ATE200470T1 - Verfahren zur herstellung von dinitramidsäure und dinitramidsalze - Google Patents

Verfahren zur herstellung von dinitramidsäure und dinitramidsalze

Info

Publication number: ATE200470T1
Authority: AT; Austria
Prior art keywords: acid; pct; salt; salts; dinitramide salt
Prior art date: 1995-08-08

Application number

AT96925240T

Other languages

English (en)

Inventor

Abraham Langlet

Henric Oestmark

Niklas Wingborg

Original Assignee

Foersvarets Forskningsanstalt

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1995-08-08

Filing date

1996-07-26

Publication date

2001-04-15

1995-08-08 Priority claimed from SE9502783A external-priority patent/SE9502783D0/xx

1996-07-26 Application filed by Foersvarets Forskningsanstalt filed Critical Foersvarets Forskningsanstalt

2001-04-15 Application granted granted Critical

2001-04-15 Publication of ATE200470T1 publication Critical patent/ATE200470T1/de

Links

MJVUDZGNBKFOBF-UHFFFAOYSA-N n-nitronitramide Chemical class [O-][N+](=O)N[N+]([O-])=O MJVUDZGNBKFOBF-UHFFFAOYSA-N 0.000 title abstract 6
239000002253 acid Substances 0.000 title abstract 5
238000004519 manufacturing process Methods 0.000 title 1
QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 4
WFDIJRYMOXRFFG-UHFFFAOYSA-N Acetic anhydride Chemical compound CC(=O)OC(C)=O WFDIJRYMOXRFFG-UHFFFAOYSA-N 0.000 abstract 3
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 abstract 3
WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 abstract 3
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 abstract 3
239000003795 chemical substances by application Substances 0.000 abstract 3
150000003839 salts Chemical class 0.000 abstract 3
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 2
GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 abstract 2
229910006069 SO3H Inorganic materials 0.000 abstract 2
229910021529 ammonia Inorganic materials 0.000 abstract 2
150000001768 cations Chemical class 0.000 abstract 2
239000002184 metal Substances 0.000 abstract 2
238000000034 method Methods 0.000 abstract 2
239000000203 mixture Substances 0.000 abstract 2
238000006386 neutralization reaction Methods 0.000 abstract 2
229910017604 nitric acid Inorganic materials 0.000 abstract 2
-1 nitrogen-containing cation Chemical class 0.000 abstract 2
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract 1
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 1
150000001298 alcohols Chemical class 0.000 abstract 1
239000007864 aqueous solution Substances 0.000 abstract 1
150000001875 compounds Chemical class 0.000 abstract 1
238000010828 elution Methods 0.000 abstract 1
230000003472 neutralizing effect Effects 0.000 abstract 1
230000000802 nitrating effect Effects 0.000 abstract 1
238000006396 nitration reaction Methods 0.000 abstract 1
150000002892 organic cations Chemical class 0.000 abstract 1
239000007800 oxidant agent Substances 0.000 abstract 1
239000003495 polar organic solvent Substances 0.000 abstract 1
238000011084 recovery Methods 0.000 abstract 1
239000011833 salt mixture Substances 0.000 abstract 1
239000000741 silica gel Substances 0.000 abstract 1
229910002027 silica gel Inorganic materials 0.000 abstract 1
239000004449 solid propellant Substances 0.000 abstract 1
IIACRCGMVDHOTQ-UHFFFAOYSA-N sulfamic acid Chemical compound NS(O)(=O)=O IIACRCGMVDHOTQ-UHFFFAOYSA-N 0.000 abstract 1
239000001117 sulphuric acid Substances 0.000 abstract 1
235000011149 sulphuric acid Nutrition 0.000 abstract 1
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
239000010457 zeolite Substances 0.000 abstract 1

Classifications

- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B41/00—Compositions containing a nitrated metallo-organic compound
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B25/00—Compositions containing a nitrated organic compound
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B31/00—Compositions containing an inorganic nitrogen-oxygen salt

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Inorganic Chemistry (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

