IL122880A - Method of preparing dinitramidic acid and salts thereof - Google Patents

Method of preparing dinitramidic acid and salts thereof

Info

Publication number: IL122880A
Authority: IL; Israel
Prior art keywords: acid; pct; salts; salt; dinitramide salt
Prior art date: 1995-08-08

Application number

IL12288096A

Other languages

English (en)

Other versions

IL122880A0 (en

Original Assignee

Forsvarets Forsknings

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1995-08-08

Filing date

1996-07-26

Publication date

2000-10-31

1995-08-08 Priority claimed from SE9502783A external-priority patent/SE9502783D0/xx

1996-07-26 Application filed by Forsvarets Forsknings filed Critical Forsvarets Forsknings

1998-08-16 Publication of IL122880A0 publication Critical patent/IL122880A0/xx

2000-10-31 Publication of IL122880A publication Critical patent/IL122880A/xx

Links

239000002253 acid Substances 0.000 title abstract 5
150000003839 salts Chemical class 0.000 title abstract 4
238000000034 method Methods 0.000 title abstract 3
MJVUDZGNBKFOBF-UHFFFAOYSA-N n-nitronitramide Chemical class [O-][N+](=O)N[N+]([O-])=O MJVUDZGNBKFOBF-UHFFFAOYSA-N 0.000 abstract 5
QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 4
WFDIJRYMOXRFFG-UHFFFAOYSA-N Acetic anhydride Chemical compound CC(=O)OC(C)=O WFDIJRYMOXRFFG-UHFFFAOYSA-N 0.000 abstract 3
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 abstract 3
WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 abstract 3
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 abstract 3
239000003795 chemical substances by application Substances 0.000 abstract 3
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 2
GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 abstract 2
229910006069 SO3H Inorganic materials 0.000 abstract 2
229910021529 ammonia Inorganic materials 0.000 abstract 2
150000001768 cations Chemical class 0.000 abstract 2
239000002184 metal Substances 0.000 abstract 2
239000000203 mixture Substances 0.000 abstract 2
238000006386 neutralization reaction Methods 0.000 abstract 2
229910017604 nitric acid Inorganic materials 0.000 abstract 2
-1 nitrogen-containing cation Chemical class 0.000 abstract 2
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract 1
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 1
150000001298 alcohols Chemical class 0.000 abstract 1
239000007864 aqueous solution Substances 0.000 abstract 1
150000001875 compounds Chemical class 0.000 abstract 1
238000010828 elution Methods 0.000 abstract 1
230000003472 neutralizing effect Effects 0.000 abstract 1
230000000802 nitrating effect Effects 0.000 abstract 1
238000006396 nitration reaction Methods 0.000 abstract 1
150000002892 organic cations Chemical class 0.000 abstract 1
239000007800 oxidant agent Substances 0.000 abstract 1
239000003495 polar organic solvent Substances 0.000 abstract 1
238000011084 recovery Methods 0.000 abstract 1
239000011833 salt mixture Substances 0.000 abstract 1
239000000741 silica gel Substances 0.000 abstract 1
229910002027 silica gel Inorganic materials 0.000 abstract 1
239000004449 solid propellant Substances 0.000 abstract 1
IIACRCGMVDHOTQ-UHFFFAOYSA-N sulfamic acid Chemical compound NS(O)(=O)=O IIACRCGMVDHOTQ-UHFFFAOYSA-N 0.000 abstract 1
239000001117 sulphuric acid Substances 0.000 abstract 1
235000011149 sulphuric acid Nutrition 0.000 abstract 1
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
239000010457 zeolite Substances 0.000 abstract 1

Classifications

- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B41/00—Compositions containing a nitrated metallo-organic compound
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B25/00—Compositions containing a nitrated organic compound
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B31/00—Compositions containing an inorganic nitrogen-oxygen salt

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Inorganic Chemistry (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

