ATE410464T1 - Verzweigte polymere aus organohydrogensilizium- verbindungen - Google Patents
Verzweigte polymere aus organohydrogensilizium- verbindungenInfo
- Publication number
- ATE410464T1 ATE410464T1 AT03790532T AT03790532T ATE410464T1 AT E410464 T1 ATE410464 T1 AT E410464T1 AT 03790532 T AT03790532 T AT 03790532T AT 03790532 T AT03790532 T AT 03790532T AT E410464 T1 ATE410464 T1 AT E410464T1
- Authority
- AT
- Austria
- Prior art keywords
- branched polymers
- bonded hydrogen
- silicon
- silicon compounds
- iii
- Prior art date
Links
- 229920000642 polymer Polymers 0.000 title abstract 2
- 150000003377 silicon compounds Chemical class 0.000 title 1
- 150000001875 compounds Chemical class 0.000 abstract 3
- 239000003054 catalyst Substances 0.000 abstract 2
- 125000004435 hydrogen atom Chemical group [H]* 0.000 abstract 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 1
- 125000001931 aliphatic group Chemical group 0.000 abstract 1
- 239000007795 chemical reaction product Substances 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 229910052751 metal Inorganic materials 0.000 abstract 1
- 239000002184 metal Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 125000005375 organosiloxane group Chemical group 0.000 abstract 1
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical group [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 abstract 1
- 238000006116 polymerization reaction Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/12—Polysiloxanes containing silicon bound to hydrogen
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/21—Cyclic compounds having at least one ring containing silicon, but no carbon in the ring
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/42—Block-or graft-polymers containing polysiloxane sequences
- C08G77/44—Block-or graft-polymers containing polysiloxane sequences containing only polysiloxane sequences
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/48—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule in which at least two but not all the silicon atoms are connected by linkages other than oxygen atoms
- C08G77/50—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule in which at least two but not all the silicon atoms are connected by linkages other than oxygen atoms by carbon linkages
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L83/00—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon only; Compositions of derivatives of such polymers
- C08L83/04—Polysiloxanes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L83/00—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon only; Compositions of derivatives of such polymers
- C08L83/04—Polysiloxanes
- C08L83/06—Polysiloxanes containing silicon bound to oxygen-containing groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/045—Polysiloxanes containing less than 25 silicon atoms
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/14—Polysiloxanes containing silicon bound to oxygen-containing groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/14—Polysiloxanes containing silicon bound to oxygen-containing groups
- C08G77/16—Polysiloxanes containing silicon bound to oxygen-containing groups to hydroxyl groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/14—Polysiloxanes containing silicon bound to oxygen-containing groups
- C08G77/18—Polysiloxanes containing silicon bound to oxygen-containing groups to alkoxy or aryloxy groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/20—Polysiloxanes containing silicon bound to unsaturated aliphatic groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/22—Polysiloxanes containing silicon bound to organic groups containing atoms other than carbon, hydrogen and oxygen
- C08G77/24—Polysiloxanes containing silicon bound to organic groups containing atoms other than carbon, hydrogen and oxygen halogen-containing groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/42—Block-or graft-polymers containing polysiloxane sequences
- C08G77/46—Block-or graft-polymers containing polysiloxane sequences containing polyether sequences
