BR0109677A - Processo para a preparação de um catalisador de dmc, catalisador, e, processo para a polimerização de óxidos de alquileno - Google Patents
Processo para a preparação de um catalisador de dmc, catalisador, e, processo para a polimerização de óxidos de alquilenoInfo
- Publication number
- BR0109677A BR0109677A BR0109677-0A BR0109677A BR0109677A BR 0109677 A BR0109677 A BR 0109677A BR 0109677 A BR0109677 A BR 0109677A BR 0109677 A BR0109677 A BR 0109677A
- Authority
- BR
- Brazil
- Prior art keywords
- dmc
- catalyst
- aqueous
- polymerization
- dmc catalyst
- Prior art date
Links
- 239000003054 catalyst Substances 0.000 title abstract 5
- 238000000034 method Methods 0.000 title abstract 4
- 125000002947 alkylene group Chemical group 0.000 title abstract 2
- 238000006116 polymerization reaction Methods 0.000 title abstract 2
- 239000007864 aqueous solution Substances 0.000 abstract 3
- 239000002184 metal Substances 0.000 abstract 3
- 239000012736 aqueous medium Substances 0.000 abstract 2
- 239000006185 dispersion Substances 0.000 abstract 2
- 239000007788 liquid Substances 0.000 abstract 2
- 150000003839 salts Chemical class 0.000 abstract 2
- 239000007787 solid Substances 0.000 abstract 2
- 239000004721 Polyphenylene oxide Substances 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 239000008139 complexing agent Substances 0.000 abstract 1
- 150000002825 nitriles Chemical class 0.000 abstract 1
- 229920000570 polyether Polymers 0.000 abstract 1
- 229920005862 polyol Polymers 0.000 abstract 1
- 150000003077 polyols Chemical class 0.000 abstract 1
- 239000000243 solution Substances 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
- B01J27/24—Nitrogen compounds
- B01J27/26—Cyanides
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
- C08G65/2645—Metals or compounds thereof, e.g. salts
- C08G65/2663—Metal cyanide catalysts, i.e. DMC's
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Organic Chemistry (AREA)
- Toxicology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- General Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Polyethers (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
Abstract
"PROCESSO PARA A PREPARAçãO DE UM CATALISADOR DE DMC, CATALISADOR, E, PROCESSO PARA A POLIMERIZAçãO DE óXIDOS DE ALQUILENO". Processo para a preparação de um catalisador de DMC útil na polimerização de óxidos de alquileno em poliéter polióis, sendo que o processo compreende as etapas de: (a) combinar uma solução aquosa de um sal de metal com uma solução aquosa de um sal de cianeto de metal e reagir estas soluções, no qual pelo menos parte desta reação ocorre na presença de um agente complexante orgânico, formando deste modo uma dispersão de um complexo de DMC sólido em um meio aquoso; (b) combinar a dispersão obtida na etapa (a) com um líquido, que é essencialmente insolúvel em água e que é capaz de extrair do meio aquoso o complexo de DMC sólido formado na etapa (a), e permitir que um sistema de duas fases seja formado consistindo de uma primeira camada aquosa e uma camada contendo o complexo de DMC e o líquido adicionado; (c) remover a primeira camada aquosa; e (d) recuperar o catalisador de DMC da camada contendo o catalisador de DMC.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP00201170 | 2000-03-30 | ||
