BRPI0416164A - processo para remover compostos de mercúrio de uma corrente contendo glicol e/ou álcool e processo para remover água, compostos de enxofre e/ou dióxido de carbono de uma corrente contendo hidrocarboneto - Google Patents

processo para remover compostos de mercúrio de uma corrente contendo glicol e/ou álcool e processo para remover água, compostos de enxofre e/ou dióxido de carbono de uma corrente contendo hidrocarboneto

Info

Publication number
BRPI0416164A
BRPI0416164A BRPI0416164-5A BRPI0416164A BRPI0416164A BR PI0416164 A BRPI0416164 A BR PI0416164A BR PI0416164 A BRPI0416164 A BR PI0416164A BR PI0416164 A BRPI0416164 A BR PI0416164A
Authority
BR
Brazil
Prior art keywords
glycol
containing stream
compounds
carbon dioxide
stream
Prior art date
Application number
BRPI0416164-5A
Other languages
English (en)
Inventor
Peter John Herbert Carnell
Original Assignee
Johnson Matthey Plc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from GB0414160A external-priority patent/GB0414160D0/en
Application filed by Johnson Matthey Plc filed Critical Johnson Matthey Plc
Publication of BRPI0416164A publication Critical patent/BRPI0416164A/pt
Publication of BRPI0416164B1 publication Critical patent/BRPI0416164B1/pt

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/0203—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of metals not provided for in B01J20/04
    • B01J20/0225—Compounds of Fe, Ru, Os, Co, Rh, Ir, Ni, Pd, Pt
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/0203—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of metals not provided for in B01J20/04
    • B01J20/0225—Compounds of Fe, Ru, Os, Co, Rh, Ir, Ni, Pd, Pt
    • B01J20/0229—Compounds of Fe
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/0203—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of metals not provided for in B01J20/04
    • B01J20/0233—Compounds of Cu, Ag, Au
    • B01J20/0237—Compounds of Cu
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/0203—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of metals not provided for in B01J20/04
    • B01J20/024—Compounds of Zn, Cd, Hg
    • B01J20/0244—Compounds of Zn
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/0203—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of metals not provided for in B01J20/04
    • B01J20/0274—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of metals not provided for in B01J20/04 characterised by the type of anion
    • B01J20/0277—Carbonates of compounds other than those provided for in B01J20/043
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/0203—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of metals not provided for in B01J20/04
    • B01J20/0274—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of metals not provided for in B01J20/04 characterised by the type of anion
    • B01J20/0285—Sulfides of compounds other than those provided for in B01J20/045
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/06—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising oxides or hydroxides of metals not provided for in group B01J20/04
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/06—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising oxides or hydroxides of metals not provided for in group B01J20/04
    • B01J20/08—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising oxides or hydroxides of metals not provided for in group B01J20/04 comprising aluminium oxide or hydroxide; comprising bauxite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/20—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising free carbon; comprising carbon obtained by carbonising processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/2803—Sorbents comprising a binder, e.g. for forming aggregated, agglomerated or granulated products
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3202—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the carrier, support or substrate used for impregnation or coating
    • B01J20/3204—Inorganic carriers, supports or substrates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3231—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the coating or impregnating layer
    • B01J20/3234—Inorganic material layers
    • B01J20/3236—Inorganic material layers containing metal, other than zeolites, e.g. oxides, hydroxides, sulphides or salts
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/11—Purification; Separation; Use of additives by absorption, i.e. purification or separation of gaseous hydrocarbons with the aid of liquids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2220/00—Aspects relating to sorbent materials
    • B01J2220/40—Aspects relating to the composition of sorbent or filter aid materials
    • B01J2220/42—Materials comprising a mixture of inorganic materials
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2220/00—Aspects relating to sorbent materials
    • B01J2220/50—Aspects relating to the use of sorbent or filter aid materials
    • B01J2220/56—Use in the form of a bed

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Water Supply & Treatment (AREA)
  • Treating Waste Gases (AREA)
  • Gas Separation By Absorption (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
  • Removal Of Specific Substances (AREA)

