ATE221893T1 - Verfahren zur herstellung von acylphosphinen und derivaten - Google Patents

Verfahren zur herstellung von acylphosphinen und derivaten

Info

Publication number: ATE221893T1
Authority: AT; Austria
Prior art keywords: mono; preparation; acylphosphines; derivatives; producing
Prior art date: 1998-11-30

Application number

AT99973034T

Other languages

English (en)

Inventor

David George Leppard

Eugen Eichenberger

Rene Kaeser

Gebhard Hug

Urs Schwendimann

Original Assignee

Ciba Sc Holding Ag

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1998-11-30

Filing date

1999-11-20

Publication date

2002-08-15

Family has litigation

First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=25690294&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=ATE221893(T1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.

1999-11-20 Application filed by Ciba Sc Holding Ag filed Critical Ciba Sc Holding Ag

2002-08-15 Application granted granted Critical

2002-08-15 Publication of ATE221893T1 publication Critical patent/ATE221893T1/de

Links

238000004519 manufacturing process Methods 0.000 title 1
238000000034 method Methods 0.000 abstract 3
238000002360 preparation method Methods 0.000 abstract 3
150000003568 thioethers Chemical class 0.000 abstract 2
WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 abstract 1
FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 abstract 1
NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 abstract 1
239000002253 acid Substances 0.000 abstract 1
229910052783 alkali metal Inorganic materials 0.000 abstract 1
150000001340 alkali metals Chemical class 0.000 abstract 1
239000003054 catalyst Substances 0.000 abstract 1
238000006243 chemical reaction Methods 0.000 abstract 1
150000004820 halides Chemical class 0.000 abstract 1
239000000543 intermediate Substances 0.000 abstract 1
238000002955 isolation Methods 0.000 abstract 1
229910052744 lithium Inorganic materials 0.000 abstract 1
229910052749 magnesium Inorganic materials 0.000 abstract 1
239000011777 magnesium Substances 0.000 abstract 1
239000000203 mixture Substances 0.000 abstract 1
230000003647 oxidation Effects 0.000 abstract 1
238000007254 oxidation reaction Methods 0.000 abstract 1
150000003003 phosphines Chemical class 0.000 abstract 1
239000011593 sulfur Substances 0.000 abstract 1
229910052717 sulfur Inorganic materials 0.000 abstract 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/50—Organo-phosphines
- C07F9/53—Organo-phosphine oxides; Organo-phosphine thioxides
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/50—Organo-phosphines
- C07F9/5036—Phosphines containing the structure -C(=X)-P or NC-P
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/50—Organo-phosphines
- C07F9/53—Organo-phosphine oxides; Organo-phosphine thioxides
- C07F9/5337—Phosphine oxides or thioxides containing the structure -C(=X)-P(=X) or NC-P(=X) (X = O, S, Se)

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Health & Medical Sciences (AREA)
Life Sciences & Earth Sciences (AREA)
Biochemistry (AREA)
General Health & Medical Sciences (AREA)
Molecular Biology (AREA)
Crystallography & Structural Chemistry (AREA)
Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Saccharide Compounds (AREA)

AT99973034T 1998-11-30 1999-11-20 Verfahren zur herstellung von acylphosphinen und derivaten ATE221893T1 (de)

Applications Claiming Priority (3)

Application Number	Priority Date	Filing Date	Title
CH237698		1998-11-30
CH243498		1998-12-08
PCT/EP1999/008968 WO2000032612A1 (en)	1998-11-30	1999-11-20	Process for preparing acylphosphines and derivatives

Publications (1)

Publication Number	Publication Date
ATE221893T1 true ATE221893T1 (de)	2002-08-15

Family

ID=25690294

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
AT99973034T ATE221893T1 (de)	1998-11-30	1999-11-20	Verfahren zur herstellung von acylphosphinen und derivaten

Country Status (14)