| EP00201170.8 | 2000-03-30 | ||
| PCT/EP2001/003498 WO2001072418A1 (en) | 2000-03-30 | 2001-03-27 | Dmc complex catalyst and process for its preparation |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| BR0109677A true BR0109677A (pt) | 2003-02-04 |
| BR0109677B1 BR0109677B1 (pt) | 2011-08-09 |
Family
ID=8171283
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BRPI0109677-0A BR0109677B1 (pt) | 2000-03-30 | 2001-03-27 | processo para a preparação de um catalisador de dmc, e, catalisador de dmc. |
Country Status (15)
| Country | Link |
|---|---|
| US (1) | US6699961B2 (pt) |
| EP (1) | EP1276562B1 (pt) |
| JP (1) | JP2003528213A (pt) |
| KR (1) | KR100788218B1 (pt) |
| CN (1) | CN1177645C (pt) |
| AT (1) | ATE249880T1 (pt) |
| AU (1) | AU2001246512A1 (pt) |
| BR (1) | BR0109677B1 (pt) |
| CA (1) | CA2404652A1 (pt) |
| DE (1) | DE60100807T2 (pt) |
| ES (1) | ES2202286T3 (pt) |
| PL (1) | PL358016A1 (pt) |
| RU (1) | RU2254918C2 (pt) |
| TW (1) | TW550114B (pt) |
| WO (1) | WO2001072418A1 (pt) |
Families Citing this family (40)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6436867B1 (en) | 2000-08-01 | 2002-08-20 | Basf Corporation | One-step synthesis of double metal cyanides |
| US6596842B2 (en) | 2001-07-16 | 2003-07-22 | Shell Oil Company | Polymerizing alkylene oxide with sound or radiation treated DMC |
| JP2005509707A (ja) * | 2001-11-19 | 2005-04-14 | シエル・インターナシヨネイル・リサーチ・マーチヤツピイ・ベー・ウイ | 有機化合物のアルコキシル化方法 |
| DE10210596A1 (de) * | 2002-03-11 | 2003-09-25 | Basf Ag | Polyether und deren Verwendung als Trägeröle |
| US6716788B2 (en) | 2002-06-14 | 2004-04-06 | Shell Oil Company | Preparation of a double metal cyanide catalyst |
| US6977236B2 (en) | 2002-06-14 | 2005-12-20 | Shell Oil Company | Preparation of a double metal cyanide catalyst |
| US7378559B2 (en) * | 2003-03-07 | 2008-05-27 | Dow Global Technologies Inc. | Continuous process and system of producing polyether polyols |
| US20050014979A1 (en) * | 2003-07-08 | 2005-01-20 | Eleveld Michiel Barend | Preparation of an alkoxylate composition using a double metal cyanide catalyst |
| US6921737B1 (en) * | 2004-05-26 | 2005-07-26 | Basf Corporation | Method of synthesizing a double metal cyanide catalyst |
| US7300993B2 (en) | 2004-06-03 | 2007-11-27 | Shell Oil Company | Process for the preparation of polyether polyols |
| US20060229375A1 (en) * | 2005-04-06 | 2006-10-12 | Yu-Ling Hsiao | Polyurethane foams made with alkoxylated vegetable oil hydroxylate |
| AR069725A1 (es) * | 2007-06-27 | 2010-02-17 | Shell Int Research | Proceso para preparar una composicion de alcoxilato y una composicion alcoxilada |
| KR101394283B1 (ko) * | 2007-09-27 | 2014-05-13 | 삼성전자주식회사 | 블루투스 모듈을 구비한 휴대 단말기 및 그의 블루투스통신 방법 |
| CN103384692A (zh) | 2011-02-24 | 2013-11-06 | 国际壳牌研究有限公司 | 制备聚醚多元醇的方法和反应器系统 |
| KR101404702B1 (ko) | 2011-03-08 | 2014-06-17 | 에스케이이노베이션 주식회사 | 에테르 결합 단위체를 함유한 이산화탄소/에폭사이드 공중합체의 제조 방법 |
| BR112013025054B1 (pt) * | 2011-03-31 | 2020-03-17 | Dow Global Technologies Llc | Método para produzir um poliéter poliol de cadeia curta |
| GB201515350D0 (en) | 2015-08-28 | 2015-10-14 | Econic Technologies Ltd | Method for preparing polyols |
| GB201703324D0 (en) | 2017-03-01 | 2017-04-12 | Econic Tech Ltd | Method for preparing polyether carbonates |
