ATE555098T1 - Verfahren zur herstellung 1,3-disubstituierter pyrazolcarbonsäureester - Google Patents

Verfahren zur herstellung 1,3-disubstituierter pyrazolcarbonsäureester

Info

Publication number
ATE555098T1
ATE555098T1 AT09780455T AT09780455T ATE555098T1 AT E555098 T1 ATE555098 T1 AT E555098T1 AT 09780455 T AT09780455 T AT 09780455T AT 09780455 T AT09780455 T AT 09780455T AT E555098 T1 ATE555098 T1 AT E555098T1
Authority
AT
Austria
Prior art keywords
pyrazolecarbonic
disubstituted
producing
acid esters
esters
Prior art date
Application number
AT09780455T
Other languages
English (en)
Inventor
Bernd Wolf
Sebastian Smidt
Volker Maywald
Chistopher Koradin
Michael Rack
Michael Keil
Thomas Zierke
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Application granted granted Critical
Publication of ATE555098T1 publication Critical patent/ATE555098T1/de

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D233/00—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings
    • C07D233/54—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members
    • C07D233/66—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D233/90—Carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C243/00—Compounds containing chains of nitrogen atoms singly-bound to each other, e.g. hydrazines, triazanes
    • C07C243/10—Hydrazines
    • C07C243/12—Hydrazines having nitrogen atoms of hydrazine groups bound to acyclic carbon atoms
    • C07C243/14—Hydrazines having nitrogen atoms of hydrazine groups bound to acyclic carbon atoms of a saturated carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C59/00—Compounds having carboxyl groups bound to acyclic carbon atoms and containing any of the groups OH, O—metal, —CHO, keto, ether, groups, groups, or groups
    • C07C59/125—Saturated compounds having only one carboxyl group and containing ether groups, groups, groups, or groups
    • C07C59/135—Saturated compounds having only one carboxyl group and containing ether groups, groups, groups, or groups containing halogen

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
AT09780455T 2008-07-21 2009-07-10 Verfahren zur herstellung 1,3-disubstituierter pyrazolcarbonsäureester ATE555098T1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP08160833 2008-07-21
PCT/EP2009/058854 WO2010009990A1 (en) 2008-07-21 2009-07-10 Process for preparing 1,3-disubstituted pyrazolecarboxylic esters

Publications (1)

Publication Number Publication Date
ATE555098T1 true ATE555098T1 (de) 2012-05-15

Family

ID=41037857

Family Applications (1)

Application Number Title Priority Date Filing Date
AT09780455T ATE555098T1 (de) 2008-07-21 2009-07-10 Verfahren zur herstellung 1,3-disubstituierter pyrazolcarbonsäureester

Country Status (11)

Country Link
US (1) US8344157B2 (de)
EP (1) EP2307384B1 (de)
JP (1) JP5558467B2 (de)
KR (1) KR20110031501A (de)
CN (1) CN102099343B (de)
AR (1) AR072580A1 (de)
AT (1) ATE555098T1 (de)
BR (1) BRPI0915801A2 (de)
IL (1) IL210308A (de)
MX (1) MX2011000209A (de)
WO (1) WO2010009990A1 (de)