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/70—Siloxanes defined by use of the MDTQ nomenclature
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Silicon Polymers (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US43590202P | 2002-12-20 | 2002-12-20 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE410464T1 true ATE410464T1 (de) | 2008-10-15 |
Family
ID=32682292
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT03790532T ATE410464T1 (de) | 2002-12-20 | 2003-12-17 | Verzweigte polymere aus organohydrogensilizium- verbindungen |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US7432338B2 (de) |
| EP (1) | EP1576034B1 (de) |
| JP (1) | JP4925026B2 (de) |
| KR (1) | KR101028347B1 (de) |
| CN (1) | CN1322031C (de) |
| AT (1) | ATE410464T1 (de) |
| AU (1) | AU2003293583A1 (de) |
| DE (1) | DE60324023D1 (de) |
| ES (1) | ES2314273T3 (de) |
| WO (1) | WO2004058858A1 (de) |
Families Citing this family (47)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ATE363518T1 (de) * | 2002-05-01 | 2007-06-15 | Dow Corning | Zusammensetzungen mit verlängerter verarbeitungszeit |
| WO2004058857A2 (en) * | 2002-12-20 | 2004-07-15 | Dow Corning Corporation | Branched polymers from organohydrogensilicon compounds |
| CN100374525C (zh) * | 2003-03-17 | 2008-03-12 | 陶氏康宁公司 | 具有改进的高温粘结强度的无溶剂硅氧烷压敏粘合剂 |
| GB0316162D0 (en) * | 2003-07-10 | 2003-08-13 | Dow Corning | Silicone release coating compositions |
| US20060134440A1 (en) * | 2004-10-27 | 2006-06-22 | Crivello James V | Silicone encapsulants for light emitting diodes |
| KR101351815B1 (ko) * | 2005-07-28 | 2014-01-15 | 다우 코닝 코포레이션 | 향상된 박리력 프로파일을 갖는 박리 피막 조성물 |
| US20080051525A1 (en) * | 2006-06-28 | 2008-02-28 | Soucek Mark D | Process for preparing substituted polysiloxane coatings |
| CN101657490B (zh) * | 2007-04-17 | 2012-07-04 | 旭化成化学株式会社 | 环氧硅酮及其制造方法、以及使用该环氧硅酮的固化性树脂组合物及其用途 |
| JP5248032B2 (ja) * | 2007-04-23 | 2013-07-31 | 株式会社Ａｄｅｋａ | ケイ素含有化合物、硬化性組成物及び硬化物 |
| JP5248034B2 (ja) * | 2007-04-23 | 2013-07-31 | 株式会社Ａｄｅｋａ | ケイ素含有化合物、硬化性組成物及び硬化物 |
| JP5248033B2 (ja) * | 2007-04-23 | 2013-07-31 | 株式会社Ａｄｅｋａ | ケイ素含有化合物、硬化性組成物及び硬化物 |
| DE102008000353A1 (de) * | 2008-02-20 | 2009-08-27 | Wacker Chemie Ag | Härtbare Polymerabmischungen |
| US20120220549A1 (en) * | 2009-09-03 | 2012-08-30 | Michael Stephen Starch | Pituitous Silicone Fluids |
| CN102482495B (zh) | 2009-09-03 | 2014-09-10 | 道康宁公司 | 具有粘液质硅酮液的个人护理组合物 |
| US9593209B2 (en) | 2009-10-22 | 2017-03-14 | Dow Corning Corporation | Process for preparing clustered functional polyorganosiloxanes, and methods for their use |
| TWI502004B (zh) * | 2009-11-09 | 2015-10-01 | Dow Corning | 群集官能性聚有機矽氧烷之製法及其使用方法 |
| EP2692776B1 (de) * | 2011-03-30 | 2017-02-22 | Asahi Kasei Kabushiki Kaisha | Organopolysiloxan, herstellungsverfahren dafür und härtbare zusammensetzung mit dem organopolysiloxan |
| WO2012165228A1 (ja) | 2011-05-30 | 2012-12-06 | 東レ・ダウコーニング株式会社 | 新規オルガノポリシロキサンエラストマー及びその利用 |
| JP6369888B2 (ja) | 2011-12-27 | 2018-08-08 | 東レ・ダウコーニング株式会社 | 新規液状オルガノポリシロキサン及びその利用 |
| TWI480316B (zh) * | 2012-07-13 | 2015-04-11 | Daxin Materials Corp | 含烯基或矽氫鍵的星狀聚矽氧烷以及熱硬化樹脂組成物 |
| WO2014059132A2 (en) | 2012-10-12 | 2014-04-17 | Dow Corning Corporation | Membranes including polysiloxane-poly(alkylene oxide) copolymers and methods of using the same |
| WO2014124367A1 (en) | 2013-02-11 | 2014-08-14 | Dow Corning Corporation | Method for forming thermally conductive thermal radical cure silicone compositions |
| KR102186328B1 (ko) | 2013-02-11 | 2020-12-03 | 다우 실리콘즈 코포레이션 | 알콕시-작용성 유기폴리실록산 수지 및 중합체와 이의 관련된 형성 방법 |
| WO2014124382A1 (en) * | 2013-02-11 | 2014-08-14 | Dow Corning Corporation | In situ method for forming thermally conductive thermal radical cure silicone composition |
| CN104968749B (zh) | 2013-02-11 | 2017-03-29 | 道康宁公司 | 稳定性热自由基可固化有机硅粘合剂组合物 |
| EP2954024B1 (de) * | 2013-02-11 | 2019-05-15 | Dow Silicones Corporation | Härtbare silikonzusammensetzungen mit geclusterten funktionalisierten polyorganosiloxanen und silikonreaktiven verdünnern |