Country	Link
US (3)	US6888031B1 (de)
EP (1)	EP1135399B2 (de)
JP (1)	JP4265871B2 (de)
KR (1)	KR100653117B1 (de)
CN (1)	CN1211388C (de)
AT (1)	ATE221893T1 (de)
AU (1)	AU760237B2 (de)
CA (1)	CA2349637C (de)
CZ (1)	CZ302512B6 (de)
DE (1)	DE69902485T3 (de)
ES (1)	ES2180347T5 (de)
SK (1)	SK286152B6 (de)
TW (1)	TW492972B (de)
WO (1)	WO2000032612A1 (de)

Families Citing this family (38)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US6888031B1 (en) *	1998-11-30	2005-05-03	Ciba Specialty Chemicals Corporation	Process for the preparation of acylphosphines, acyl oxides and acyl sulfides
GB2360283B (en)	2000-02-08	2002-08-21	Ciba Sc Holding Ag	Monoacylarylphosphines and acylphosphine oxides and sulphides
GB2365430B (en)	2000-06-08	2002-08-28	Ciba Sc Holding Ag	Acylphosphine photoinitiators and intermediates
CN100437354C (zh) *	2001-08-21	2008-11-26	西巴特殊化学品控股有限公司	红移单-和双-酰基氧化膦和硫化膦及其作为光引发剂的应用
DE10206117A1 (de)	2002-02-13	2003-08-14	Basf Ag	Acyl- und Bisacylphosphinderivate
DE10244684A1 (de)	2002-09-24	2004-04-01	Basf Ag	Verfahren zur Herstellung von Acylphosphinoxiden
ATE435230T1 (de) *	2002-12-04	2009-07-15	Ciba Holding Inc	Verfahren zur synthese von cycloorganylphosphanen und von di(alkali/erdalkalimetall)oligophosphandiiden
DE10315671A1 (de) *	2003-04-04	2004-10-14	Basf Ag	Verfahren zur Herstellung von Acylphosphinoxid-Feststoffen
PL1648908T3 (pl) *	2003-07-18	2007-01-31	Igm Malta Ltd	Sposób wytwarzania acylofosfanów i ich pochodnych
TW200523265A (en) *	2003-07-31	2005-07-16	Basf Ag	A process for the preparation of acylphosphines
CN101065388B (zh) *	2004-11-23	2011-12-21	西巴特殊化学品控股有限公司	制备酰基磷烷及其衍生物的方法
EP1838721B1 (de) *	2005-01-17	2011-12-21	Basf Se	Verfahren zur herstellung von acylphosphan und deren oxide und sulfide
DE102005005946A1 (de) *	2005-02-10	2006-08-17	Basf Ag	Verfahren zur Herstellung tertiärer Phosphine
JP5623416B2 (ja)	2008-11-03	2014-11-12	ビーエーエスエフソシエタス・ヨーロピアＢａｓｆＳｅ	光開始剤混合物
EP2421903B1 (de) *	2009-04-20	2014-11-19	ETH Zurich	Polymernanopartikel
CN102875598B (zh) *	2011-07-11	2016-09-07	深圳市有为化学技术有限公司	(二苯膦氧基)(均三甲苯基)甲酮和(苯膦氧基)双(均三甲苯基甲酮)的制备方法
CN102875597B (zh) *	2011-07-11	2017-05-03	深圳市有为化学技术有限公司	芳香酮膦氧杂化型化合物
CN102675365A (zh) *	2012-05-16	2012-09-19	湖北固润科技股份有限公司	一种紫外光引发剂xbpo合成方法
GB201213163D0 (en)	2012-07-24	2012-09-05	Lambson Ltd	Photopolymerisation processes and novel compounds therefor
ES2720760T3 (es)	2012-10-01	2019-07-24	Eth Zuerich	Un procedimiento para la preparación de acilofosfanos
US8934023B2 (en)	2013-03-15	2015-01-13	Freefly Systems, Inc.	Method and system for introducing controlled disturbance into an actively stabilized system
CN104592298B (zh) *	2014-12-31	2016-07-06	湖北固润科技股份有限公司	一种酰基膦高效光引发剂及其制备方法
CN105541913B (zh) *	2015-12-03	2017-08-25	天津久日新材料股份有限公司	一种2,4,6‑三甲基苯甲酰基二苯基氧化膦的制备方法
CN105732710A (zh) *	2016-03-16	2016-07-06	三峡大学	一种光引发剂联苯基四(2,4,6-三甲基苯甲酰基)氧化膦的制备方法及其应用
CN105732709A (zh) *	2016-03-16	2016-07-06	三峡大学	一种光引发剂2,4,6-三甲基苯甲酰二环己基氧膦，制备方法及其应用
CN107304220B (zh) *	2016-04-22	2020-03-31	江苏英力科技发展有限公司	一种“一锅法”合成2,4,6-三甲基苯甲酰基-二苯基氧化膦的方法
EP3296301A1 (de)	2016-09-19	2018-03-21	ETH Zürich	Vielseitiges verfahren zur herstellung von acylphosphinen
JP6916484B2 (ja) *	2017-03-28	2021-08-11	国立大学法人千葉大学	アシルホスフィンの製造方法
EP3409680B1 (de)	2017-05-30	2021-01-06	IGM Group B.V.	Synthese von bis(acyl)phosphinen durch aktivierung von nicht-reaktiven metallphosphiden
EP3539924A1 (de) *	2018-03-14	2019-09-18	ETH Zurich	Neuartige vinylphosphine und daraus erhältliche photoinitiatoren
CN110734461A (zh) *	2018-07-20	2020-01-31	深圳市有为化学技术有限公司	化合物2,4,6-三甲基苯甲酰基二苯基氧化膦的制备
JP7432616B2 (ja) *	2018-12-07	2024-02-16	アンチンライティングオプトエレクトロニクステクノロジーカンパニーリミテッド	アシルホスフィンオキシド化合物及びその調製方法
CN111138491B (zh) *	2019-12-31	2022-08-05	天津久日新材料股份有限公司	一种制备光引发剂tpo同时副产氯苄的方法
CN111087425B (zh)	2020-01-10	2022-04-19	天津大学	一种大粒度苯基双(2,4,6-三甲基苯甲酰基)氧化膦晶型及其结晶方法
CN112279940B (zh) *	2020-04-17	2023-06-27	山东科技大学	一种酰基膦光引发剂及其制备方法
CN112159429B (zh) *	2020-10-29	2022-06-21	天津久日新材料股份有限公司	一种双(2,4,6-三甲基苯甲酰基)苯基氧化膦的制备方法
IT202300028218A1 (it)	2023-12-28	2025-06-28	Igm Resins Italia Srl	Nuova forma solida di bis(2,4,6-trimetilbenzoil)-n-ottilfosfina ossido
JP7600464B1 (ja) *	2024-10-03	2024-12-16	サカタインクス株式会社	活性エネルギー線硬化型インクジェット印刷用インク