AT96925240T 1995-08-08 1996-07-26 Verfahren zur herstellung von dinitramidsäure und dinitramidsalze ATE200470T1 (de)

Applications Claiming Priority (3)

Application Number	Priority Date	Filing Date	Title
SE9502783A SE9502783D0 (sv)	1995-08-08	1995-08-08	Sätt att framställa dinitramidsyra och salter därav
SE9503326A SE516719C2 (sv)	1995-08-08	1995-09-26	Sätt att framställa dinitramidsyra och salter därav
PCT/SE1996/000976 WO1997006099A1 (en)	1995-08-08	1996-07-26	Method of preparing dinitramidic acid and salts thereof

Publications (1)

Publication Number	Publication Date
ATE200470T1 true ATE200470T1 (de)	2001-04-15

Family

ID=26662358

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
AT96925240T ATE200470T1 (de)	1995-08-08	1996-07-26	Verfahren zur herstellung von dinitramidsäure und dinitramidsalze

Country Status (14)

Country	Link
US (1)	US5976483A (de)
EP (1)	EP0843647B1 (de)
JP (1)	JP4118947B2 (de)
AT (1)	ATE200470T1 (de)
AU (1)	AU703767B2 (de)
BR (1)	BR9609993A (de)
CA (1)	CA2227625C (de)
DE (1)	DE69612497T2 (de)
ES (1)	ES2159039T3 (de)
IL (1)	IL122880A (de)
NO (1)	NO321198B1 (de)
SE (1)	SE516719C2 (de)
TR (1)	TR199800129T1 (de)
WO (1)	WO1997006099A1 (de)

Families Citing this family (21)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
SE511285C2 (sv) *	1997-04-29	1999-09-06	Foersvarets Forskningsanstalt	Smältgjutna laddningar
SE509312C2 (sv)	1997-05-21	1999-01-11	Foersvarets Forskningsanstalt	Förening som utgöres av guanylureadinitramid, explosivämne innehållande föreningen samt användning av föreningen i gasgeneratorer.
SE512396C2 (sv) *	1997-10-28	2000-03-13	Foersvarets Forskningsanstalt	Sätt att framställa prills av ammoniumdinitramid (ADN)
SE511675C2 (sv) *	1998-03-10	1999-11-08	Foersvarets Forskningsanstalt	Sätt att framställa dinitramidsalter
EP0950648A1 (de) *	1998-04-15	1999-10-20	Nederlandse Organisatie Voor Toegepast-Natuurwetenschappelijk Onderzoek Tno	Monergoles flüssiges Treibstoffsystem
US6984273B1 (en) *	1999-07-29	2006-01-10	Aerojet-General Corporation	Premixed liquid monopropellant solutions and mixtures
US6513834B1 (en)	2000-08-29	2003-02-04	Trw Inc.	Monopropellant smokeless gas generant materials
US6635131B2 (en) *	2001-03-26	2003-10-21	Trw Inc.	Gas generating material for a vehicle occupant protection apparatus
US6787119B2 (en) *	2002-03-13	2004-09-07	Council Of Scientific And Industrial Research	Process for the preparation of dinitramidic acid and salts thereof
SE526402C2 (sv) *	2004-01-21	2005-09-06	Foersvarets Materielverk	Sätt att framställa salt av dinitramidsyra
JP4500576B2 (ja) *	2004-04-01	2010-07-14	ダイセル化学工業株式会社	ガス発生剤組成物
US7526524B2 (en) *	2004-05-26	2009-04-28	At&T Intellectual Property I, L.P.	Network conferencing using method for distributed computing and/or distributed objects
US7598002B2 (en) *	2005-01-11	2009-10-06	Material Methods Llc	Enhanced electrochemical cells with solid-electrolyte interphase promoters
US7872430B2 (en) *	2005-11-18	2011-01-18	Cree, Inc.	Solid state lighting panels with variable voltage boost current sources
FR2935969B1 (fr) *	2008-09-18	2011-05-13	Snpe Materiaux Energetiques	Procede d'obtention de cristaux d'adn par cristallisation en milieu visqueux ; cristaux d'adn et les materiaux energetiques en contenant
CN102731345A (zh) *	2011-12-29	2012-10-17	湖北航天化学技术研究所	一种合成n-脒基脲二硝酰胺盐的方法
SE537747C2 (sv)	2014-01-30	2015-10-13	Totalförsvarets Forskningsinstitut	Syntes av ammoniumdinitramid, ADN
KR101702100B1 (ko) *	2015-04-07	2017-02-02	경희대학교 산학협력단	구아니딘 디나이트라마이드의 제조방법
SE541421C2 (en) *	2017-06-01	2019-09-24	Foi Grindsjoens Forskningscentrum	Synthesis of Ammonium Dinitramide (ADN)
PL3853174T3 (pl)	2018-09-17	2023-03-20	Totalförsvarets Forskningsinstitut	Synteza dinitroamidku amonu (ADN)
CN116059692B (zh) *	2021-11-03	2025-09-30	中国科学院大连化学物理研究所	一种二硝酰胺铵的可控温快速提取装置及工艺

