ATE488486T1 - Verfahren zur herstellung von cyclohexanon - Google Patents
Verfahren zur herstellung von cyclohexanonInfo
- Publication number
- ATE488486T1 ATE488486T1 AT05822993T AT05822993T ATE488486T1 AT E488486 T1 ATE488486 T1 AT E488486T1 AT 05822993 T AT05822993 T AT 05822993T AT 05822993 T AT05822993 T AT 05822993T AT E488486 T1 ATE488486 T1 AT E488486T1
- Authority
- AT
- Austria
- Prior art keywords
- cyclohexanone
- cyclohexane
- caprolactam
- cyclohexanol
- raw material
- Prior art date
Links
- JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 title abstract 12
- 238000004519 manufacturing process Methods 0.000 title abstract 3
- 238000000034 method Methods 0.000 abstract 4
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 abstract 3
- HPXRVTGHNJAIIH-UHFFFAOYSA-N cyclohexanol Chemical compound OC1CCCCC1 HPXRVTGHNJAIIH-UHFFFAOYSA-N 0.000 abstract 2
- JBKVHLHDHHXQEQ-UHFFFAOYSA-N epsilon-caprolactam Chemical compound O=C1CCCCCN1 JBKVHLHDHHXQEQ-UHFFFAOYSA-N 0.000 abstract 2
- 239000012535 impurity Substances 0.000 abstract 2
- 239000002994 raw material Substances 0.000 abstract 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract 1
- 230000015572 biosynthetic process Effects 0.000 abstract 1
- RALDHUZFXJKFQB-UHFFFAOYSA-N cyclopentene-1-carbaldehyde Chemical compound O=CC1=CCCC1 RALDHUZFXJKFQB-UHFFFAOYSA-N 0.000 abstract 1
- 238000006356 dehydrogenation reaction Methods 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 230000003647 oxidation Effects 0.000 abstract 1
- 238000007254 oxidation reaction Methods 0.000 abstract 1
- 229910052760 oxygen Inorganic materials 0.000 abstract 1
- 239000001301 oxygen Substances 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 abstract 1
- 238000003786 synthesis reaction Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C407/00—Preparation of peroxy compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C409/00—Peroxy compounds
- C07C409/02—Peroxy compounds the —O—O— group being bound between a carbon atom, not further substituted by oxygen atoms, and hydrogen, i.e. hydroperoxides
- C07C409/14—Peroxy compounds the —O—O— group being bound between a carbon atom, not further substituted by oxygen atoms, and hydrogen, i.e. hydroperoxides the carbon atom belonging to a ring other than a six-membered aromatic ring
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
- C07C45/32—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen
- C07C45/33—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
- C07C49/385—Saturated compounds containing a keto group being part of a ring
- C07C49/403—Saturated compounds containing a keto group being part of a ring of a six-membered ring
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
- C07D201/02—Preparation of lactams
- C07D201/04—Preparation of lactams from or via oximes by Beckmann rearrangement
- C07D201/06—Preparation of lactams from or via oximes by Beckmann rearrangement from ketones by simultaneous oxime formation and rearrangement
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
- C07C2601/14—The ring being saturated
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR0412976A FR2878847B1 (fr) | 2004-12-07 | 2004-12-07 | Procede de preparation de cyclohexanone |
| PCT/FR2005/002979 WO2006061487A1 (fr) | 2004-12-07 | 2005-11-30 | Procede de preparation de cyclohexanone |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE488486T1 true ATE488486T1 (de) | 2010-12-15 |
Family
ID=34952021