Abstract

"PROCESSO PARA REMOVER COMPOSTOS DE MERCúRIO DE UMA CORRENTE CONTENDO GLICOL E/OU áLCOOL E PROCESSO PARA REMOVER áGUA, COMPOSTOS DE ENXOFRE E/OU DIóXIDO DE CARBONO DE UMA CORRENTE CONTENDO HIDROCARBONETO". A invenção é um processo para remover compostos de mercúrio de uma corrente absorvente líquida contendo glicol ou álcool a qual contem compostos de mercúrio, especialmente uma corrente de glicol a qual tem sido usada em uma planta de secagem de glicol para remover água de corrente de gás natural. O processo compreende contactar a corrente absorvente líquida carregada com mercúrio com um leito de partículas absorventes sólidas, compreendendo um metal sulfetado, opcionalmente suportado em material de suporte, ou enxofre suportado em carbono.
BRPI0416164-5B1A 2003-11-05 2004-10-29 Processo para remover compostos de mercúrio de uma corrente contendo glicol e/ou álcool e processo para remover água, compostos de enxofre e/ou dióxido de carbono de uma corrente contendo hidrocarboneto BRPI0416164B1 (pt)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
GB0325769.8 2003-11-05
GBGB0325769.8A GB0325769D0 (en) 2003-11-05 2003-11-05 Removal of mercury compounds from glycol
GB0414160A GB0414160D0 (en) 2004-06-24 2004-06-24 Removal of mercury compounds from glycol
GB0414160.2 2004-06-24
PCT/GB2004/004593 WO2005047438A1 (en) 2003-11-05 2004-10-29 Removal of mercury compounds from glycol

Publications (2)

Publication Number Publication Date
BRPI0416164A true BRPI0416164A (pt) 2007-01-23
BRPI0416164B1 BRPI0416164B1 (pt) 2015-03-03

Family

ID=34593728

Family Applications (1)

Application Number Title Priority Date Filing Date
BRPI0416164-5B1A BRPI0416164B1 (pt) 2003-11-05 2004-10-29 Processo para remover compostos de mercúrio de uma corrente contendo glicol e/ou álcool e processo para remover água, compostos de enxofre e/ou dióxido de carbono de uma corrente contendo hidrocarboneto

Country Status (8)

Country Link
US (1) US7435338B2 (pt)
EP (1) EP1680490A1 (pt)
AU (1) AU2004289867B2 (pt)
BR (1) BRPI0416164B1 (pt)
EG (1) EG24723A (pt)
GB (1) GB0325769D0 (pt)
NO (1) NO332292B1 (pt)
WO (1) WO2005047438A1 (pt)

