NO332292B1 - Fremgangsmate for fjerning av kvikksolvforbindelser fra en glykol- og/eller alkoholholdig strom og fremgangsmate for a fjerne vann, svovelforbindelse og/eller karbondioksid fra en hydrokarbonholdig strom - Google Patents

Fremgangsmate for fjerning av kvikksolvforbindelser fra en glykol- og/eller alkoholholdig strom og fremgangsmate for a fjerne vann, svovelforbindelse og/eller karbondioksid fra en hydrokarbonholdig strom Download PDF

Info

Publication number: NO332292B1
Authority: NO; Norway
Prior art keywords: stream; glycol; mercury; absorbent; liquid absorbent
Prior art date: 2003-11-05

Application number

NO20061393A

Other languages

English (en)

Norwegian (no)

Other versions

NO20061393L (no

Inventor

Peter John Herbert Carnell

Original Assignee

Johnson Matthey Plc

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2003-11-05

Filing date

2006-03-27

Publication date

2012-08-20

2004-06-24 Priority claimed from GB0414160A external-priority patent/GB0414160D0/en

2006-03-27 Application filed by Johnson Matthey Plc filed Critical Johnson Matthey Plc

2006-06-02 Publication of NO20061393L publication Critical patent/NO20061393L/no

2012-08-20 Publication of NO332292B1 publication Critical patent/NO332292B1/no

Links

LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 title claims abstract description 91
WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 title claims abstract description 45
238000000034 method Methods 0.000 title claims abstract description 30
150000002731 mercury compounds Chemical class 0.000 title claims abstract description 23
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 22
230000001476 alcoholic effect Effects 0.000 title claims abstract 4
150000003464 sulfur compounds Chemical class 0.000 title claims description 18
CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 title claims description 12
229910002092 carbon dioxide Inorganic materials 0.000 title claims description 6
239000001569 carbon dioxide Substances 0.000 title claims description 5
239000002250 absorbent Substances 0.000 claims abstract description 73
230000002745 absorbent Effects 0.000 claims abstract description 73
QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 claims abstract description 39
229910052753 mercury Inorganic materials 0.000 claims abstract description 35
239000007788 liquid Substances 0.000 claims abstract description 30
239000002245 particle Substances 0.000 claims abstract description 17
229910052751 metal Inorganic materials 0.000 claims abstract description 14
239000002184 metal Substances 0.000 claims abstract description 14
NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims abstract description 12
239000011593 sulfur Substances 0.000 claims abstract description 12
229910052717 sulfur Inorganic materials 0.000 claims abstract description 12
239000007787 solid Substances 0.000 claims abstract description 11
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 5
229910052799 carbon Inorganic materials 0.000 claims abstract description 5
239000012876 carrier material Substances 0.000 claims abstract description 4
229940100892 mercury compound Drugs 0.000 claims description 20
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 12
239000000203 mixture Substances 0.000 claims description 12
150000001875 compounds Chemical class 0.000 claims description 11
239000002243 precursor Substances 0.000 claims description 11
150000002736 metal compounds Chemical class 0.000 claims description 10
239000004215 Carbon black (E152) Substances 0.000 claims description 8
RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 claims description 8
229930195733 hydrocarbon Natural products 0.000 claims description 8
150000002430 hydrocarbons Chemical class 0.000 claims description 7
UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 claims description 4
XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims description 4
239000004568 cement Substances 0.000 claims description 4
229910052976 metal sulfide Inorganic materials 0.000 claims description 4
238000011065 in-situ storage Methods 0.000 claims description 3
WWNBZGLDODTKEM-UHFFFAOYSA-N sulfanylidenenickel Chemical compound [Ni]=S WWNBZGLDODTKEM-UHFFFAOYSA-N 0.000 claims description 3
FMRLDPWIRHBCCC-UHFFFAOYSA-L Zinc carbonate Chemical compound [Zn+2].[O-]C([O-])=O FMRLDPWIRHBCCC-UHFFFAOYSA-L 0.000 claims description 2
JJWKPURADFRFRB-UHFFFAOYSA-N carbonyl sulfide Chemical compound O=C=S JJWKPURADFRFRB-UHFFFAOYSA-N 0.000 claims description 2
BWFPGXWASODCHM-UHFFFAOYSA-N copper monosulfide Chemical compound [Cu]=S BWFPGXWASODCHM-UHFFFAOYSA-N 0.000 claims description 2
TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 claims description 2
229920001021 polysulfide Polymers 0.000 claims description 2
239000011667 zinc carbonate Substances 0.000 claims description 2
229910000010 zinc carbonate Inorganic materials 0.000 claims description 2
235000004416 zinc carbonate Nutrition 0.000 claims description 2
239000011787 zinc oxide Substances 0.000 claims description 2
PCHQDTOLHOFHHK-UHFFFAOYSA-L zinc;hydrogen carbonate Chemical compound [Zn+2].OC([O-])=O.OC([O-])=O PCHQDTOLHOFHHK-UHFFFAOYSA-L 0.000 claims description 2
MBMLMWLHJBBADN-UHFFFAOYSA-N Ferrous sulfide Chemical compound [Fe]=S MBMLMWLHJBBADN-UHFFFAOYSA-N 0.000 claims 1
LSDPWZHWYPCBBB-UHFFFAOYSA-N Methanethiol Chemical compound SC LSDPWZHWYPCBBB-UHFFFAOYSA-N 0.000 claims 1
VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 abstract description 22
238000001035 drying Methods 0.000 abstract description 14