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT05822993T ATE488486T1 (de) | 2004-12-07 | 2005-11-30 | Verfahren zur herstellung von cyclohexanon |
Country Status (14)
| Country | Link |
|---|---|
| US (1) | US7579506B2 (de) |
| EP (1) | EP1819655B1 (de) |
| JP (1) | JP5005545B2 (de) |
| KR (1) | KR100924256B1 (de) |
| CN (1) | CN101137608B (de) |
| AT (1) | ATE488486T1 (de) |
| DE (1) | DE602005024853D1 (de) |
| ES (1) | ES2353236T3 (de) |
| FR (1) | FR2878847B1 (de) |
| PL (1) | PL1819655T3 (de) |
| RU (1) | RU2373181C2 (de) |
| TW (1) | TWI361804B (de) |
| UA (1) | UA83597C2 (de) |
| WO (1) | WO2006061487A1 (de) |
Families Citing this family (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7714172B2 (en) * | 2006-06-29 | 2010-05-11 | Basf Se | Method for the production of cyclic ketones |
| WO2012036818A1 (en) | 2010-09-14 | 2012-03-22 | Exxonmobil Chemical Patents Inc. | Cyclohexanone compositions |
| WO2012146145A1 (zh) * | 2011-04-29 | 2012-11-01 | 岳阳昌德化工实业有限公司 | 一种环己烷氧化的方法 |
| WO2013083513A1 (en) * | 2011-12-07 | 2013-06-13 | Dsm Ip Assets B.V. | Process for the production of a mixture comprising cyclohexanol and cyclohexanone |
| CN103987452B (zh) * | 2011-12-07 | 2016-02-24 | Capiii有限公司 | 包含环己醇和环己酮的混合物的制备方法 |
| CN102627541B (zh) * | 2012-03-28 | 2014-07-23 | 湖北三宁化工股份有限公司 | 一种环己烷氧化制备环己醇和环己酮的工艺及其设备 |
| CN103265418A (zh) * | 2013-06-08 | 2013-08-28 | 南京德力菲技术咨询有限公司 | 一种水合环己烯法环己醇制己内酰胺原料环己酮的方法 |
| CN106660935A (zh) * | 2014-05-12 | 2017-05-10 | 微麦德斯公司 | 从5‑(卤甲基)糠醛产生化合物的方法 |
| WO2016053466A1 (en) | 2014-09-30 | 2016-04-07 | Exxonmobil Chemical Patents Inc. | Process for making cyclohexanone |
| TWI691480B (zh) * | 2014-12-15 | 2020-04-21 | 荷蘭商卡普三世責任有限公司 | 用來建構用於生產環己酮之設備的方法 |
| US20180186715A1 (en) | 2015-07-29 | 2018-07-05 | Exxonmobil Chemical Patents Inc. | Cyclohexanone Compositions and Processes for Making Such Compositions |
| WO2017023429A1 (en) | 2015-07-31 | 2017-02-09 | Exxonmobil Chemical Patents Inc. | Process for making cyclohexanone |
| EP3328823A1 (de) | 2015-07-31 | 2018-06-06 | ExxonMobil Chemical Patents Inc. | Verfahren zur herstellung von cyclohexanon |
| RU2618273C1 (ru) * | 2015-11-10 | 2017-05-03 | Федеральное государственное бюджетное образовательное учреждение высшего образования "Московский технологический университет " | Способ выделения циклогексанона из реакционной смеси вода - ацетонитрил - циклогексен - циклогексанон |
| US10941099B2 (en) | 2017-06-28 | 2021-03-09 | Exxonmobil Chemical Patents Inc. | Cyclohexanone-containing products and processes for making the same |
| WO2019005276A1 (en) | 2017-06-28 | 2019-01-03 | Exxonmobil Chemical Patents Inc. | PRODUCTS CONTAINING CYCLOHEXANONE AND METHODS OF MAKING THE SAME |
| WO2019005274A1 (en) | 2017-06-28 | 2019-01-03 | Exxonmobil Chemical Patents Inc. | PROCESS FOR PRODUCTION OF CYCLOHEXANONE |
| CN108164396B (zh) * | 2018-01-04 | 2021-03-16 | 中石化上海工程有限公司 | 高效分离精制环戊醇的方法 |
| RU2676037C1 (ru) * | 2018-04-17 | 2018-12-25 | Федеральное государственное бюджетное образовательное учреждение высшего образования "МИРЭА - Российский технологический университет" | Способ разделения смеси циклогексен-вода-циклогексанон-дмсо |
| CN112745208B (zh) * | 2019-10-30 | 2022-09-09 | 中国石油化工股份有限公司 | 一种环己酮回收分离工艺及系统 |
Family Cites Families (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1188584B (de) * | 1961-11-28 | 1965-03-11 | Basf Ag | Verfahren zur Gewinnung von reinem, gegebenenfalls methylsubstituiertem Cyclohexanon |
| BE659166A (de) * | 1964-02-03 | 1965-08-02 | ||
| NL7215853A (de) * | 1972-11-23 | 1974-05-27 | ||