| PL3622003T3 (pl) * | 2017-05-10 | 2025-02-24 | Dow Global Technologies Llc | Proces polimeryzacji polieterowej |
| GB201717459D0 (en) | 2017-10-24 | 2017-12-06 | Econic Tech Limited | Methods for forming polycarbonate ether polyols and high molecular weight polyether carbonates |
| GB201717441D0 (en) | 2017-10-24 | 2017-12-06 | Econic Tech Ltd | A polymerisation process |
| CN112004862A (zh) | 2018-04-25 | 2020-11-27 | 汉高股份有限及两合公司 | 用于制备羟基官能化聚醚-聚硅氧烷嵌段共聚物的方法 |
| CN112368317B (zh) | 2018-06-19 | 2024-04-02 | 汉高股份有限及两合公司 | 高活性双金属氰化物化合物 |
| GB201814526D0 (en) | 2018-09-06 | 2018-10-24 | Econic Tech Ltd | Methods for forming polycarbonate ether polyols and high molecular weight polyether carbonates |
| ES2977551T3 (es) | 2018-12-06 | 2024-08-26 | Henkel Ag & Co Kgaa | Composición curable que comprende copolímeros de polisiloxano polialquilenglicol en cepillo |
| ES2985743T3 (es) | 2018-12-06 | 2024-11-07 | Henkel Ag & Co Kgaa | Preparación de copolímeros en cepillo de polisiloxano-polialquilenglicol |
| GB201906214D0 (en) | 2019-05-02 | 2019-06-19 | Econic Tech Ltd | A polyol block copolymer, compositions and processes therefor |
| GB201906210D0 (en) | 2019-05-02 | 2019-06-19 | Econic Tech Limited | A polyol block copolymer, compositions and processes therefor |
| GB202003002D0 (en) | 2020-03-02 | 2020-04-15 | Crane Ltd | Method of preparation of a polyol block copolymer |
| GB202003003D0 (en) | 2020-03-02 | 2020-04-15 | Econic Tech Ltd | A polyol block copolymer |
| ES3052737T3 (en) | 2020-07-01 | 2026-01-13 | Henkel Ag & Co Kgaa | Bi-functionalized polysiloxane brush copolymers |
| GB202017531D0 (en) | 2020-11-05 | 2020-12-23 | Econic Tech Limited | (poly)ol block copolymer |
| EP4384316A1 (en) | 2021-08-11 | 2024-06-19 | Econic Technologies Ltd | Method for preparing surfactants by copolymerisation of epoxides and co2 using a mixture of a macrocyclic bimetal catalyst and a double metal cyanide catalyst |
| GB202115335D0 (en) | 2021-10-25 | 2021-12-08 | Econic Tech Ltd | Surface-active agent |
| CN120457154A (zh) * | 2022-12-22 | 2025-08-08 | Gs加德士 | 双金属氰化物催化剂及其制备方法 |
| GB2626546A (en) | 2023-01-25 | 2024-07-31 | Econic Tech Ltd | Surface-active agent |
| GB2626989A (en) | 2023-02-10 | 2024-08-14 | Econic Tech Ltd | Surface-active agent |
| GB2629367A (en) | 2023-04-25 | 2024-10-30 | Econic Tech Ltd | Surface-active agent |
| EP4702078A1 (en) | 2023-04-25 | 2026-03-04 | Unilever IP Holdings B.V. | Compositions |
| EP4480992A1 (en) | 2023-06-19 | 2024-12-25 | Henkel AG & Co. KGaA | Polyether-polysiloxane gradient copolymers |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3427335A (en) * | 1963-02-14 | 1969-02-11 | Gen Tire & Rubber Co | Double metal cyanides complexed with an acyclic aliphatic saturated monoether,an ester and a cyclic ether and methods for making the same |
| US3829505A (en) * | 1970-02-24 | 1974-08-13 | Gen Tire & Rubber Co | Polyethers and method for making the same |
| AU551979B2 (en) * | 1982-03-31 | 1986-05-15 | Shell Internationale Research Maatschappij B.V. | Epoxy polymerisation catalysts |
| JPH04284850A (ja) * | 1991-03-13 | 1992-10-09 | Asahi Glass Co Ltd | 複合金属シアン化物錯体触媒の製造方法 |
| US5158922A (en) * | 1992-02-04 | 1992-10-27 | Arco Chemical Technology, L.P. | Process for preparing metal cyanide complex catalyst |
