BE904217A - Procede de preparation d'une phenyluree substituee. - Google Patents
Procede de preparation d'une phenyluree substituee.Info
- Publication number
- BE904217A BE904217A BE0/216258A BE216258A BE904217A BE 904217 A BE904217 A BE 904217A BE 0/216258 A BE0/216258 A BE 0/216258A BE 216258 A BE216258 A BE 216258A BE 904217 A BE904217 A BE 904217A
- Authority
- BE
- Belgium
- Prior art keywords
- preparation
- substituted phenylurea
- aniline
- substituted
- phenylurea
- Prior art date
Links
- LUBJCRLGQSPQNN-UHFFFAOYSA-N 1-Phenylurea Chemical class NC(=O)NC1=CC=CC=C1 LUBJCRLGQSPQNN-UHFFFAOYSA-N 0.000 title abstract 4
- 238000000034 method Methods 0.000 title abstract 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 2
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N N-phenyl amine Natural products NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 abstract 2
- 125000002490 anilino group Chemical class [H]N(*)C1=C([H])C([H])=C([H])C([H])=C1[H] 0.000 abstract 2
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 abstract 1
- 229910021529 ammonia Inorganic materials 0.000 abstract 1
- 239000004202 carbamide Substances 0.000 abstract 1
- 230000008030 elimination Effects 0.000 abstract 1
- 238000003379 elimination reaction Methods 0.000 abstract 1
- 239000004009 herbicide Substances 0.000 abstract 1
- 239000003960 organic solvent Substances 0.000 abstract 1
- 125000000467 secondary amino group Chemical group [H]N([*:1])[*:2] 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C275/00—Derivatives of urea, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
- C07C275/28—Derivatives of urea, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups having nitrogen atoms of urea groups bound to carbon atoms of six-membered aromatic rings of a carbon skeleton
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C273/00—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
- C07C273/18—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of substituted ureas
- C07C273/1854—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of substituted ureas by reactions not involving the formation of the N-C(O)-N- moiety
- C07C273/1863—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of substituted ureas by reactions not involving the formation of the N-C(O)-N- moiety from urea
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Procédé de préparation d'une phénylurée substituée dans lequel on fait réagir simultanément une aniline convenablement substituée, de l'urée en excès dans un rapport molaire d'au moins 1,1 par rapport à l'aniline, et une amine secondaire, dans un solvant organique non hydroxylé, à une température de 130 à 250 degrés, avec élimination de l'amoniac au fur et à mesure de sa formation. Les phénylurées obtenues sont utilisées comme herbicides.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR8502079A FR2577221B1 (fr) | 1985-02-11 | 1985-02-11 | Procede de preparation d'une phenyluree substituee |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| BE904217A true BE904217A (fr) | 1986-08-11 |
Family
ID=9316250
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BE0/216258A BE904217A (fr) | 1985-02-11 | 1986-02-11 | Procede de preparation d'une phenyluree substituee. |
Country Status (27)
| Country | Link |
|---|---|
| US (1) | US4814499A (fr) |
| JP (1) | JPS61183258A (fr) |
| KR (1) | KR940003067B1 (fr) |
| CN (1) | CN1009274B (fr) |
| AT (1) | AT395848B (fr) |
| AU (1) | AU577178B2 (fr) |
| BE (1) | BE904217A (fr) |
| BR (1) | BR8600539A (fr) |
| CH (1) | CH666681A5 (fr) |
| DD (1) | DD242803A5 (fr) |
| DE (1) | DE3602657A1 (fr) |
| DK (1) | DK169030B1 (fr) |
| ES (1) | ES8702347A1 (fr) |
| FI (1) | FI84597C (fr) |
| FR (1) | FR2577221B1 (fr) |
| GB (1) | GB2170808B (fr) |
| HU (1) | HU199111B (fr) |
| IE (1) | IE58978B1 (fr) |
| IN (1) | IN166514B (fr) |
| IT (1) | IT1190483B (fr) |
| LU (1) | LU86296A1 (fr) |
| NL (1) | NL8600189A (fr) |
