ATE475467T1 - Verfahren zur wiedergewinnung von katalysatoren aus hydrocyanierungsproduktgemischen - Google Patents

Verfahren zur wiedergewinnung von katalysatoren aus hydrocyanierungsproduktgemischen

Info

Publication number
ATE475467T1
ATE475467T1 AT04700629T AT04700629T ATE475467T1 AT E475467 T1 ATE475467 T1 AT E475467T1 AT 04700629 T AT04700629 T AT 04700629T AT 04700629 T AT04700629 T AT 04700629T AT E475467 T1 ATE475467 T1 AT E475467T1
Authority
AT
Austria
Prior art keywords
diphosphite
containing compounds
organic
saturated
disclosed
Prior art date
Application number
AT04700629T
Other languages
English (en)
Inventor
Scott Jackson
Ronald Mckinney
Original Assignee
Invista Tech Sarl
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Invista Tech Sarl filed Critical Invista Tech Sarl
Application granted granted Critical
Publication of ATE475467T1 publication Critical patent/ATE475467T1/de

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/18—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes containing nitrogen, phosphorus, arsenic or antimony as complexing atoms, e.g. in pyridine ligands, or in resonance therewith, e.g. in isocyanide ligands C=N-R or as complexed central atoms
    • B01J31/1845—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes containing nitrogen, phosphorus, arsenic or antimony as complexing atoms, e.g. in pyridine ligands, or in resonance therewith, e.g. in isocyanide ligands C=N-R or as complexed central atoms the ligands containing phosphorus
    • B01J31/185—Phosphites ((RO)3P), their isomeric phosphonates (R(RO)2P=O) and RO-substitution derivatives thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B01D11/0426—Counter-current multistage extraction towers in a vertical or sloping position
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B01D11/0446—Juxtaposition of mixers-settlers
    • B01D11/0457—Juxtaposition of mixers-settlers comprising rotating mechanisms, e.g. mixers, mixing pumps
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/26—Catalysts comprising hydrides, coordination complexes or organic compounds containing in addition, inorganic metal compounds not provided for in groups B01J31/02 - B01J31/24
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/40—Regeneration or reactivation
    • B01J31/4015—Regeneration or reactivation of catalysts containing metals
    • B01J31/4053—Regeneration or reactivation of catalysts containing metals with recovery of phosphorous catalyst system constituents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J38/00—Regeneration or reactivation of catalysts, in general
    • B01J38/48—Liquid treating or treating in liquid phase, e.g. dissolved or suspended
    • B01J38/50—Liquid treating or treating in liquid phase, e.g. dissolved or suspended using organic liquids
    • B01J38/56—Hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/025—Purification; Separation; Stabilisation; Desodorisation of organo-phosphorus compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2231/00—Catalytic reactions performed with catalysts classified in B01J31/00
    • B01J2231/30—Addition reactions at carbon centres, i.e. to either C-C or C-X multiple bonds
    • B01J2231/32—Addition reactions to C=C or C-C triple bonds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/02—Compositional aspects of complexes used, e.g. polynuclearity
    • B01J2531/0261—Complexes comprising ligands with non-tetrahedral chirality
    • B01J2531/0266—Axially chiral or atropisomeric ligands, e.g. bulky biaryls such as donor-substituted binaphthalenes, e.g. "BINAP" or "BINOL"
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/80—Complexes comprising metals of Group VIII as the central metal
    • B01J2531/84—Metals of the iron group
    • B01J2531/847—Nickel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/0234—Nitrogen-, phosphorus-, arsenic- or antimony-containing compounds
    • B01J31/0235—Nitrogen containing compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/0234—Nitrogen-, phosphorus-, arsenic- or antimony-containing compounds
    • B01J31/0255—Phosphorus containing compounds
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/584—Recycling of catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
AT04700629T 2003-01-08 2004-01-07 Verfahren zur wiedergewinnung von katalysatoren aus hydrocyanierungsproduktgemischen ATE475467T1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US10/338,567 US6936171B2 (en) 2003-01-08 2003-01-08 Process for catalyst recovery from hydrocyanation product mixtures
PCT/US2004/000375 WO2004062765A1 (en) 2003-01-08 2004-01-07 Process for catalyst recovery from hydrocyanation product mixtures

Publications (1)

Publication Number Publication Date
ATE475467T1 true ATE475467T1 (de) 2010-08-15

Family

ID=32710978

Family Applications (1)

Application Number Title Priority Date Filing Date
AT04700629T ATE475467T1 (de) 2003-01-08 2004-01-07 Verfahren zur wiedergewinnung von katalysatoren aus hydrocyanierungsproduktgemischen

Country Status (8)

Country Link
US (1) US6936171B2 (de)
EP (1) EP1581323B1 (de)
CN (1) CN100386128C (de)
AT (1) ATE475467T1 (de)
DE (1) DE602004028336D1 (de)
MY (1) MY135238A (de)
TW (1) TW200417412A (de)
WO (1) WO2004062765A1 (de)

Families Citing this family (30)

