氧化氢和过氧化物还原剂用于处理钻井液、压裂液、回流水和排放水的用途
US20140256811A1 (en)	2013-03-05	2014-09-11	Ecolab Usa Inc.	Efficient stabilizer in controlling self accelerated decomposition temperature of peroxycarboxylic acid compositions with mineral acids
US10165774B2 (en)	2013-03-05	2019-01-01	Ecolab Usa Inc.	Defoamer useful in a peracid composition with anionic surfactants
CN104003972A (zh) *	2014-04-28	2014-08-27	安徽红太阳新材料有限公司	一种制备己内酯的方法
CN104130234A (zh) *	2014-07-25	2014-11-05	南京红太阳新材料有限公司	一种制备己内酯的方法
US10172351B2 (en)	2015-09-04	2019-01-08	Ecolab Usa Inc.	Performic acid on-site generator and formulator
CN105315442A (zh) *	2015-12-01	2016-02-10	仇颖超	一种淀粉改性聚己内酯塑料材料的制备方法
GB2548138A (en) *	2016-03-09	2017-09-13	Perstorp Ab	Production equipment (II) for production of a caprolactone
GB2548137A (en) *	2016-03-09	2017-09-13	Perstorp Ab	Production equipment (I) for production of a caprolactone
CN107163018A (zh) *	2017-06-23	2017-09-15	中山大学惠州研究院	一种分离ε‑己内酯的精馏方法
AU2019325568B2 (en)	2018-08-22	2022-03-10	Ecolab Usa Inc.	Hydrogen peroxide and peracid stabilization with molecules based on a pyridine carboxylic acid at C-3, -4 or -5
US11185893B2 (en)	2019-05-31	2021-11-30	Ecolab Usa Inc.	Peracid compositions with conductivity monitoring capability
WO2021026410A1 (en)	2019-08-07	2021-02-11	Ecolab Usa Inc.	Polymeric and solid-supported chelators for stabilization of peracid-containing compositions
CN111763192B (zh) *	2020-07-14	2023-09-12	湖南瑞源石化股份有限公司	一种ε-己内酯的制备方法及其装置
CN115490623B (zh) *	2021-06-18	2024-08-30	中国石油化工股份有限公司	合成无水过氧有机酸的方法和合成ε-己内酯的方法
CN114835669A (zh) *	2022-03-23	2022-08-02	华东理工大学	高纯度ε-己内酯的微流控合成方法
CN115812713B (zh) *	2022-11-29	2024-03-29	湖南聚仁新材料股份公司	消毒剂和己内酯生产过程中联产过氧羧酸消毒剂的方法
CN119588424B (zh) *	2023-09-11	2026-03-24	中国石油化工股份有限公司	一种催化剂组合物以及制备过氧酸的方法

Family Cites Families (19)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US3064008A (en) *		1962-11-13		I i i i i i
US2914556A (en) *	1956-04-13	1959-11-24	Union Carbide Corp	Preparation of lactone adducts
US3189619A (en) *	1962-09-25	1965-06-15	Exxon Research Engineering Co	Synthesis of carpolactone
US3317563A (en) *	1963-12-26	1967-05-02	Celanese Corp	Preparation of epsilon-caprolactone
FR1474098A (fr) *	1966-01-25	1967-03-24	Electro Chimie Soc D	Procédé de préparation d'epsilon-caprolactone
FR1474903A (fr) *	1966-02-12	1967-03-31	Electrochimie Soc	Procédé de préparation d'epsiloncaprolactone
GB1140184A (en) *	1967-06-13	1969-01-15	Chisso Corp	Process for manufacturing e-caprolactone
US3624258A (en) *	1969-03-22	1971-11-30	Teijin Ltd	Process for the preparation of {68 -caprolactone
DE2038455A1 (de) *	1970-08-01	1972-02-10	Bayer Ag	Verfahren zur Herstellung von epsilon-Caprolacton
US3781350A (en) *	1971-07-09	1973-12-25	Teijin Ltd	Process for preparation of omega-hydroxy saturated aliphatic monocarboxylic acids
US3825570A (en) *	1971-11-02	1974-07-23	Teijin Ltd	Process for the preparation of epsilon-caprolactone
US4183863A (en) *	1978-04-18	1980-01-15	Union Carbide Corporation	Conversion of cyclohexanol to ε-caprolactone
DE2920436A1 (de) *	1979-05-19	1980-12-04	Bayer Ag	Verfahren zur herstellung von epsilon -caprolacton
DE2934659A1 (de) *	1979-08-28	1981-03-19	Bayer Ag, 5090 Leverkusen	Verfahren zur herstellung von sehr reinem epsilon -caprolacton
FR2500453A1 (fr) *	1981-02-20	1982-08-27	Ugine Kuhlmann	Procede d'obtention de l'epsilon-caprolactone
FR2519985A1 (fr) *	1982-01-15	1983-07-22	Ugine Kuhlmann	Procede perfectionne de fabrication de l'e-caprolactone
JPH0237919B2 (ja) *	1983-05-04	1990-08-28	Mitsubishi Chem Ind	Kapurorakutonnoseizohoho
JPS61200120A (ja) *	1985-03-01	1986-09-04	Nippon Shokubai Kagaku Kogyo Co Ltd	ラクトン変性化合物の製造方法
DE3823213A1 (de) *	1988-07-08	1990-01-11	Basf Ag	Verfahren zur herstellung von caprolacton