Families Citing this family (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB0616343D0 (en) 2006-08-17 2006-09-27 Johnson Matthey Plc Mercury removal
GB0802828D0 (en) * 2008-02-15 2008-03-26 Johnson Matthey Plc Absorbents
WO2010061212A1 (en) * 2008-11-25 2010-06-03 Johnson Matthey Plc Reduced copper sulphide sorbent for removing heavy metals
US8043510B2 (en) * 2009-10-29 2011-10-25 Conocophillips Company Mercury removal with sorbents magnetically separable from treated fluids
EP2508243A1 (en) * 2011-04-06 2012-10-10 Shell Internationale Research Maatschappij B.V. Method and apparatus for removing mercury from waste water from hydrocarbon well stream
US8876952B2 (en) 2012-02-06 2014-11-04 Uop Llc Method of removing mercury from a fluid stream using high capacity copper adsorbents
GB201204650D0 (en) 2012-03-16 2012-05-02 Johnson Matthey Plc A method for producing a sulphided copper sorbent
AU2013269181B2 (en) * 2012-05-30 2016-03-24 Grant Prideco, Inc. System and method for removal of heavy metal ions from a rich hydrate inhibitor stream
US9724637B2 (en) 2012-06-22 2017-08-08 Shell Oil Company Method and apparatus for circulating a glycol stream, and method of producing a natural gas product stream
EP3476460B1 (en) * 2012-09-07 2022-11-02 Chevron U.S.A. Inc. Method for removing mercury from natural gas
WO2017027550A1 (en) 2015-08-12 2017-02-16 Uop Llc Composition and process for removing chlorides from a gaseous stream
US10041014B2 (en) * 2016-06-10 2018-08-07 Chevron U.S.A. Inc. Process, method and system for removal of mercury in a gas dehydration process
WO2017214531A1 (en) * 2016-06-10 2017-12-14 Chevron U.S.A. Inc. Hydrophobic adsorbents and mercury removal processes therewith
CN110523219B (zh) * 2019-09-10 2020-08-28 艾凡佳德(上海)环保科技有限公司 一种含乙二醇的工业尾气的处理系统及其使用方法
CN111394144A (zh) * 2020-03-13 2020-07-10 山西新华化工有限责任公司 一种脱汞剂及制备方法
CN111762855A (zh) * 2020-06-16 2020-10-13 唐山周行科技发展有限公司 一种含汞废水脱汞装置及方法
FR3130635A1 (fr) 2021-12-20 2023-06-23 IFP Energies Nouvelles Procede de captation de metaux lourds par co-alimentation d’un flux sulfurant
FR3130636A1 (fr) 2021-12-20 2023-06-23 IFP Energies Nouvelles Procede de rejuvenation de masses de captation de metaux lourds
CN117443077B (zh) * 2023-10-27 2024-03-15 临沂广辰化工有限公司 一种菊酸乙酯提纯加工装置及方法

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2529802A1 (fr) * 1982-07-06 1984-01-13 Pro Catalyse Masses d'absorption pour l'elimination du mercure
CA1325993C (en) * 1988-05-16 1994-01-11 Mitsui Chemicals, Incorporated Method of removing mercury from hydrocarbon oils
JP2578514B2 (ja) * 1989-03-03 1997-02-05 三井石油化学工業株式会社 液体炭化水素化合物中の水銀の除去方法
US5080799A (en) * 1990-05-23 1992-01-14 Mobil Oil Corporation Hg removal from wastewater by regenerative adsorption
GB9906717D0 (en) 1999-03-23 1999-05-19 Norske Stats Oljeselskap Method and apparatus for drying of natural gas
US6475451B1 (en) * 2000-08-23 2002-11-05 Gas Technology Institute Mercury removal from gaseous process streams
US6558642B2 (en) * 2001-03-29 2003-05-06 Merck & Co., Inc. Method of adsorbing metals and organic compounds from vaporous streams
US20060205591A1 (en) * 2005-03-11 2006-09-14 Do-Hee Lee Adsorbent for removing mercury using sulfided iron compounds containing oxygen and method of producing same

Also Published As

Publication number Publication date
BRPI0416164B1 (pt) 2015-03-03
US20070134143A1 (en) 2007-06-14
WO2005047438A1 (en) 2005-05-26
NO20061393L (no) 2006-06-02
GB0325769D0 (en) 2003-12-10
US7435338B2 (en) 2008-10-14
EG24723A (en) 2010-06-07
AU2004289867B2 (en) 2009-04-23
EP1680490A1 (en) 2006-07-19
AU2004289867A1 (en) 2005-05-26
NO332292B1 (no) 2012-08-20

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B25G Requested change of headquarter approved

Owner name: JOHNSON MATTHEY PLC (GB)

Free format text: SEDE ALTERADA CONFORME SOLICITADO NA PETICAO NO 020080116639/RJ DE 04/09/2008.

B06A Patent application procedure suspended [chapter 6.1 patent gazette]
B09A Decision: intention to grant [chapter 9.1 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 10 (DEZ) ANOS CONTADOS A PARTIR DE 03/03/2015, OBSERVADAS AS CONDICOES LEGAIS.

B21F Lapse acc. art. 78, item iv - on non-payment of the annual fees in time
B24J Lapse because of non-payment of annual fees (definitively: art 78 iv lpi, resolution 113/2013 art. 12)