ATE448239T1 - Destillatives verfahren zur gewinnung und auftrennung von phytosterolen und phytostanolen aus tallölpech - Google Patents
Destillatives verfahren zur gewinnung und auftrennung von phytosterolen und phytostanolen aus tallölpechInfo
- Publication number
- ATE448239T1 ATE448239T1 AT03701377T AT03701377T ATE448239T1 AT E448239 T1 ATE448239 T1 AT E448239T1 AT 03701377 T AT03701377 T AT 03701377T AT 03701377 T AT03701377 T AT 03701377T AT E448239 T1 ATE448239 T1 AT E448239T1
- Authority
- AT
- Austria
- Prior art keywords
- pitch
- phytostanols
- phytosterols
- distilling
- distillation column
- Prior art date
Links
- 229940068065 phytosterols Drugs 0.000 title abstract 7
- 238000004821 distillation Methods 0.000 title abstract 4
- 238000000605 extraction Methods 0.000 title 1
- 238000000926 separation method Methods 0.000 title 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 3
- 239000002253 acid Substances 0.000 abstract 2
- 239000002002 slurry Substances 0.000 abstract 2
- 239000000243 solution Substances 0.000 abstract 2
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 abstract 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 1
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 abstract 1
- 150000007513 acids Chemical class 0.000 abstract 1
- 229910052783 alkali metal Inorganic materials 0.000 abstract 1
- 150000001340 alkali metals Chemical class 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 239000002585 base Substances 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- 235000014113 dietary fatty acids Nutrition 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 229930195729 fatty acid Natural products 0.000 abstract 1
- 239000000194 fatty acid Substances 0.000 abstract 1
- 150000004665 fatty acids Chemical class 0.000 abstract 1
- 239000000706 filtrate Substances 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 230000003472 neutralizing effect Effects 0.000 abstract 1
- 238000005191 phase separation Methods 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
- 239000003784 tall oil Substances 0.000 abstract 1
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 abstract 1
- 238000005406 washing Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07J—STEROIDS
- C07J9/00—Normal steroids containing carbon, hydrogen, halogen or oxygen substituted in position 17 beta by a chain of more than two carbon atoms, e.g. cholane, cholestane, coprostane
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/001—Refining fats or fatty oils by a combination of two or more of the means hereafter
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/02—Refining fats or fatty oils by chemical reaction
- C11B3/06—Refining fats or fatty oils by chemical reaction with bases
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/12—Refining fats or fatty oils by distillation
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Microbiology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Steroid Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US10/060,022 US20030144536A1 (en) | 2002-01-28 | 2002-01-28 | Process of extracting and purifying phytosterols and phytostanols from tall oil pitch |
| PCT/CA2003/000098 WO2003064442A2 (en) | 2002-01-28 | 2003-01-27 | Distalliative process of extracting and purifying phytosterols and phytostanols from tall oil pitch |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE448239T1 true ATE448239T1 (de) | 2009-11-15 |
Family
ID=27609947
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT03701377T ATE448239T1 (de) | 2002-01-28 | 2003-01-27 | Destillatives verfahren zur gewinnung und auftrennung von phytosterolen und phytostanolen aus tallölpech |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US20030144536A1 (de) |
| EP (1) | EP1470149B1 (de) |
| JP (1) | JP2005516069A (de) |
| CN (1) | CN1639184A (de) |
| AT (1) | ATE448239T1 (de) |
| AU (1) | AU2003203072B2 (de) |
| BR (1) | BR0307270A (de) |
| CA (1) | CA2474592A1 (de) |
| DE (1) | DE60329977D1 (de) |
| ES (1) | ES2335754T3 (de) |
| NZ (1) | NZ534369A (de) |
| WO (1) | WO2003064442A2 (de) |
Families Citing this family (25)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BR0106522A (pt) * | 2001-12-17 | 2003-09-09 | Resitec Ind Quimica Ltda | Processo para separar produtos valiosos insaponificáveis obtidos de matérias primas diversas |
| CN100334103C (zh) * | 2005-09-20 | 2007-08-29 | 南京工业大学 | 一种从植物油沥青中提取植物甾醇乙酸酯的方法 |
| US8309156B2 (en) * | 2005-12-20 | 2012-11-13 | Pharmachem Laboratories, Inc. | Compositions comprising one or more phytosterols and/or phytostanols, or derivatives thereof, and high HLB emulsifiers |