1990
- 1990-04-25 JP JP2107674A patent/JPH0798816B2/ja not_active Expired - Fee Related
1991
- 1991-04-22 EP EP91303594A patent/EP0454397B1/de not_active Expired - Lifetime
- 1991-04-22 AT AT91303594T patent/ATE120742T1/de not_active IP Right Cessation
- 1991-04-22 US US07/689,151 patent/US5250707A/en not_active Expired - Fee Related
- 1991-04-22 DE DE69108600T patent/DE69108600T2/de not_active Expired - Fee Related
- 1991-04-24 CA CA002040270A patent/CA2040270A1/en not_active Abandoned
- 1991-10-25 CN CN91109988A patent/CN1035379C/zh not_active Expired - Fee Related

Also Published As

Publication number	Publication date
DE69108600D1 (de)	1995-05-11
JPH0798816B2 (ja)	1995-10-25
JPH049378A (ja)	1992-01-14
EP0454397A1 (de)	1991-10-30
CN1035379C (zh)	1997-07-09
DE69108600T2 (de)	1996-01-11
EP0454397B1 (de)	1995-04-05
US5250707A (en)	1993-10-05
CA2040270A1 (en)	1991-10-26
CN1071923A (zh)	1993-05-12

Legal Events

Date	Code	Title	Description
1995-10-15	RER	Ceased as to paragraph 5 lit. 3 law introducing patent treaties

Publication	Publication Date	Title
DE69108600D1 (de)	1995-05-11	Verfahren zur Herstellung von e-Caprolacton.
DE69517301D1 (de)	2000-07-06	Verfahren zur herstellung von aromatischen carbonsäuren mit effektiver energierückgewinnung
DE68915672D1 (de)	1994-07-07	Verfahren zur Herstellung von Phenol und Wiedergewinnung von Propylen daraus.
MX9102659A (es)	1992-06-01	Oxidacion de celulosa mediante una solucion de hidrocarburo perfluorado.
ATE74333T1 (de)	1992-04-15	Katalytisches verfahren zur herstellung von wasserstoffperoxyd aus wasserstoff und sauerstoff mittels eines bromidpromotor.
ATE47381T1 (de)	1989-11-15	Verfahren zur herstellung von ameisensaeure.
ATE82576T1 (de)	1992-12-15	Verfahren zur herstellung von nphosphonmethylglyzin.
ATE194614T1 (de)	2000-07-15	Verfahren zur herstellung von 3- arylbenzofuranonen
ATE271070T1 (de)	2004-07-15	Verfahren zur herstellung eines metallocen- katalysatorsystems
DE3772847D1 (de)	1991-10-17	Verfahren zur herstellung von 2-methyl-1,4-naphthochinon.
ATE156134T1 (de)	1997-08-15	Verfahren zur herstellung von alkylpolyglukosiden
DE58902856D1 (de)	1993-01-14	Verfahren zur herstellung von o-substituierten hydroxylaminen.
ATE112553T1 (de)	1994-10-15	Verfahren zur herstellung von kohlensäureestern.
DE69700009D1 (de)	1998-07-09	Verfahren zur Herstellung von Peressigsäure
ATE131149T1 (de)	1995-12-15	Verfahren zur herstellung von 5-(2,4- difluorphenyl)-salizylsäure.
DE3770952D1 (de)	1991-08-01	Verfahren zur herstellung von hydroxylaminen.
ATE119154T1 (de)	1995-03-15	Verfahren zur herstellung von 2-chlor-5- chlormethyl-pyridin.
ATE162172T1 (de)	1998-01-15	Verfahren zur kontinuierlichen herstellung von terpenestern
DE69005309D1 (de)	1994-01-27	Verfahren zur herstellung von peroxykarbonsäuren unter verwendung eines enzymkatalysators.
DE3889041D1 (de)	1994-05-19	Herstellung von Immunonähe-Katalysatoren.
ATE14427T1 (de)	1985-08-15	Verfahren zur herstellung von epsiloncaprolaktam.
DE68900323D1 (de)	1991-11-21	Verfahren zur herstellung von alkylpyruvaten.
DE3767397D1 (de)	1991-02-21	Verfahren zur herstellung von kaliumnitrat.
ATE203525T1 (de)	2001-08-15	Verfahren zur herstellung von 4-amino-1,2,4- triazolen
ATE190306T1 (de)	2000-03-15	Verfahren zur herstellung von 2-chlor-5- aminomethylpyridin