239000003345 natural gas Substances 0.000 abstract description 9
239000007789 gas Substances 0.000 description 36
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 27
ZIBGPFATKBEMQZ-UHFFFAOYSA-N triethylene glycol Chemical compound OCCOCCOCCO ZIBGPFATKBEMQZ-UHFFFAOYSA-N 0.000 description 12
238000010521 absorption reaction Methods 0.000 description 7
PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 6
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 5
150000001298 alcohols Chemical class 0.000 description 5
239000011230 binding agent Substances 0.000 description 5
230000008929 regeneration Effects 0.000 description 5
238000011069 regeneration method Methods 0.000 description 5
239000000243 solution Substances 0.000 description 4
RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 3
239000005749 Copper compound Substances 0.000 description 3
230000015572 biosynthetic process Effects 0.000 description 3
238000009835 boiling Methods 0.000 description 3
229910052802 copper Inorganic materials 0.000 description 3
239000010949 copper Substances 0.000 description 3
230000018044 dehydration Effects 0.000 description 3
238000006297 dehydration reaction Methods 0.000 description 3
238000010438 heat treatment Methods 0.000 description 3
239000000463 material Substances 0.000 description 3
229910052759 nickel Inorganic materials 0.000 description 3
238000005406 washing Methods 0.000 description 3
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 2
XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 2
238000004140 cleaning Methods 0.000 description 2
239000000356 contaminant Substances 0.000 description 2
238000001816 cooling Methods 0.000 description 2
229940116318 copper carbonate Drugs 0.000 description 2
150000001880 copper compounds Chemical class 0.000 description 2
GEZOTWYUIKXWOA-UHFFFAOYSA-L copper;carbonate Chemical compound [Cu+2].[O-]C([O-])=O GEZOTWYUIKXWOA-UHFFFAOYSA-L 0.000 description 2
239000012024 dehydrating agents‎ Substances 0.000 description 2
238000010790 dilution Methods 0.000 description 2
239000012895 dilution Substances 0.000 description 2
150000002170 ethers Chemical class 0.000 description 2
150000002334 glycols Chemical class 0.000 description 2
238000002347 injection Methods 0.000 description 2
239000007924 injection Substances 0.000 description 2
150000002739 metals Chemical class 0.000 description 2
239000002808 molecular sieve Substances 0.000 description 2
229920001223 polyethylene glycol Polymers 0.000 description 2
239000000377 silicon dioxide Substances 0.000 description 2
URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 description 2
UWHCKJMYHZGTIT-UHFFFAOYSA-N tetraethylene glycol Chemical compound OCCOCCOCCOCCO UWHCKJMYHZGTIT-UHFFFAOYSA-N 0.000 description 2
230000003313 weakening effect Effects 0.000 description 2
HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
239000006096 absorbing agent Substances 0.000 description 1
239000002253 acid Substances 0.000 description 1
239000004411 aluminium Substances 0.000 description 1
229910052782 aluminium Inorganic materials 0.000 description 1
XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
229910021529 ammonia Inorganic materials 0.000 description 1
238000000889 atomisation Methods 0.000 description 1
230000015556 catabolic process Effects 0.000 description 1
239000003054 catalyst Substances 0.000 description 1
239000003245 coal Substances 0.000 description 1
238000005260 corrosion Methods 0.000 description 1
230000007797 corrosion Effects 0.000 description 1
238000000354 decomposition reaction Methods 0.000 description 1
238000001514 detection method Methods 0.000 description 1
MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 1
239000006185 dispersion Substances 0.000 description 1
238000004821 distillation Methods 0.000 description 1
230000007613 environmental effect Effects 0.000 description 1
UVGCAWDXQWPTEK-UHFFFAOYSA-N ethane;hydrate Chemical class O.CC UVGCAWDXQWPTEK-UHFFFAOYSA-N 0.000 description 1
238000002474 experimental method Methods 0.000 description 1
239000012530 fluid Substances 0.000 description 1
238000004508 fractional distillation Methods 0.000 description 1
125000003827 glycol group Chemical group 0.000 description 1
239000008187 granular material Substances 0.000 description 1
-1 hydrocarbon hydrates Chemical class 0.000 description 1
229910052739 hydrogen Inorganic materials 0.000 description 1
239000001257 hydrogen Substances 0.000 description 1
125000004435 hydrogen atom Chemical class [H]* 0.000 description 1
229910052742 iron Inorganic materials 0.000 description 1
239000012528 membrane Substances 0.000 description 1
VUZPPFZMUPKLLV-UHFFFAOYSA-N methane;hydrate Chemical class C.O VUZPPFZMUPKLLV-UHFFFAOYSA-N 0.000 description 1
238000002156 mixing Methods 0.000 description 1
150000002816 nickel compounds Chemical class 0.000 description 1
239000003208 petroleum Substances 0.000 description 1
239000011148 porous material Substances 0.000 description 1
230000002035 prolonged effect Effects 0.000 description 1
238000000746 purification Methods 0.000 description 1
230000001105 regulatory effect Effects 0.000 description 1
239000000741 silica gel Substances 0.000 description 1
229910002027 silica gel Inorganic materials 0.000 description 1
238000005486 sulfidation Methods 0.000 description 1
238000003786 synthesis reaction Methods 0.000 description 1
239000002351 wastewater Substances 0.000 description 1
239000011701 zinc Substances 0.000 description 1
229910052725 zinc Inorganic materials 0.000 description 1

