ATE58722T1 - Verfahren zur herstellung von n-methylcarbamaten. - Google Patents
Verfahren zur herstellung von n-methylcarbamaten.Info
- Publication number
- ATE58722T1 ATE58722T1 AT85200685T AT85200685T ATE58722T1 AT E58722 T1 ATE58722 T1 AT E58722T1 AT 85200685 T AT85200685 T AT 85200685T AT 85200685 T AT85200685 T AT 85200685T AT E58722 T1 ATE58722 T1 AT E58722T1
- Authority
- AT
- Austria
- Prior art keywords
- methyl isocyanate
- outcoming
- production
- methylurethane
- methylcarbamate
- Prior art date
Links
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- KXDHJXZQYSOELW-UHFFFAOYSA-M Carbamate Chemical compound NC([O-])=O KXDHJXZQYSOELW-UHFFFAOYSA-M 0.000 title 1
- HAMGRBXTJNITHG-UHFFFAOYSA-N methyl isocyanate Chemical compound CN=C=O HAMGRBXTJNITHG-UHFFFAOYSA-N 0.000 abstract 3
- KJCVRFUGPWSIIH-UHFFFAOYSA-N 1-naphthol Chemical compound C1=CC=C2C(O)=CC=CC2=C1 KJCVRFUGPWSIIH-UHFFFAOYSA-N 0.000 abstract 2
- BAVYZALUXZFZLV-UHFFFAOYSA-N Methylamine Chemical compound NC BAVYZALUXZFZLV-UHFFFAOYSA-N 0.000 abstract 2
- QHGZFCAIXRVHID-UHFFFAOYSA-N ethyl n-methyl-n-phenylcarbamate Chemical compound CCOC(=O)N(C)C1=CC=CC=C1 QHGZFCAIXRVHID-UHFFFAOYSA-N 0.000 abstract 2
- UFEJKYYYVXYMMS-UHFFFAOYSA-N methylcarbamic acid Chemical class CNC(O)=O UFEJKYYYVXYMMS-UHFFFAOYSA-N 0.000 abstract 2
- 150000002989 phenols Chemical class 0.000 abstract 2
- 239000011541 reaction mixture Substances 0.000 abstract 2
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 230000005494 condensation Effects 0.000 abstract 1
- 238000009833 condensation Methods 0.000 abstract 1
- 238000010924 continuous production Methods 0.000 abstract 1
- ROORDVPLFPIABK-UHFFFAOYSA-N diphenyl carbonate Chemical compound C=1C=CC=CC=1OC(=O)OC1=CC=CC=C1 ROORDVPLFPIABK-UHFFFAOYSA-N 0.000 abstract 1
- 239000007791 liquid phase Substances 0.000 abstract 1
- 239000003960 organic solvent Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C227/02—Formation of carboxyl groups in compounds containing amino groups, e.g. by oxidation of amino alcohols
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C269/00—Preparation of derivatives of carbamic acid, i.e. compounds containing any of the groups, the nitrogen atom not being part of nitro or nitroso groups
- C07C269/04—Preparation of derivatives of carbamic acid, i.e. compounds containing any of the groups, the nitrogen atom not being part of nitro or nitroso groups from amines with formation of carbamate groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C263/00—Preparation of derivatives of isocyanic acid
- C07C263/04—Preparation of derivatives of isocyanic acid from or via carbamates or carbamoyl halides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C269/00—Preparation of derivatives of carbamic acid, i.e. compounds containing any of the groups, the nitrogen atom not being part of nitro or nitroso groups
- C07C269/02—Preparation of derivatives of carbamic acid, i.e. compounds containing any of the groups, the nitrogen atom not being part of nitro or nitroso groups from isocyanates with formation of carbamate groups
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/582—Recycling of unreacted starting or intermediate materials
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
- Indole Compounds (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| IT19453/85A IT1183332B (it) | 1985-02-08 | 1985-02-08 | Procedimento per la produzione di n-metilcarbammati |