| FR2604998B1 (fr) * | 1986-10-10 | 1989-06-09 | Rhone Poulenc Chimie | Procede de preparation d'un melange renfermant du cyclohexanol et de la cyclohexanone a partir du cyclohexane |
| JP2511507B2 (ja) | 1988-09-28 | 1996-06-26 | 富士写真フイルム株式会社 | 画像露光装置 |
| US4918239A (en) * | 1988-12-27 | 1990-04-17 | National Science Council | Method of producing cyclohexanone from cyclohexanol through oxidative dehydrogenation |
| JPH06104637B2 (ja) * | 1990-04-06 | 1994-12-21 | 三菱化成株式会社 | シクロヘキサノン及びシクロヘキサノールの混合物から不純物を除去する方法 |
| NL9100521A (nl) * | 1991-03-25 | 1992-10-16 | Stamicarbon | Werkwijze voor de bereiding van een alkanon en/of alkanol. |
| DE4205633A1 (de) | 1992-02-25 | 1993-08-26 | Bayer Antwerpen Nv | Verfahren zur reinigung von cyclohexanon |
| JP2500977B2 (ja) | 1992-03-24 | 1996-05-29 | 三菱化学株式会社 | シクロヘキサノンの製造方法 |
| NL9201269A (nl) * | 1992-07-15 | 1994-02-01 | Dsm Nv | Werkwijze voor de bereiding van cyclohexylhydroperoxide. |
| JPH11322661A (ja) * | 1998-05-11 | 1999-11-24 | Mitsubishi Chemical Corp | シクロヘキサノンの製造方法及びε−カプロラクタムの製造方法 |
| JP4150771B2 (ja) * | 1999-04-07 | 2008-09-17 | 独立行政法人産業技術総合研究所 | シクロヘキサノール脱水素反応用触媒 |
| JP2002292282A (ja) | 2001-03-29 | 2002-10-08 | Sud-Chemie Catalysts Inc | シクロヘキサノール脱水素触媒及びその製造方法 |
| US6703529B1 (en) * | 2002-09-12 | 2004-03-09 | E. I. Du Pont De Nemours And Company | Process for oxidation of cyclohexane |
| EP1433774A1 (de) * | 2002-12-27 | 2004-06-30 | Koninklijke DSM N.V. | Verfahren zur Reduzierung der Aldehydkonzentration in einer Cyclohexanon- und eine oder mehrere Aldehyd enthaltende Mischung |
-
2004
- 2004-12-07 FR FR0412976A patent/FR2878847B1/fr not_active Expired - Fee Related
-
2005
- 2005-11-30 ES ES05822993T patent/ES2353236T3/es not_active Expired - Lifetime
- 2005-11-30 DE DE602005024853T patent/DE602005024853D1/de not_active Expired - Lifetime
- 2005-11-30 UA UAA200706285A patent/UA83597C2/uk unknown
- 2005-11-30 PL PL05822993T patent/PL1819655T3/pl unknown
- 2005-11-30 KR KR1020077012801A patent/KR100924256B1/ko not_active Expired - Fee Related
- 2005-11-30 WO PCT/FR2005/002979 patent/WO2006061487A1/fr not_active Ceased
- 2005-11-30 RU RU2007125672/04A patent/RU2373181C2/ru not_active IP Right Cessation
- 2005-11-30 EP EP05822993A patent/EP1819655B1/de not_active Expired - Lifetime
- 2005-11-30 AT AT05822993T patent/ATE488486T1/de not_active IP Right Cessation
- 2005-11-30 CN CN2005800417907A patent/CN101137608B/zh not_active Expired - Fee Related
- 2005-11-30 US US11/792,373 patent/US7579506B2/en not_active Expired - Fee Related
- 2005-11-30 JP JP2007544940A patent/JP5005545B2/ja not_active Expired - Fee Related
- 2005-12-07 TW TW094143258A patent/TWI361804B/zh not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| UA83597C2 (uk) | 2008-07-25 |
| ES2353236T3 (es) | 2011-02-28 |
| RU2007125672A (ru) | 2009-01-20 |
| KR20070085836A (ko) | 2007-08-27 |
| DE602005024853D1 (de) | 2010-12-30 |
| WO2006061487A1 (fr) | 2006-06-15 |
| US20080064902A1 (en) | 2008-03-13 |
| CN101137608B (zh) | 2012-01-25 |
| JP2008523037A (ja) | 2008-07-03 |
| FR2878847A1 (fr) | 2006-06-09 |
| TWI361804B (en) | 2012-04-11 |
| US7579506B2 (en) | 2009-08-25 |
| CN101137608A (zh) | 2008-03-05 |
| PL1819655T3 (pl) | 2011-05-31 |
| KR100924256B1 (ko) | 2009-10-30 |
| EP1819655B1 (de) | 2010-11-17 |
| TW200631932A (en) | 2006-09-16 |
| JP5005545B2 (ja) | 2012-08-22 |
| RU2373181C2 (ru) | 2009-11-20 |
| EP1819655A1 (de) | 2007-08-22 |
| FR2878847B1 (fr) | 2007-01-05 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| RER | Ceased as to paragraph 5 lit. 3 law introducing patent treaties |