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
BE519373A (de) *	1952-04-25
US5254324A (en) *	1990-06-18	1993-10-19	Sri International	Dinitramide salts and method of making same
US5198204A (en) *	1990-06-18	1993-03-30	Sri International	Method of forming dinitramide salts
US5316749A (en) *	1991-07-30	1994-05-31	Sri International	Process for forming ammonium dinitramide salt by reaction between ammonia and a nitronium-containing compound
US5415852A (en) *	1992-01-29	1995-05-16	Sri International	Process for forming a dinitramide salt or acid by reaction of a salt or free acid of an N(alkoxycarbonyl)N-nitroamide with a nitronium-containing compound followed by reaction of the intermediate product respectively with a base or alcohol

1995
- 1995-09-26 SE SE9503326A patent/SE516719C2/sv not_active IP Right Cessation
1996
- 1996-07-26 TR TR1998/00129T patent/TR199800129T1/xx unknown
- 1996-07-26 WO PCT/SE1996/000976 patent/WO1997006099A1/en not_active Ceased
- 1996-07-26 US US08/983,462 patent/US5976483A/en not_active Expired - Lifetime
- 1996-07-26 BR BR9609993A patent/BR9609993A/pt not_active Application Discontinuation
- 1996-07-26 IL IL12288096A patent/IL122880A/xx not_active IP Right Cessation
- 1996-07-26 JP JP50836697A patent/JP4118947B2/ja not_active Expired - Fee Related
- 1996-07-26 CA CA002227625A patent/CA2227625C/en not_active Expired - Fee Related
- 1996-07-26 AT AT96925240T patent/ATE200470T1/de not_active IP Right Cessation
- 1996-07-26 DE DE69612497T patent/DE69612497T2/de not_active Expired - Lifetime
- 1996-07-26 EP EP96925240A patent/EP0843647B1/de not_active Expired - Lifetime
- 1996-07-26 ES ES96925240T patent/ES2159039T3/es not_active Expired - Lifetime
- 1996-07-26 AU AU65396/96A patent/AU703767B2/en not_active Ceased
1998
- 1998-02-06 NO NO19980534A patent/NO321198B1/no not_active IP Right Cessation

Also Published As

Publication number	Publication date
SE9503326L (sv)	1997-02-09
WO1997006099A1 (en)	1997-02-20
IL122880A (en)	2000-10-31
BR9609993A (pt)	1999-07-06
NO980534L (no)	1998-02-06
CA2227625A1 (en)	1997-02-20
AU703767B2 (en)	1999-04-01
SE516719C2 (sv)	2002-02-19
DE69612497D1 (de)	2001-05-17
DE69612497T2 (de)	2001-10-18
AU6539696A (en)	1997-03-05
JPH11514323A (ja)	1999-12-07
JP4118947B2 (ja)	2008-07-16
SE9503326D0 (sv)	1995-09-26
CA2227625C (en)	2008-06-03
IL122880A0 (en)	1998-08-16
ES2159039T3 (es)	2001-09-16
US5976483A (en)	1999-11-02
EP0843647B1 (de)	2001-04-11
EP0843647A1 (de)	1998-05-27
TR199800129T1 (xx)	1998-04-21
NO980534D0 (no)	1998-02-06
NO321198B1 (no)	2006-04-03