IL12288096A 1995-08-08 1996-07-26 Method of preparing dinitramidic acid and salts thereof IL122880A (en)

Applications Claiming Priority (3)

Application Number	Priority Date	Filing Date	Title
SE9502783A SE9502783D0 (sv)	1995-08-08	1995-08-08	Sätt att framställa dinitramidsyra och salter därav
SE9503326A SE516719C2 (sv)	1995-08-08	1995-09-26	Sätt att framställa dinitramidsyra och salter därav
PCT/SE1996/000976 WO1997006099A1 (en)	1995-08-08	1996-07-26	Method of preparing dinitramidic acid and salts thereof

Publications (2)

Publication Number	Publication Date
IL122880A0 IL122880A0 (en)	1998-08-16
IL122880A true IL122880A (en)	2000-10-31

Family

ID=26662358

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
IL12288096A IL122880A (en)	1995-08-08	1996-07-26	Method of preparing dinitramidic acid and salts thereof

Country Status (14)

Country	Link
US (1)	US5976483A (de)
EP (1)	EP0843647B1 (de)
JP (1)	JP4118947B2 (de)
AT (1)	ATE200470T1 (de)
AU (1)	AU703767B2 (de)
BR (1)	BR9609993A (de)
CA (1)	CA2227625C (de)
DE (1)	DE69612497T2 (de)
ES (1)	ES2159039T3 (de)
IL (1)	IL122880A (de)
NO (1)	NO321198B1 (de)
SE (1)	SE516719C2 (de)
TR (1)	TR199800129T1 (de)
WO (1)	WO1997006099A1 (de)

Families Citing this family (21)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
SE511285C2 (sv) *	1997-04-29	1999-09-06	Foersvarets Forskningsanstalt	Smältgjutna laddningar
SE509312C2 (sv)	1997-05-21	1999-01-11	Foersvarets Forskningsanstalt	Förening som utgöres av guanylureadinitramid, explosivämne innehållande föreningen samt användning av föreningen i gasgeneratorer.
SE512396C2 (sv) *	1997-10-28	2000-03-13	Foersvarets Forskningsanstalt	Sätt att framställa prills av ammoniumdinitramid (ADN)
SE511675C2 (sv) *	1998-03-10	1999-11-08	Foersvarets Forskningsanstalt	Sätt att framställa dinitramidsalter
EP0950648A1 (de) *	1998-04-15	1999-10-20	Nederlandse Organisatie Voor Toegepast-Natuurwetenschappelijk Onderzoek Tno	Monergoles flüssiges Treibstoffsystem
US6984273B1 (en) *	1999-07-29	2006-01-10	Aerojet-General Corporation	Premixed liquid monopropellant solutions and mixtures
US6513834B1 (en)	2000-08-29	2003-02-04	Trw Inc.	Monopropellant smokeless gas generant materials
US6635131B2 (en) *	2001-03-26	2003-10-21	Trw Inc.	Gas generating material for a vehicle occupant protection apparatus
US6787119B2 (en) *	2002-03-13	2004-09-07	Council Of Scientific And Industrial Research	Process for the preparation of dinitramidic acid and salts thereof
SE526402C2 (sv)	2004-01-21	2005-09-06	Foersvarets Materielverk	Sätt att framställa salt av dinitramidsyra
JP4500576B2 (ja) *	2004-04-01	2010-07-14	ダイセル化学工業株式会社	ガス発生剤組成物
US7526524B2 (en) *	2004-05-26	2009-04-28	At&T Intellectual Property I, L.P.	Network conferencing using method for distributed computing and/or distributed objects
US7598002B2 (en) *	2005-01-11	2009-10-06	Material Methods Llc	Enhanced electrochemical cells with solid-electrolyte interphase promoters
US7872430B2 (en) *	2005-11-18	2011-01-18	Cree, Inc.	Solid state lighting panels with variable voltage boost current sources
FR2935969B1 (fr) *	2008-09-18	2011-05-13	Snpe Materiaux Energetiques	Procede d'obtention de cristaux d'adn par cristallisation en milieu visqueux ; cristaux d'adn et les materiaux energetiques en contenant
CN102731345A (zh) *	2011-12-29	2012-10-17	湖北航天化学技术研究所	一种合成n-脒基脲二硝酰胺盐的方法
SE537747C2 (sv) *	2014-01-30	2015-10-13	Totalförsvarets Forskningsinstitut	Syntes av ammoniumdinitramid, ADN
KR101702100B1 (ko) *	2015-04-07	2017-02-02	경희대학교 산학협력단	구아니딘 디나이트라마이드의 제조방법
SE541421C2 (en) *	2017-06-01	2019-09-24	Foi Grindsjoens Forskningscentrum	Synthesis of Ammonium Dinitramide (ADN)
FI3853174T3 (fi)	2018-09-17	2023-02-21		Ammoniumdinitramidin (ADN) synteesi
CN116059692B (zh) *	2021-11-03	2025-09-30	中国科学院大连化学物理研究所	一种二硝酰胺铵的可控温快速提取装置及工艺