| US8318962B2 (en) * | 2006-12-29 | 2012-11-27 | Cognis Ip Management Gmbh | Process for recovering sterols from a crude source containing sterol esters |
| FI20070137A0 (fi) | 2007-02-15 | 2007-02-15 | Raisio Benecol Oy | Menetelmä rasvahappojen, hartsihappojen ja sterolien eristämiseksi mäntyöljypiestä |
| FI20080174A0 (fi) * | 2008-02-29 | 2008-02-29 | Raisio Nutrition Ltd | Menetelmä sterolien ja happojen erottamiseksi mäntyöljypiestä |
| FI124101B (en) | 2012-05-14 | 2014-03-14 | Hankkija Maatalous Oy | Modified tall oil fatty acid |
| US8709238B2 (en) | 2012-05-18 | 2014-04-29 | Uop Llc | Process for separating crude tall oil for processing into fuels |
| FI124918B (fi) | 2013-05-14 | 2015-03-31 | Hankkija Maatalous Oy | Mäntyöljyrasvahappo |
| FI125051B (fi) | 2013-10-24 | 2015-05-15 | Hankkija Oy | Mäntyöljyrasvahappo |
| HUE050907T2 (hu) | 2013-11-13 | 2021-01-28 | Hankkija Oy | Gyantasavakat tartalmazó takarmány-kiegészítõ |
| CN103897009B (zh) * | 2014-04-14 | 2015-08-12 | 西安海斯夫生物科技有限公司 | 一种木浆浮油的分离方法 |
| MY185625A (en) * | 2015-07-02 | 2021-05-26 | Malaysian Palm Oil Board Mpob | Method of extracting and concentrating phytosterol from palm oil by-product |
| MX2018015242A (es) | 2016-06-10 | 2019-08-12 | Alm Holding Co | Esterol crudo como aditivo en aglutinante de asfalto. |
| JP7169265B2 (ja) | 2016-08-09 | 2022-11-10 | エー.エル.エム.ホールディング カンパニー | アスファルトバインダ中の添加剤としてのステロールブレンド |
| CN106433474A (zh) * | 2016-11-21 | 2017-02-22 | 无锡市伟丰印刷机械厂 | 一种松脂用高效溶解提纯设备 |
| PE20191365A1 (es) | 2017-02-02 | 2019-10-01 | Alm Holding Co | Emulsiones bituminosas que contienen aditivos de esteroles para pavimento asfaltico |
| WO2019023172A1 (en) | 2017-07-26 | 2019-01-31 | A.L.M Holding Company | USE OF STEROLS FROM ANIMAL WASTE AS ADDITIVE IN ASPHALT BINDER |
| CN107417759B (zh) * | 2017-08-11 | 2020-04-17 | 内蒙古昶辉生物科技股份有限公司 | 从纸浆浮油沥青中提炼植物甾醇以及甾醇酯的制备方法 |
| CR20200164A (es) | 2017-10-20 | 2020-10-22 | Alm Holding Co | Tratamiento de superficie de emulsion de asfalto conteniendo esteroles |
| CA3101341A1 (en) * | 2018-06-01 | 2019-12-05 | Raisio Nutrition Ltd | Process for isolation of sterols and a fraction rich in fatty acids and resin acids |
| CN108912199A (zh) * | 2018-06-21 | 2018-11-30 | 江苏科鼐生物制品有限公司 | 一种木甾醇的制备方法及系统 |
| CN108912198A (zh) * | 2018-06-21 | 2018-11-30 | 江苏科鼐生物制品有限公司 | 一种高收率木甾醇的制备方法及系统 |
| CN108912196A (zh) * | 2018-06-21 | 2018-11-30 | 江苏科鼐生物制品有限公司 | 一种植物甾醇汽提脱溶剂的方法及系统 |
| CN115281250B (zh) * | 2022-09-20 | 2024-02-09 | 青岛葆福德生物医药科技有限公司 | 一种降血脂食用油配方及其制备工艺 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2835682A (en) * | 1955-08-08 | 1958-05-20 | Swift & Co | Sterol recovery process |
| US3649580A (en) * | 1969-03-13 | 1972-03-14 | Arizona Chem | Tall oil pitch tackifiers in ethylene-propylene terpolymer rubber |
| US3556827A (en) * | 1969-12-29 | 1971-01-19 | Kenneth E Mcconnaughay | Aggregate binder and paving composition |
| CA2230373A1 (en) * | 1998-02-20 | 1999-08-20 | Forbes Medi-Tech Inc. | Method for the preparation of phytosterols from tall oil pitch |
| US7371876B2 (en) * | 1999-04-27 | 2008-05-13 | Sterol Technologies Ltd. | Process for the purification of sterols from hydrocarbon extracts using evaporative fractionation |
-
2002
- 2002-01-28 US US10/060,022 patent/US20030144536A1/en not_active Abandoned
-
2003
- 2003-01-27 JP JP2003564062A patent/JP2005516069A/ja active Pending
- 2003-01-27 WO PCT/CA2003/000098 patent/WO2003064442A2/en not_active Ceased
- 2003-01-27 BR BR0307270-3A patent/BR0307270A/pt not_active Application Discontinuation
- 2003-01-27 ES ES03701377T patent/ES2335754T3/es not_active Expired - Lifetime
- 2003-01-27 NZ NZ534369A patent/NZ534369A/en not_active IP Right Cessation
- 2003-01-27 EP EP03701377A patent/EP1470149B1/de not_active Revoked
- 2003-01-27 AU AU2003203072A patent/AU2003203072B2/en not_active Ceased
- 2003-01-27 CN CN03804912.0A patent/CN1639184A/zh active Pending
- 2003-01-27 DE DE60329977T patent/DE60329977D1/de not_active Expired - Lifetime
- 2003-01-27 AT AT03701377T patent/ATE448239T1/de not_active IP Right Cessation
- 2003-01-27 CA CA002474592A patent/CA2474592A1/en not_active Abandoned
Also Published As
| Publication number | Publication date |
|---|---|
| DE60329977D1 (de) | 2009-12-24 |
| EP1470149B1 (de) | 2009-11-11 |
| JP2005516069A (ja) | 2005-06-02 |
| CN1639184A (zh) | 2005-07-13 |
| BR0307270A (pt) | 2004-12-14 |
| AU2003203072B2 (en) | 2009-04-23 |
| WO2003064442A3 (en) | 2003-10-02 |
| US20030144536A1 (en) | 2003-07-31 |
| ES2335754T3 (es) | 2010-04-05 |
| EP1470149A2 (de) | 2004-10-27 |
| WO2003064442A2 (en) | 2003-08-07 |
| NZ534369A (en) | 2006-07-28 |
| CA2474592A1 (en) | 2003-08-07 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| RER | Ceased as to paragraph 5 lit. 3 law introducing patent treaties |