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE2962089D1 (en)	1978-07-14	1982-03-18	Basf Ag	Light-curable moulding, impregnating and coating compositions and shaped articles prepared therefrom
DE2909994A1 (de)	1979-03-14	1980-10-02	Basf Ag	Acylphosphinoxidverbindungen, ihre herstellung und verwendung
DE3020092A1 (de) *	1980-05-27	1981-12-10	Basf Ag, 6700 Ludwigshafen	Acylphosphinverbindungen und ihre verwendung
DE3034697A1 (de)	1980-09-15	1982-05-06	Basf Ag, 6700 Ludwigshafen	Acylphosphinsulfidverbindungen, ihre herstellung und verwendung
DE3443221A1 (de)	1984-11-27	1986-06-05	ESPE Fabrik pharmazeutischer Präparate GmbH, 8031 Seefeld	Bisacylphosphinoxide, ihre herstellung und verwendung
US5218009A (en) *	1989-08-04	1993-06-08	Ciba-Geigy Corporation	Mono- and di-acylphosphine oxides
RU2091385C1 (ru)	1991-09-23	1997-09-27	Циба-Гейги АГ	Бисацилфосфиноксиды, состав и способ нанесения покрытий
ZA941879B (en)	1993-03-18	1994-09-19	Ciba Geigy	Curing compositions containing bisacylphosphine oxide photoinitiators
TW381106B (en) *	1994-09-02	2000-02-01	Ciba Sc Holding Ag	Alkoxyphenyl-substituted bisacylphosphine oxides
EP0779891B1 (de) *	1994-09-08	1998-12-23	Ciba SC Holding AG	Neue acylphosphinoxide
TW323274B (de) *	1994-10-13	1997-12-21	Ciba Sc Holding Ag
US6888031B1 (en) *	1998-11-30	2005-05-03	Ciba Specialty Chemicals Corporation	Process for the preparation of acylphosphines, acyl oxides and acyl sulfides
GB2360283B (en) *	2000-02-08	2002-08-21	Ciba Sc Holding Ag	Monoacylarylphosphines and acylphosphine oxides and sulphides