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
NL74128C (de) *	1952-04-25
US5198204A (en) *	1990-06-18	1993-03-30	Sri International	Method of forming dinitramide salts
US5254324A (en) *	1990-06-18	1993-10-19	Sri International	Dinitramide salts and method of making same
US5316749A (en) *	1991-07-30	1994-05-31	Sri International	Process for forming ammonium dinitramide salt by reaction between ammonia and a nitronium-containing compound
US5415852A (en) *	1992-01-29	1995-05-16	Sri International	Process for forming a dinitramide salt or acid by reaction of a salt or free acid of an N(alkoxycarbonyl)N-nitroamide with a nitronium-containing compound followed by reaction of the intermediate product respectively with a base or alcohol

1995
- 1995-09-26 SE SE9503326A patent/SE516719C2/sv not_active IP Right Cessation
1996
- 1996-07-26 TR TR1998/00129T patent/TR199800129T1/xx unknown
- 1996-07-26 WO PCT/SE1996/000976 patent/WO1997006099A1/en not_active Ceased
- 1996-07-26 JP JP50836697A patent/JP4118947B2/ja not_active Expired - Fee Related
- 1996-07-26 AU AU65396/96A patent/AU703767B2/en not_active Ceased
- 1996-07-26 US US08/983,462 patent/US5976483A/en not_active Expired - Lifetime
- 1996-07-26 ES ES96925240T patent/ES2159039T3/es not_active Expired - Lifetime
- 1996-07-26 CA CA002227625A patent/CA2227625C/en not_active Expired - Fee Related
- 1996-07-26 IL IL12288096A patent/IL122880A/xx not_active IP Right Cessation
- 1996-07-26 DE DE69612497T patent/DE69612497T2/de not_active Expired - Lifetime
- 1996-07-26 EP EP96925240A patent/EP0843647B1/de not_active Expired - Lifetime
- 1996-07-26 AT AT96925240T patent/ATE200470T1/de not_active IP Right Cessation
- 1996-07-26 BR BR9609993A patent/BR9609993A/pt not_active Application Discontinuation
1998
- 1998-02-06 NO NO19980534A patent/NO321198B1/no not_active IP Right Cessation