Legal Events

Date	Code	Title
2002-05-15	EEIH	Change in the person of patent owner
2002-05-15	UEP	Publication of translation of european patent specification
2012-04-15	REN	Ceased due to non-payment of the annual fee

Publication	Publication Date	Title
ATE200470T1 (de)	2001-04-15	Verfahren zur herstellung von dinitramidsäure und dinitramidsalze
Nagano et al.	1995	Reactions of nitric oxide with amines in the presence of dioxygen
DE69415149D1 (de)	1999-01-21	Verfahren zur nitrierung von aromatischen verbindungen verbindungen unter milden, nicht korrosiven bedingungen
Zolfigol et al.	2000	An Efficient Method for N-Nitrosation of Secondary Amines Under Mild and Heterogeneous Conditions
IL157176A (en)	2010-02-17	A method for the purification of 2-nitro-4-methylsulfonylbenzoic acid, 2-nitro-4-methylsulfonylbenzoic acid is purified as stated, and a process for preparing a mesothorium that includes its use
DE69815399D1 (de)	2003-07-10	Verfahren zur nitrierung von aromatischen verbindungen mit hilfe eines nichtsauren nitrierungsprozesses
PL118036B1 (en)	1981-09-30	Method of reduction of nitrosating agents concentration in 1-chloro-2,6-dinitro-4-/trifluoromethyl/benzene v 1-khloro-2,6-dinitro-4/triftorometilo/benzole
Herbst et al.	1953	The nitration of 5-aminotetrazole
PT96973A (pt)	1991-10-31	Processo para a preparacao de precursores acilados de o-3-amino-3-desoxi-alfa-d-glucopiranosil (1-->6)-o-6-amino-6-desoxi-alfa-d-glucopiranosil-(1-->4)-n'-(4-amino-2-hidroxi-1-oxobutil)-2-desoxi-d-estreptamina (amicacina)
KR890001947A (ko)	1989-04-06	2,2-비스-(3- 아미노페닐)헥사플루오로프로판의 유도체 및 2.2-비스-(3.4-디아미노페닐)헥사플루오로프로판의 제조방법
KR930016387A (ko)	1993-08-26	니트로벤젠의 제조방법
US20110160450A1 (en)	2011-06-30	Explosive
RU92009774A (ru)	1996-12-20	Способ получения производных 2-р-4(5'')-нитроимидазолов
JP3205177B2 (ja)	2001-09-04	グリシンの精製法
Matsuya et al.	1997	A mild dehydrazination reaction of arylhydrazines using nitric oxide in the presence of oxygen
KR860001107A (ko)	1986-02-22	6-또는 11-치환 아포빈카민산 유도체의 제조방법
Hall et al.	1951	The Chemistry of Linear Substituted Nitroguanidines
CN116059693A (zh)	2023-05-05	一种二硝酰胺铵水溶液的合成方法
KR800000975B1 (ko)	1980-09-17	3, 3'-트리아릴메탄-디카복실산 유도체의 제법
DK0893431T3 (da)	2002-10-21	Fremgangsmåde til oprensning af dinitroaniliner
RU2068407C1 (ru)	1996-10-27	Способ получения 4- и/или 6-нитро-2-аминофенолов
RU97109023A (ru)	1999-05-10	Способ получения тетразола и его солей
Gănescu et al.	0	SOUTHERN BRAZILIAN JOURNAL OF CHEMISTRY
Ward et al.	1961	956. Nitration of the N-acyl-nitronaphthylamines
SANDSTRÖM et al.	1985	Sequence of E. coli tRNA" Using 2'-O-(3-Methoxy