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8586750B2 (en) 2008-05-02 2013-11-19 Basf Se Method for the production of halogen-substituted 2-(aminomethylidene)-3-oxobutyric acid esters
PL2300417T3 (pl) 2008-05-02 2015-12-31 Basf Se Sposób wytwarzania estrów kwasu 2-(aminometylideno)-4,4-difluoro-3-oksomasłowego
BRPI0911767A2 (pt) 2008-05-05 2015-07-28 Basf Se Processo, e, composto.
CN102471278B (zh) 2009-07-28 2015-04-01 先正达参股股份有限公司 关于吡唑的烷基化方法
GB201004299D0 (en) * 2010-03-15 2010-04-28 Syngenta Participations Ag Process
WO2012025469A1 (en) * 2010-08-24 2012-03-01 Solvay Sa Improved process for the preparation of esters of 1-h-pyrazole-4-carboxylic acids
CN102702104B (zh) * 2012-06-08 2015-02-25 巨化集团公司 一种3-二氟甲基-1-甲基吡唑-4-甲酸乙酯的连续化合成方法
CN102766096A (zh) * 2012-07-20 2012-11-07 苏州汉德创宏生化科技有限公司 合成3-二氟甲基-1-甲基-1-氢-吡唑-4-甲酸及其酯类的方法
JP5140776B1 (ja) * 2012-09-05 2013-02-13 タマ化学工業株式会社 １−置換−３−フルオロアルキルピラゾール−４−カルボン酸エステルの製造方法
US8871947B2 (en) 2013-02-04 2014-10-28 KingChem LLC Preparation of alkyl 3-difluoromethyl-1-methyl-1H-pyrazole-4-carboxylic acid ester
US9139507B2 (en) 2013-12-09 2015-09-22 KingChem LLC. Process for the preparation of alkyl 3-difluoromethyl-1-methyl-1H-pyrazole-4-carboxylate and its analogs
CN105218448B (zh) * 2015-07-31 2017-11-07 江苏恒润制药有限公司 一种1‑甲基‑3‑二氟甲基‑4‑吡唑甲酸的合成方法
JP6995195B2 (ja) 2018-05-18 2022-02-04 富士フイルム株式会社 ３－ジフルオロメチルピラゾール化合物の製造方法及び３－ジフルオロメチルピラゾール－４－カルボン酸化合物の製造方法、並びに、ピラゾリジン化合物
WO2019224677A1 (en) 2018-05-21 2019-11-28 Pi Industries Ltd. Method for preparing substituted heterocyclic compounds
CN114058007B (zh) * 2021-11-22 2022-10-25 华南理工大学 一种有机碱催化炔羧酸聚合制备聚羰基烯醇酯类化合物的方法