Also Published As

Publication number	Publication date
TR199800129T1 (xx)	1998-04-21
NO980534D0 (no)	1998-02-06
NO980534L (no)	1998-02-06
US5976483A (en)	1999-11-02
SE9503326D0 (sv)	1995-09-26
AU703767B2 (en)	1999-04-01
EP0843647B1 (de)	2001-04-11
JPH11514323A (ja)	1999-12-07
ATE200470T1 (de)	2001-04-15
SE516719C2 (sv)	2002-02-19
CA2227625A1 (en)	1997-02-20
ES2159039T3 (es)	2001-09-16
DE69612497T2 (de)	2001-10-18
NO321198B1 (no)	2006-04-03
CA2227625C (en)	2008-06-03
BR9609993A (pt)	1999-07-06
JP4118947B2 (ja)	2008-07-16
AU6539696A (en)	1997-03-05
DE69612497D1 (de)	2001-05-17
IL122880A0 (en)	1998-08-16
WO1997006099A1 (en)	1997-02-20
SE9503326L (sv)	1997-02-09
EP0843647A1 (de)	1998-05-27

Legal Events

Date	Code	Title
2001-03-19	FF	Patent granted
2001-06-14	KB	Patent renewed
2002-09-12	KB	Patent renewed
2006-09-05	KB	Patent renewed
2010-11-30	KB	Patent renewed
2014-08-31	KB	Patent renewed
2017-02-28	EXP	Patent expired

Publication	Publication Date	Title
IL122880A0 (en)	1998-08-16	Method of preparing dinitramidic acid and salts thereof
US5032291A (en)	1991-07-16	Catalytic reduction of nitro- and nitroso- substituted compounds
ES2127381T3 (es)	1999-04-16	Nuevo procedimiento para la nitracion de compuestos aromaticos en condiciones suaves, no corrosivas.
Zolfigol et al.	2000	An Efficient Method for N-Nitrosation of Secondary Amines Under Mild and Heterogeneous Conditions
PL118036B1 (en)	1981-09-30	Method of reduction of nitrosating agents concentration in 1-chloro-2,6-dinitro-4-/trifluoromethyl/benzene v 1-khloro-2,6-dinitro-4/triftorometilo/benzole
Omietanski et al.	1956	Reactions of Chloramine with Anhydrous Primary and Secondary Amines
US20050038297A1 (en)	2005-02-17	Synthesis and purification of 1,3,5-triamino-2,4,6-trinitrobenzene (TATB)
PL119759B1 (en)	1982-01-30	Method of removal of nitrosoamines from dinitroanilines
KR890001947A (ko)	1989-04-06	2,2-비스-(3- 아미노페닐)헥사플루오로프로판의 유도체 및 2.2-비스-(3.4-디아미노페닐)헥사플루오로프로판의 제조방법
CA2552765C (en)	2012-11-27	Method of producing salts of dinitramidic acid
US20110160450A1 (en)	2011-06-30	Explosive
JPS58124594A (ja)	1983-07-25	残留水中の芳香族第一アミンの分解方法
RU92009774A (ru)	1996-12-20	Способ получения производных 2-р-4(5'')-нитроимидазолов
Matsuya et al.	1997	A mild dehydrazination reaction of arylhydrazines using nitric oxide in the presence of oxygen
US5998676A (en)	1999-12-07	Conversion of picrate to picric acid in a liquid-liquid two phase system
KR860001107A (ko)	1986-02-22	6-또는 11-치환 아포빈카민산 유도체의 제조방법
CN116059693A (zh)	2023-05-05	一种二硝酰胺铵水溶液的合成方法
KR800000975B1 (ko)	1980-09-17	3, 3'-트리아릴메탄-디카복실산 유도체의 제법
Hall et al.	1951	The Chemistry of Linear Substituted Nitroguanidines
JPS5490180A (en)	1979-07-17	Purification and recovery of n,n'-disubstituted bipyridium
Stern et al.	1998	Process for preparing ammonium dinitramide
ES2074952A1 (es)	1995-09-16	Composicion explosiva de tipo hidrogel y su procedimiento de fabricacion.
RU1825357C (ru)	1993-06-30	Способ получени нитромезитилена
Al-Kaabi et al.	1984	Unusual rate-limiting proton transfer in the acid-catalysed reactions of N-nitroso compounds
Ward et al.	1961	956. Nitration of the N-acyl-nitronaphthylamines