Classifications

- B—PERFORMING OPERATIONS; TRANSPORTING
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- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
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- B01J20/0225—Compounds of Fe, Ru, Os, Co, Rh, Ir, Ni, Pd, Pt
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- B01J20/0229—Compounds of Fe
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- B01J20/024—Compounds of Zn, Cd, Hg
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B01J20/3202—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the carrier, support or substrate used for impregnation or coating
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
- C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
- C—CHEMISTRY; METALLURGY
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- C07C7/00—Purification; Separation; Use of additives
- C07C7/11—Purification; Separation; Use of additives by absorption, i.e. purification or separation of gaseous hydrocarbons with the aid of liquids
- B—PERFORMING OPERATIONS; TRANSPORTING
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- B01J2220/42—Materials comprising a mixture of inorganic materials
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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- B01J2220/56—Use in the form of a bed

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Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Analytical Chemistry (AREA)
Chemical Kinetics & Catalysis (AREA)
Inorganic Chemistry (AREA)
Oil, Petroleum & Natural Gas (AREA)
Engineering & Computer Science (AREA)
Water Supply & Treatment (AREA)
Treating Waste Gases (AREA)
Gas Separation By Absorption (AREA)
Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
Removal Of Specific Substances (AREA)

NO20061393A 2003-11-05 2006-03-27 Fremgangsmate for fjerning av kvikksolvforbindelser fra en glykol- og/eller alkoholholdig strom og fremgangsmate for a fjerne vann, svovelforbindelse og/eller karbondioksid fra en hydrokarbonholdig strom NO332292B1 (no)

Applications Claiming Priority (3)

Application Number	Priority Date	Filing Date	Title
GBGB0325769.8A GB0325769D0 (en)	2003-11-05	2003-11-05	Removal of mercury compounds from glycol
GB0414160A GB0414160D0 (en)	2004-06-24	2004-06-24	Removal of mercury compounds from glycol
PCT/GB2004/004593 WO2005047438A1 (en)	2003-11-05	2004-10-29	Removal of mercury compounds from glycol

Publications (2)

Publication Number	Publication Date
NO20061393L NO20061393L (no)	2006-06-02
NO332292B1 true NO332292B1 (no)	2012-08-20

Family

ID=34593728

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
NO20061393A NO332292B1 (no)	2003-11-05	2006-03-27	Fremgangsmate for fjerning av kvikksolvforbindelser fra en glykol- og/eller alkoholholdig strom og fremgangsmate for a fjerne vann, svovelforbindelse og/eller karbondioksid fra en hydrokarbonholdig strom

Country Status (8)