| US5470813A (en) | 1993-11-23 | 1995-11-28 | Arco Chemical Technology, L.P. | Double metal cyanide complex catalysts |
| JP3517949B2 (ja) * | 1994-05-16 | 2004-04-12 | 旭硝子株式会社 | 複合金属シアン化物錯体触媒の製造方法 |
| US5482908A (en) | 1994-09-08 | 1996-01-09 | Arco Chemical Technology, L.P. | Highly active double metal cyanide catalysts |
| US5627122A (en) | 1995-07-24 | 1997-05-06 | Arco Chemical Technology, L.P. | Highly active double metal cyanide complex catalysts |
| US5627120A (en) | 1996-04-19 | 1997-05-06 | Arco Chemical Technology, L.P. | Highly active double metal cyanide catalysts |
| JP3620152B2 (ja) * | 1996-06-27 | 2005-02-16 | 旭硝子株式会社 | ポリエーテル製造用複合金属シアン化物錯体触媒およびその製造方法 |
| DE19654340A1 (de) | 1996-12-24 | 1998-08-06 | Huels Chemische Werke Ag | Verfahren zur Herstellung von höheren Oxo-Alkoholen |
-
2001
- 2001-03-27 EP EP01919398A patent/EP1276562B1/en not_active Expired - Lifetime
- 2001-03-27 WO PCT/EP2001/003498 patent/WO2001072418A1/en not_active Ceased
- 2001-03-27 AT AT01919398T patent/ATE249880T1/de not_active IP Right Cessation
- 2001-03-27 RU RU2002129013/04A patent/RU2254918C2/ru active
- 2001-03-27 JP JP2001570372A patent/JP2003528213A/ja active Pending
- 2001-03-27 US US10/239,614 patent/US6699961B2/en not_active Expired - Lifetime
- 2001-03-27 CA CA002404652A patent/CA2404652A1/en not_active Abandoned
- 2001-03-27 CN CNB018084419A patent/CN1177645C/zh not_active Expired - Lifetime
- 2001-03-27 KR KR1020027013072A patent/KR100788218B1/ko not_active Expired - Lifetime
- 2001-03-27 DE DE60100807T patent/DE60100807T2/de not_active Expired - Lifetime
- 2001-03-27 ES ES01919398T patent/ES2202286T3/es not_active Expired - Lifetime
- 2001-03-27 AU AU2001246512A patent/AU2001246512A1/en not_active Abandoned
- 2001-03-27 BR BRPI0109677-0A patent/BR0109677B1/pt not_active IP Right Cessation
- 2001-03-27 PL PL01358016A patent/PL358016A1/xx unknown
- 2001-05-07 TW TW090110849A patent/TW550114B/zh not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| PL358016A1 (en) | 2004-08-09 |
| CN1426325A (zh) | 2003-06-25 |
| US20030069389A1 (en) | 2003-04-10 |
| BR0109677B1 (pt) | 2011-08-09 |
| ATE249880T1 (de) | 2003-10-15 |
| EP1276562B1 (en) | 2003-09-17 |
| US6699961B2 (en) | 2004-03-02 |
| KR100788218B1 (ko) | 2007-12-26 |
| TW550114B (en) | 2003-09-01 |
| ES2202286T3 (es) | 2004-04-01 |
| DE60100807T2 (de) | 2004-08-05 |
| JP2003528213A (ja) | 2003-09-24 |
| AU2001246512A1 (en) | 2001-10-08 |
| CN1177645C (zh) | 2004-12-01 |
| WO2001072418A1 (en) | 2001-10-04 |
| RU2254918C2 (ru) | 2005-06-27 |
| CA2404652A1 (en) | 2001-10-04 |
| DE60100807D1 (de) | 2003-10-23 |
| RU2002129013A (ru) | 2004-02-27 |
| EP1276562A1 (en) | 2003-01-22 |
| KR20030003245A (ko) | 2003-01-09 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| B06A | Patent application procedure suspended [chapter 6.1 patent gazette] | ||
| B09A | Decision: intention to grant [chapter 9.1 patent gazette] | ||
| B16A | Patent or certificate of addition of invention granted [chapter 16.1 patent gazette] |
Free format text: PRAZO DE VALIDADE: 10 (DEZ) ANOS CONTADOS A PARTIR DE 09/08/2011, OBSERVADAS AS CONDICOES LEGAIS. |
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| B21A | Patent or certificate of addition expired [chapter 21.1 patent gazette] |
Free format text: PATENTE EXTINTA EM 09.08.2021 |