| EP85200685A EP0190466B1 (de) | 1985-02-08 | 1985-05-02 | Verfahren zur Herstellung von N-Methylcarbamaten |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE58722T1 true ATE58722T1 (de) | 1990-12-15 |
Family
ID=11158136
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT85200685T ATE58722T1 (de) | 1985-02-08 | 1985-05-02 | Verfahren zur herstellung von n-methylcarbamaten. |
Country Status (15)
| Country | Link |
|---|---|
| US (1) | US4659845A (de) |
| EP (1) | EP0190466B1 (de) |
| JP (1) | JPH0617356B2 (de) |
| KR (1) | KR870000673B1 (de) |
| CN (1) | CN1004353B (de) |
| AT (1) | ATE58722T1 (de) |
| AU (1) | AU580823B2 (de) |
| BR (1) | BR8502202A (de) |
| CA (1) | CA1249594A (de) |
| DE (1) | DE3580749D1 (de) |
| IL (1) | IL75080A (de) |
| IT (1) | IT1183332B (de) |
| MX (1) | MX168252B (de) |
| SU (1) | SU1433410A3 (de) |
| ZA (1) | ZA859406B (de) |
Families Citing this family (23)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB8714873D0 (en) * | 1987-06-25 | 1987-07-29 | Bp Chemicals Additives | Additives |
| IT1222428B (it) * | 1987-07-31 | 1990-09-05 | Enichem Sintesi | Procedimento perfezionato per la produzione di n alchilcarbammati |
| US5220069A (en) * | 1990-09-20 | 1993-06-15 | Union Carbide Chemicals & Plastics Technology Corporation | Processes for the preparation of carbamates |
| US5284962A (en) * | 1992-10-09 | 1994-02-08 | E. I. Du Pont De Nemours And Company | Multistage process for making methyl carbamates |
| US5613856A (en) * | 1995-07-11 | 1997-03-25 | Hoover; Robert | Ski training system |
| WO2000014057A1 (en) * | 1998-07-30 | 2000-03-16 | Aventis Cropscience S.A. | New process for carbamate production |
| IT1318395B1 (it) * | 2000-03-17 | 2003-08-25 | Enichem Spa | Processo in continuo per la sintesi di uretani aromatici. |
| TWI361179B (en) * | 2006-11-17 | 2012-04-01 | Asahi Kasei Chemicals Corp | A process for producing isocyanates |
| TW200844080A (en) | 2007-01-11 | 2008-11-16 | Asahi Kasei Chemicals Corp | Process for producing isocyanate |
| CN101652344B (zh) | 2007-03-30 | 2014-06-04 | 旭化成化学株式会社 | 使用含有氨基甲酸酯和芳香族羟基化合物的组合物制造异氰酸酯的方法、以及氨基甲酸酯输送用和储藏用组合物 |
| JP5313164B2 (ja) | 2007-11-19 | 2013-10-09 | 旭化成ケミカルズ株式会社 | イソシアネートおよび芳香族ヒドロキシ化合物の製造方法 |
| TWI408120B (zh) * | 2008-05-15 | 2013-09-11 | Asahi Kasei Chemicals Corp | A process for producing isocyanates using diaryl carbonates |
| US8895774B2 (en) | 2008-05-15 | 2014-11-25 | Asahi Kasei Chemicals Corporation | Process for producing isocyanates using diaryl carbonate |
| KR20130127550A (ko) * | 2008-05-15 | 2013-11-22 | 아사히 가세이 케미칼즈 가부시키가이샤 | 이소시아네이트의 제조 방법 |
| US8058469B2 (en) | 2008-11-03 | 2011-11-15 | Sabic Innovative Plastics Ip B.V. | Method for making carbamates, ureas and isocyanates |
| ES2345028B2 (es) | 2009-03-10 | 2011-06-06 | Universidad Politecnica De Valencia | Preparacion de carbamatos en "one pot" con catalizadores solidos. |
| DE102012100127B4 (de) * | 2012-01-10 | 2017-06-29 | Karlsruher Institut für Technologie | Herstellung von Carbamaten über eine basenkatalysierte Lossen- Umlagerung |
| JP5650777B2 (ja) * | 2013-03-11 | 2015-01-07 | 旭化成ケミカルズ株式会社 | 炭酸ジアリールを用いるイソシアネートの製造方法 |
| TWI561504B (en) * | 2015-07-17 | 2016-12-11 | Great Eastern Resins Ind Co Ltd | Two-step and one-pot processes for preparation of aliphatic diisocyanates |