Family Cites Families (34)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0822853B2 (ja) 1987-10-23 1996-03-06 三井東圧化学株式会社 ピラゾール−４−カルボン酸類およびその製造方法
JPH0266612A (ja) 1988-08-31 1990-03-06 Toshiba Corp 冷蔵庫の温度制御回路
US5093347A (en) * 1991-01-28 1992-03-03 Monsanto Company 3-difluoromethylpyrazolecarboxamide fungicides, compositions and use
IL103614A (en) * 1991-11-22 1998-09-24 Basf Ag Carboxamides for controlling botrytis and certain novel such compounds
US5223526A (en) 1991-12-06 1993-06-29 Monsanto Company Pyrazole carboxanilide fungicides and use
TW268881B (de) * 1992-07-07 1996-01-21 Ciba Geigy Ag
DE4231517A1 (de) * 1992-09-21 1994-03-24 Basf Ag Carbonsäureanilide, Verfahren zu ihrer Herstellung und sie enthaltende Mittel zur Bekämpfung von Schadpilzen
KR100344363B1 (ko) * 1993-11-30 2002-11-30 일라이 릴리 앤드 캄파니 2,2-디플루오로케텐실릴아세탈의제조방법
US5498624A (en) 1995-05-03 1996-03-12 Monsanto Company Selected pyrazolyl derivatives
JP2000212166A (ja) 1999-01-26 2000-08-02 Mitsui Chemicals Inc １，３―ジアルキルピラゾ―ル―４―カルボン酸エステルの製造法
DE10161978A1 (de) 2001-12-17 2003-06-26 Bayer Ag Verfahren zur Herstellung von 2-Halogenacyl-3-amino-acrylsäure-derivate
DE10204391A1 (de) 2002-02-04 2003-08-14 Bayer Cropscience Ag Difluormethylthiazolylcarboxanilide
DE10215292A1 (de) * 2002-02-19 2003-08-28 Bayer Cropscience Ag Disubstitutierte Pyrazolylcarbocanilide
EP1644314B1 (de) 2003-07-01 2011-08-10 Bayer Cropscience AG Verfahren zum herstellen von difluoracetessigs urealkylestern
DE10349500A1 (de) 2003-10-23 2005-06-02 Bayer Cropscience Ag Verfahren zum Herstellen von 2-Dihalogenacyl-3-amino-acrylsäureestern und 3-Dihalogenmethyl-pyrazol-4-carbonsäureestern
DE10351088A1 (de) * 2003-10-31 2005-06-02 Bayer Cropscience Gmbh Verfahren zum Herstellen von fluormethyl-substituierten Heterocyclen
US20080108686A1 (en) * 2004-06-18 2008-05-08 Basf Aktiengesellschaft N-(Ortho-Phenyl)-1-Methyl-3-Difluoromethylpyrazole-4-Carboxanilides And Their Use As Fungicides
DE102004041532A1 (de) * 2004-08-27 2006-03-02 Bayer Cropscience Ag Biphenylthiazolcarboxamide
US7863460B2 (en) * 2005-02-25 2011-01-04 Sagami Chemical Research Center Process for producing 1-substituted-3-fluoroalkylpyrazole-4-carboxylate
US20090233795A1 (en) 2005-07-05 2009-09-17 Basf Akitengesellschaft Fungicidal Mixtres Based On 3-Monosubstituted N-Bipenyl-Pyrazolecarboxamides
US20090123561A1 (en) 2005-07-14 2009-05-14 Basf Aktiengeselllschaft Fungicide mixtures based on 1-methyl-pyrazol-4-ylcarboxanilides
CN101277938B (zh) 2005-09-16 2012-01-11 先正达参股股份有限公司 酰胺的制备方法
JP5424874B2 (ja) * 2006-06-22 2014-02-26 ビーエーエスエフ ソシエタス・ヨーロピア マロノニトリル化合物
DE102006039909A1 (de) * 2006-08-25 2008-03-13 Bayer Cropscience Ag Verfahren zum Herstellen von 3-Dihalomethyl-pyrazol-4-carbonsäurederivaten
WO2008053043A1 (de) * 2006-11-03 2008-05-08 Basf Se Verfahren zur herstellung von difluormethylpyrazolylcarboxylaten
BRPI0720410A2 (pt) * 2006-12-21 2013-12-31 Basf Se Processos para a preparação de composto, para a preparação de amidas, e, compostos.
KR20090121392A (ko) 2007-03-16 2009-11-25 바스프 에스이 디클로로-플루오로-트리플루오로메틸벤젠의 혼합물을 사용하여 2,6-디클로로-4-(트리플루오로메틸)페닐히드라진을 제조하는 방법
SI2164831T1 (sl) * 2007-06-01 2013-09-30 Basf Se Postopek za proizvodnjo N-substituiranih(3-dihalometil-1-metil- pirazole-4-il) karboksamidov
EA200901652A1 (ru) 2007-06-15 2010-06-30 Басф Се Способ получения дифторметилзамещённых пиразоловых соединений
EP2042482A1 (de) 2007-09-26 2009-04-01 Bayer CropScience AG Verfahren zur Herstellung von 2-Dihalogenacyl-3-amino-acrylsäure-Derivaten
EP2072497A1 (de) 2007-12-21 2009-06-24 Bayer CropScience AG Verfahren zum Herstellen von 2-Fluoracyl-3-amino-acrylsäure-Derivaten
PL2300417T3 (pl) * 2008-05-02 2015-12-31 Basf Se Sposób wytwarzania estrów kwasu 2-(aminometylideno)-4,4-difluoro-3-oksomasłowego
US8586750B2 (en) * 2008-05-02 2013-11-19 Basf Se Method for the production of halogen-substituted 2-(aminomethylidene)-3-oxobutyric acid esters
BRPI0911767A2 (pt) * 2008-05-05 2015-07-28 Basf Se Processo, e, composto.

Also Published As

Publication number Publication date
MX2011000209A (es) 2011-03-01
JP5558467B2 (ja) 2014-07-23
WO2010009990A1 (en) 2010-01-28
AR072580A1 (es) 2010-09-08
BRPI0915801A2 (pt) 2015-08-04
JP2011528683A (ja) 2011-11-24
IL210308A0 (en) 2011-03-31
IL210308A (en) 2013-11-28
CN102099343B (zh) 2014-06-04
EP2307384A1 (de) 2011-04-13
CN102099343A (zh) 2011-06-15
US8344157B2 (en) 2013-01-01
EP2307384B1 (de) 2012-04-25
KR20110031501A (ko) 2011-03-28
US20110118474A1 (en) 2011-05-19

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