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US6906218B2 (en) * 2002-12-18 2005-06-14 Invista North America S.A.R.L. Cyclohexane derivatives and methods for their preparation
FR2850966B1 (fr) 2003-02-10 2005-03-18 Rhodia Polyamide Intermediates Procede de fabrication de composes dinitriles
FR2854891B1 (fr) 2003-05-12 2006-07-07 Rhodia Polyamide Intermediates Procede de preparation de dinitriles
FR2854892B1 (fr) 2003-05-12 2005-06-24 Rhodia Polyamide Intermediates Procede de fabrication de dinitriles
DE102004050935A1 (de) * 2004-10-18 2006-04-20 Basf Ag Extraktion von Nickel(0)-Komplexen aus Nitrilgemischen mit verminderter Mulmbildung
EP1996598B1 (de) 2006-03-17 2013-10-16 Invista Technologies S.à.r.l. Verfahren zur reinigung von triorganophosphiten durch bearbeitung mit einem basischen zusatz
CN101460229A (zh) * 2006-04-07 2009-06-17 巴斯夫欧洲公司 从腈混合物分离镍(0)配合物和含磷配体的方法
US7919646B2 (en) 2006-07-14 2011-04-05 Invista North America S.A R.L. Hydrocyanation of 2-pentenenitrile
US7659422B2 (en) * 2006-07-14 2010-02-09 Invista North America S.A.R.L. Hydrocyanation process with reduced yield losses
US7709674B2 (en) 2006-07-14 2010-05-04 Invista North America S.A R.L Hydrocyanation process with reduced yield losses
US7880028B2 (en) 2006-07-14 2011-02-01 Invista North America S.A R.L. Process for making 3-pentenenitrile by hydrocyanation of butadiene
US7709673B2 (en) * 2006-07-14 2010-05-04 Invista North America S.A R.L. Process for making 3-pentenenitrile by hydrocyanation of butadiene
WO2009091790A1 (en) 2008-01-15 2009-07-23 Invista Technologies S.A.R.L. Hydrocyanation of pentenenitriles
CN101910119B (zh) 2008-01-15 2013-05-29 因温斯特技术公司 用于制备和精制3-戊烯腈，和用于精制2-甲基-3-丁烯腈的方法
WO2012005910A1 (en) 2010-07-07 2012-01-12 Invista Technologies S.A. R.L. Process for making nitriles
HK1199630A1 (en) * 2011-12-21 2015-07-10 因温斯特技术公司 Extraction solvent control for reducing stable emulsions
EP2794048B1 (de) 2011-12-21 2022-01-05 INVISTA Textiles (U.K.) Limited Regelung des extraktionslösungsmittels zur verminderung stabiler emulsionen
CN103402595B (zh) 2011-12-21 2016-02-03 因温斯特技术公司 用于减少稳定乳液的萃取溶剂控制
EP2794046B1 (de) 2011-12-21 2016-02-03 Invista Technologies S.A R.L. Regelung des extraktionslösungsmittels zur verminderung stabiler emulsionen
EP3010616B1 (de) 2013-06-20 2022-09-28 INVISTA Textiles (U.K.) Limited Steuerung eines extraktionslösungsmittels zur reduzierung stabiler emulsionen
EP3010617B1 (de) 2013-06-20 2022-11-30 INVISTA Textiles (U.K.) Limited Steuerung eines extraktionslösungsmittels zur reduzierung stabiler emulsionen
EP3010615B1 (de) 2013-06-20 2022-09-28 INVISTA Textiles (U.K.) Limited Verfahren zur rückgewinnung von diphosphonithaltigen verbindungen mittels eines mehrstufigen gegenstrom-flüssig-flüssig-extraktors mit misch-absetzer und rückführung der schweren phase
WO2014205195A1 (en) * 2013-06-20 2014-12-24 Invista Technologies S.A.R.L. Extraction solvent control for reducing stable emulsions
US9676800B2 (en) 2013-06-20 2017-06-13 Invista North America S.A.R.L. Extraction solvent control for reducing stable emulsions
CN105531257B (zh) 2013-07-17 2019-12-17 英威达纺织（英国）有限公司 通过蒸馏将溶剂与镍催化剂分离
CN103408178B (zh) * 2013-08-22 2015-07-22 太原理工大学 从hpf焦化脱硫废液中回收脱硫催化剂的工艺
US9914700B2 (en) 2014-06-27 2018-03-13 Invista North America S.A R.L. Enhanced extraction of impurities from mixture comprising nitriles
CN107207406B (zh) 2014-06-27 2019-12-03 英威达纺织（英国）有限公司 用增强的液-液萃取制造腈的整合方法
CN113044904B (zh) * 2021-05-10 2022-06-03 中国科学院过程工程研究所 协同萃取煤化工废水中难降解污染物和酚的萃取剂及方法
CN119390607B (zh) * 2024-09-27 2025-11-25 中国天辰工程有限公司 一种氢氰化反应方法

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Also Published As

Publication number Publication date
MY135238A (en) 2008-03-31
US6936171B2 (en) 2005-08-30
US20040140263A1 (en) 2004-07-22
EP1581323A4 (de) 2008-07-02
EP1581323A1 (de) 2005-10-05
TW200417412A (en) 2004-09-16
WO2004062765A1 (en) 2004-07-29
CN100386128C (zh) 2008-05-07
CN1723067A (zh) 2006-01-18
EP1581323B1 (de) 2010-07-28
DE602004028336D1 (de) 2010-09-09

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