1999
- 1999-11-20 US US09/856,769 patent/US6888031B1/en not_active Expired - Lifetime
- 1999-11-20 WO PCT/EP1999/008968 patent/WO2000032612A1/en not_active Ceased
- 1999-11-20 CZ CZ20011875A patent/CZ302512B6/cs not_active IP Right Cessation
- 1999-11-20 KR KR1020017006727A patent/KR100653117B1/ko not_active Expired - Lifetime
- 1999-11-20 SK SK727-2001A patent/SK286152B6/sk not_active IP Right Cessation
- 1999-11-20 CN CNB998137138A patent/CN1211388C/zh not_active Expired - Lifetime
- 1999-11-20 CA CA002349637A patent/CA2349637C/en not_active Expired - Lifetime
- 1999-11-20 DE DE69902485T patent/DE69902485T3/de not_active Expired - Lifetime
- 1999-11-20 JP JP2000585253A patent/JP4265871B2/ja not_active Expired - Lifetime
- 1999-11-20 AU AU13845/00A patent/AU760237B2/en not_active Expired
- 1999-11-20 ES ES99973034T patent/ES2180347T5/es not_active Expired - Lifetime
- 1999-11-20 EP EP99973034A patent/EP1135399B2/de not_active Expired - Lifetime
- 1999-11-20 AT AT99973034T patent/ATE221893T1/de active
- 1999-11-29 TW TW088120769A patent/TW492972B/zh not_active IP Right Cessation
2004
- 2004-05-17 US US10/847,095 patent/US7094931B2/en not_active Expired - Lifetime
2006
- 2006-02-06 US US11/348,042 patent/US7214830B2/en not_active Expired - Lifetime

Also Published As

Publication number	Publication date
ES2180347T3 (es)	2003-02-01
JP4265871B2 (ja)	2009-05-20
SK286152B6 (sk)	2008-04-07
JP2002531460A (ja)	2002-09-24
DE69902485D1 (de)	2002-09-12
WO2000032612A1 (en)	2000-06-08
DE69902485T3 (de)	2007-03-15
US6888031B1 (en)	2005-05-03
CN1211388C (zh)	2005-07-20
CA2349637A1 (en)	2000-06-08
US7214830B2 (en)	2007-05-08
SK7272001A3 (en)	2001-12-03
CN1328564A (zh)	2001-12-26
EP1135399B2 (de)	2006-08-09
TW492972B (en)	2002-07-01
US20040248855A1 (en)	2004-12-09
EP1135399A1 (de)	2001-09-26
AU760237B2 (en)	2003-05-08
US7094931B2 (en)	2006-08-22
EP1135399B1 (de)	2002-08-07
KR100653117B1 (ko)	2006-12-21
US20060128959A1 (en)	2006-06-15
KR20010093124A (ko)	2001-10-27
AU1384500A (en)	2000-06-19
DE69902485T2 (de)	2003-05-08
CZ302512B6 (cs)	2011-06-29
CZ20011875A3 (cs)	2001-09-12
ES2180347T5 (es)	2007-04-01
CA2349637C (en)	2008-12-23

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2003-02-15

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