Country	Link
US (1)	US7435338B2 (pt)
EP (1)	EP1680490A1 (pt)
AU (1)	AU2004289867B2 (pt)
BR (1)	BRPI0416164B1 (pt)
EG (1)	EG24723A (pt)
GB (1)	GB0325769D0 (pt)
NO (1)	NO332292B1 (pt)
WO (1)	WO2005047438A1 (pt)

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WO2010061212A1 (en) *	2008-11-25	2010-06-03	Johnson Matthey Plc	Reduced copper sulphide sorbent for removing heavy metals
US8043510B2 (en) *	2009-10-29	2011-10-25	Conocophillips Company	Mercury removal with sorbents magnetically separable from treated fluids
EP2508243A1 (en) *	2011-04-06	2012-10-10	Shell Internationale Research Maatschappij B.V.	Method and apparatus for removing mercury from waste water from hydrocarbon well stream
US8876952B2 (en)	2012-02-06	2014-11-04	Uop Llc	Method of removing mercury from a fluid stream using high capacity copper adsorbents
GB201204650D0 (en)	2012-03-16	2012-05-02	Johnson Matthey Plc	A method for producing a sulphided copper sorbent
AU2013269181B2 (en) *	2012-05-30	2016-03-24	Grant Prideco, Inc.	System and method for removal of heavy metal ions from a rich hydrate inhibitor stream
US9724637B2 (en)	2012-06-22	2017-08-08	Shell Oil Company	Method and apparatus for circulating a glycol stream, and method of producing a natural gas product stream
EP3476460B1 (en) *	2012-09-07	2022-11-02	Chevron U.S.A. Inc.	Method for removing mercury from natural gas
WO2017027550A1 (en)	2015-08-12	2017-02-16	Uop Llc	Composition and process for removing chlorides from a gaseous stream
US10041014B2 (en) *	2016-06-10	2018-08-07	Chevron U.S.A. Inc.	Process, method and system for removal of mercury in a gas dehydration process
WO2017214531A1 (en) *	2016-06-10	2017-12-14	Chevron U.S.A. Inc.	Hydrophobic adsorbents and mercury removal processes therewith
CN110523219B (zh) *	2019-09-10	2020-08-28	艾凡佳德(上海)环保科技有限公司	一种含乙二醇的工业尾气的处理系统及其使用方法
CN111394144A (zh) *	2020-03-13	2020-07-10	山西新华化工有限责任公司	一种脱汞剂及制备方法
CN111762855A (zh) *	2020-06-16	2020-10-13	唐山周行科技发展有限公司	一种含汞废水脱汞装置及方法
FR3130635A1 (fr)	2021-12-20	2023-06-23	IFP Energies Nouvelles	Procede de captation de metaux lourds par co-alimentation d’un flux sulfurant
FR3130636A1 (fr)	2021-12-20	2023-06-23	IFP Energies Nouvelles	Procede de rejuvenation de masses de captation de metaux lourds
CN117443077B (zh) *	2023-10-27	2024-03-15	临沂广辰化工有限公司	一种菊酸乙酯提纯加工装置及方法

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2003
- 2003-11-05 GB GBGB0325769.8A patent/GB0325769D0/en not_active Ceased
2004
- 2004-10-29 AU AU2004289867A patent/AU2004289867B2/en not_active Ceased
- 2004-10-29 EP EP04791629A patent/EP1680490A1/en not_active Withdrawn
- 2004-10-29 US US10/575,555 patent/US7435338B2/en not_active Expired - Fee Related
- 2004-10-29 BR BRPI0416164-5B1A patent/BRPI0416164B1/pt not_active IP Right Cessation
- 2004-10-29 WO PCT/GB2004/004593 patent/WO2005047438A1/en not_active Ceased
2006
- 2006-03-27 NO NO20061393A patent/NO332292B1/no not_active IP Right Cessation
- 2006-05-02 EG EGNA2006000415 patent/EG24723A/xx active

Also Published As

Publication number	Publication date
BRPI0416164B1 (pt)	2015-03-03
US20070134143A1 (en)	2007-06-14
WO2005047438A1 (en)	2005-05-26
NO20061393L (no)	2006-06-02
GB0325769D0 (en)	2003-12-10
US7435338B2 (en)	2008-10-14
EG24723A (en)	2010-06-07
BRPI0416164A (pt)	2007-01-23
AU2004289867B2 (en)	2009-04-23
EP1680490A1 (en)	2006-07-19
AU2004289867A1 (en)	2005-05-26

Legal Events

Date	Code	Title	Description
2017-05-29	MM1K	Lapsed by not paying the annual fees

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