| NZ (1) | NZ215067A (fr) |
| PH (1) | PH20993A (fr) |
| PL (1) | PL257891A1 (fr) |
| SE (1) | SE465927B (fr) |
| ZA (1) | ZA86931B (fr) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE59005183D1 (de) * | 1989-11-10 | 1994-05-05 | Agrolinz Agrarchemikalien | Verfahren zur Herstellung reiner, unsymmetrisch disubstituierter Harnstoffe. |
| AT397384B (de) * | 1991-08-16 | 1994-03-25 | Chemie Linz Gmbh | Verfahren zur herstellung reiner n,n'-unsymmetrisch substituierter phenylharnstoffe |
| CN1045002C (zh) * | 1995-03-28 | 1999-09-08 | 天津大学 | 2,6-二氯苯胺的制备方法 |
| CN106008276B (zh) * | 2016-05-20 | 2018-07-06 | 湖北出入境检验检疫局检验检疫技术中心 | 苯脲类除草剂或氘代标记的苯脲类除草剂的合成方法 |
| CN110938019B (zh) * | 2019-12-10 | 2022-06-24 | 江苏快达农化股份有限公司 | 连续化合成异丙隆方法 |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2878284A (en) * | 1945-06-09 | 1959-03-17 | Du Pont | Process for preparing symmetrical hexachlorodiphenyl urea |
| US2673877A (en) * | 1951-10-26 | 1954-03-30 | Du Pont | Preparation of chlorphenyldimethyl-ureas |
| US2729677A (en) * | 1954-03-16 | 1956-01-03 | Allied Chem & Dye Corp | Process for the manufacture of substituted ureas |
| US2768971A (en) * | 1954-05-26 | 1956-10-30 | Ici Ltd | Preparation of alkyl-aryl-ureas |
| DE1064051B (de) * | 1958-04-09 | 1959-08-27 | Basf Ag | Verfahren zur Herstellung von substituierten Harnstoffen |
| NL255093A (fr) * | 1959-08-21 | |||
| CA1201725A (fr) * | 1979-12-06 | 1986-03-11 | Terence Gilkerson | Derive de l'uree, sa preparation, herbicide qui le renferme, et methode de repression des mauvaises herbes |
| DE3133794A1 (de) * | 1980-01-25 | 1982-04-01 | Daroczi I | Verfahren zur Herstellung von N'-(mono-oder disubstituierten) N-Aryl-Harnstoff-Derivaten |
| CH652391A5 (de) * | 1982-01-15 | 1985-11-15 | Sandoz Ag | Harnstoff-derivate. |
| IT1152510B (it) * | 1982-08-25 | 1987-01-07 | Anic Spa | Procedimento per la produzione di uree asimmetriche sostituite |
-
1985
- 1985-02-11 FR FR8502079A patent/FR2577221B1/fr not_active Expired
-
1986
- 1986-01-28 IN IN79/DEL/86A patent/IN166514B/en unknown
- 1986-01-28 NL NL8600189A patent/NL8600189A/nl not_active Application Discontinuation
- 1986-01-29 DE DE19863602657 patent/DE3602657A1/de not_active Ceased
- 1986-01-30 PH PH33351A patent/PH20993A/en unknown
- 1986-02-06 CN CN86101095A patent/CN1009274B/zh not_active Expired
- 1986-02-06 LU LU86296A patent/LU86296A1/fr unknown
- 1986-02-07 ZA ZA86931A patent/ZA86931B/xx unknown
- 1986-02-07 BR BR8600539A patent/BR8600539A/pt not_active IP Right Cessation
- 1986-02-07 NZ NZ215067A patent/NZ215067A/xx unknown
- 1986-02-07 JP JP61025684A patent/JPS61183258A/ja active Pending
- 1986-02-07 AU AU53299/86A patent/AU577178B2/en not_active Ceased
- 1986-02-07 US US06/827,782 patent/US4814499A/en not_active Expired - Fee Related
- 1986-02-07 IE IE35286A patent/IE58978B1/en not_active IP Right Cessation
- 1986-02-07 DD DD86286892A patent/DD242803A5/de unknown
- 1986-02-07 IT IT47634/86A patent/IT1190483B/it active
- 1986-02-10 DK DK063186A patent/DK169030B1/da not_active IP Right Cessation
- 1986-02-10 PL PL25789186A patent/PL257891A1/xx unknown
- 1986-02-10 GB GB08603223A patent/GB2170808B/en not_active Expired
- 1986-02-10 ES ES551790A patent/ES8702347A1/es not_active Expired
- 1986-02-10 AT AT0032586A patent/AT395848B/de not_active IP Right Cessation
- 1986-02-10 KR KR1019860000901A patent/KR940003067B1/ko not_active Expired - Fee Related
- 1986-02-10 FI FI860597A patent/FI84597C/fi not_active IP Right Cessation
- 1986-02-10 HU HU86542A patent/HU199111B/hu not_active IP Right Cessation
- 1986-02-11 CH CH545/86A patent/CH666681A5/fr not_active IP Right Cessation
- 1986-02-11 SE SE8600596A patent/SE465927B/sv not_active IP Right Cessation
- 1986-02-11 BE BE0/216258A patent/BE904217A/fr not_active IP Right Cessation
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| RE | Patent lapsed |
Owner name: ROHNE-POULENC AGROCHIMIE Effective date: 19950228 |