| CN106349110A (zh) * | 2015-07-17 | 2017-01-25 | 大东树脂化学股份有限公司 | 制备脂肪族二异氰酸酯的二步法及一锅化合成法 |
| WO2018212206A1 (ja) | 2017-05-15 | 2018-11-22 | 旭化成株式会社 | イソシアネートの製造方法 |
| CN109384692A (zh) * | 2018-12-12 | 2019-02-26 | 湖南海利常德农药化工有限公司 | 一种残杀威的制备方法 |
| CN116271907B (zh) * | 2023-03-20 | 2025-12-30 | 中国天辰工程有限公司 | 一种六亚甲基二异氰酸酯绿色制备的方法和系统 |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1099084A (en) * | 1966-02-08 | 1968-01-17 | Toa Noyaku Kabushiki Kaisha | Derivatives of phenyl n-methylcarbamates |
| IT1051034B (it) | 1975-12-03 | 1981-04-21 | Snam Progetti | Procedimento per la preparazione di uretani aromatici |
| US4123450A (en) * | 1977-09-22 | 1978-10-31 | Fmc Corporation | Process for preparing alkyl isocyanates |
| DE2756928A1 (de) * | 1977-12-21 | 1979-07-05 | Bayer Ag | Verfahren zur kontinuierlichen herstellung von monoisocyanaten |
| CA1130702A (en) | 1979-06-11 | 1982-08-31 | Terence A. Trevor | Sign routing machine |
| DE80584T1 (de) | 1981-11-25 | 1983-09-15 | Rockwell International Corp., 15219 Pittsburgh, Pa. | Verfahren zur handhabung von zeitungen. |
| DE3215591A1 (de) * | 1982-04-27 | 1983-10-27 | Bayer Ag, 5090 Leverkusen | Verfahren zur kontinuierlichen thermischen spaltung von carbamidsaeureestern |
| IT1164223B (it) * | 1983-05-13 | 1987-04-08 | Anic Spa | Procedimento perfezionato per la produzione di isocianati alchilici |
-
1985
- 1985-02-08 IT IT19453/85A patent/IT1183332B/it active
- 1985-05-02 EP EP85200685A patent/EP0190466B1/de not_active Expired - Lifetime
- 1985-05-02 KR KR1019850002994A patent/KR870000673B1/ko not_active Expired
- 1985-05-02 DE DE8585200685T patent/DE3580749D1/de not_active Expired - Fee Related
- 1985-05-02 AT AT85200685T patent/ATE58722T1/de not_active IP Right Cessation
- 1985-05-02 CA CA000480624A patent/CA1249594A/en not_active Expired
- 1985-05-03 IL IL75080A patent/IL75080A/xx unknown
- 1985-05-07 US US06/731,538 patent/US4659845A/en not_active Expired - Lifetime
- 1985-05-07 BR BR8502202A patent/BR8502202A/pt not_active IP Right Cessation
- 1985-05-07 JP JP60095687A patent/JPH0617356B2/ja not_active Expired - Fee Related
- 1985-12-09 ZA ZA859406A patent/ZA859406B/xx unknown
- 1985-12-13 AU AU51215/85A patent/AU580823B2/en not_active Ceased
- 1985-12-20 SU SU853995137A patent/SU1433410A3/ru active
- 1985-12-28 CN CN85109417.1A patent/CN1004353B/zh not_active Expired
- 1985-12-31 MX MX112485D patent/MX168252B/es unknown
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0617356B2 (ja) | 1994-03-09 |
| IL75080A0 (en) | 1985-09-29 |
| BR8502202A (pt) | 1986-04-15 |
| CN1004353B (zh) | 1989-05-31 |
| CN85109417A (zh) | 1986-12-03 |
| AU5121585A (en) | 1986-08-14 |
| DE3580749D1 (de) | 1991-01-10 |
| SU1433410A3 (ru) | 1988-10-23 |
| ZA859406B (en) | 1986-08-27 |
| CA1249594A (en) | 1989-01-31 |
| KR860006435A (ko) | 1986-09-11 |
| AU580823B2 (en) | 1989-02-02 |
| US4659845A (en) | 1987-04-21 |
| EP0190466A1 (de) | 1986-08-13 |
| EP0190466B1 (de) | 1990-11-28 |
| IT1183332B (it) | 1987-10-22 |
| IT8519453A0 (it) | 1985-02-08 |
| IL75080A (en) | 1989-07-31 |
| JPS61183257A (ja) | 1986-08-15 |
| MX168252B (es) | 1993-05-14 |
| KR870000673B1 (ko) | 1987-04-06 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| UEP | Publication of translation of european patent specification | ||
| REN | Ceased due to non-payment of the annual fee |