| US9944758B2 (en) | 2013-02-11 | 2018-04-17 | Dow Corning Corporation | Clustered functional polyorganosiloxanes, processes for forming same and methods for their use |
| JP6426629B2 (ja) | 2013-02-11 | 2018-11-21 | ダウ シリコーンズ コーポレーション | アルコキシ官能性シロキサン反応性樹脂を含む湿気硬化性ホットメルトシリコーン接着剤組成物 |
| US9530946B2 (en) * | 2013-04-12 | 2016-12-27 | Milliken & Company | Light emitting diode |
| US10940099B2 (en) | 2015-04-08 | 2021-03-09 | Dow Silicones Corporation | Pituitous silicone emulsions |
| EP3196229B1 (de) | 2015-11-05 | 2018-09-26 | Dow Silicones Corporation | Verzweigte polyorganosiloxane und zugehörige härtbare zusammensetzungen, verfahren, verwendungen und vorrichtungen |
| CN108291030B (zh) * | 2015-12-07 | 2021-01-05 | 美国陶氏有机硅公司 | 使用铱络合物催化剂氢化硅烷化羧酸烷基酯和氢封端的有机硅氧烷寡聚物的方法和组合物 |
| CN111417672A (zh) * | 2017-09-26 | 2020-07-14 | 美国圣戈班性能塑料公司 | 可光致固化组合物及将其用于进行3d打印的方法 |
| CN107722959B (zh) * | 2017-09-28 | 2020-07-21 | 河南大学 | 一种胍胶压裂液有机钛交联剂及其制备方法 |
| CN111032604B (zh) | 2017-10-19 | 2020-10-30 | 美国陶氏有机硅公司 | 含有可用作氢化硅烷化反应抑制剂的2-取代的-1-炔基-1-环己醇的聚有机硅氧烷组合物 |
| US10743608B2 (en) | 2017-12-28 | 2020-08-18 | Under Armour, Inc. | Fiber reinforced plate for articles of footwear and methods of making |
| JP6948501B2 (ja) * | 2018-04-17 | 2021-10-13 | ジェレスト， インコーポレイテッド | ヒドリドシロキサニル置換シクロトリシロキサン、その製造方法、及びそれから誘導されるポリマー製品 |
| US11643506B2 (en) | 2018-12-21 | 2023-05-09 | Dow Silicones Corporation | Polyfunctional organosiloxanes, compositions containing same, and methods for the preparation thereof |
| JP7463373B2 (ja) | 2018-12-21 | 2024-04-08 | ダウ シリコーンズ コーポレーション | 官能化ポリオルガノシロキサンの調製方法 |
| EP4212575B1 (de) | 2018-12-21 | 2024-05-29 | Dow Silicones Corporation | Verfahren zur herstellung polyfunktioneller organosiloxane und zusammensetzungen damit |
| EP3898776B1 (de) | 2018-12-21 | 2023-03-01 | Dow Silicones Corporation | Polyfunktionale organosiloxane, zusammensetzungen damit und verfahren zur herstellung davon |
| KR20210114430A (ko) * | 2018-12-31 | 2021-09-23 | 다우 실리콘즈 코포레이션 | 분지형 유기규소 화합물, 그의 제조 방법, 및 그로 형성된 공중합체 |
| US11976172B2 (en) | 2019-04-16 | 2024-05-07 | Saint-Gobain Performance Plastics Corporation | Dual cure compositions |
| CN113795539B (zh) | 2019-05-16 | 2023-08-04 | 美国陶氏有机硅公司 | 聚硅氧烷受控剥离添加剂、其制备方法及剥离涂料组合物 |
| WO2021113317A1 (en) * | 2019-12-02 | 2021-06-10 | Dow Silicones Corporation | Composition for preparing a release coating |
| CN113785026B (zh) | 2019-12-02 | 2022-12-09 | 美国陶氏有机硅公司 | 用于制备防粘涂料的组合物 |
| CN112266480A (zh) * | 2020-11-03 | 2021-01-26 | 湖北双键精细化工有限公司 | 一种高收率的支链硅油合成工艺 |
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-
2003
- 2003-12-17 EP EP03790532A patent/EP1576034B1/de not_active Expired - Lifetime
- 2003-12-17 AU AU2003293583A patent/AU2003293583A1/en not_active Abandoned
- 2003-12-17 DE DE60324023T patent/DE60324023D1/de not_active Expired - Lifetime
- 2003-12-17 KR KR1020057011468A patent/KR101028347B1/ko not_active Expired - Fee Related
- 2003-12-17 AT AT03790532T patent/ATE410464T1/de not_active IP Right Cessation
- 2003-12-17 CN CNB2003801068783A patent/CN1322031C/zh not_active Expired - Fee Related
- 2003-12-17 WO PCT/US2003/040262 patent/WO2004058858A1/en not_active Ceased
- 2003-12-17 JP JP2004563699A patent/JP4925026B2/ja not_active Expired - Fee Related
- 2003-12-17 ES ES03790532T patent/ES2314273T3/es not_active Expired - Lifetime
- 2003-12-17 US US10/538,680 patent/US7432338B2/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| AU2003293583A1 (en) | 2004-07-22 |
| CN1729231A (zh) | 2006-02-01 |
| KR20050085810A (ko) | 2005-08-29 |
| US20060116500A1 (en) | 2006-06-01 |
| ES2314273T3 (es) | 2009-03-16 |
| JP2006511645A (ja) | 2006-04-06 |
| DE60324023D1 (de) | 2008-11-20 |
| EP1576034A1 (de) | 2005-09-21 |
| EP1576034B1 (de) | 2008-10-08 |
| JP4925026B2 (ja) | 2012-04-25 |
| KR101028347B1 (ko) | 2011-04-11 |
| WO2004058858A1 (en) | 2004-07-15 |
| US7432338B2 (en) | 2008-10-07 |
| CN1322031C (zh) | 2007-06-20 |
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| Date | Code | Title | Description |
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| RER | Ceased as to paragraph 5 lit. 3 law introducing patent treaties |