BRPI0704638A2 - processo para a purificaÇço de uma soluÇço de hidrocarbonetos derivada da sÍntese de um carboxilato de lantanÍdeo, mÉtodo para a determinaÇço do teor de Ácido carboxÍlico e/ou Água de uma soluÇço do carboxilato de lantanÍdeo, soluÇço de hidrocarbonetos contendo um carboxilato de lantanÍdeo, e, uso da soluÇço - Google Patents

processo para a purificaÇço de uma soluÇço de hidrocarbonetos derivada da sÍntese de um carboxilato de lantanÍdeo, mÉtodo para a determinaÇço do teor de Ácido carboxÍlico e/ou Água de uma soluÇço do carboxilato de lantanÍdeo, soluÇço de hidrocarbonetos contendo um carboxilato de lantanÍdeo, e, uso da soluÇço

Info

Publication number
BRPI0704638A2
BRPI0704638A2 BRPI0704638-3A BRPI0704638A BRPI0704638A2 BR PI0704638 A2 BRPI0704638 A2 BR PI0704638A2 BR PI0704638 A BRPI0704638 A BR PI0704638A BR PI0704638 A2 BRPI0704638 A2 BR PI0704638A2
Authority
BR
Brazil
Prior art keywords
solution
lanthanide carboxylate
lanthanide
carboxylate
purification
Prior art date
Application number
BRPI0704638-3A
Other languages
English (en)
Inventor
Paolo Biagini
Mario Salvalaggio
Franco Cambisi
Lucia Bonoldi
Liliana Gila
Original Assignee
Polimeri Europa Spa
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Polimeri Europa Spa filed Critical Polimeri Europa Spa
Publication of BRPI0704638A2 publication Critical patent/BRPI0704638A2/pt
Publication of BRPI0704638B1 publication Critical patent/BRPI0704638B1/pt

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/487Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/47Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/41Preparation of salts of carboxylic acids
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/48Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F36/00Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, at least one having two or more carbon-to-carbon double bonds
    • C08F36/02Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, at least one having two or more carbon-to-carbon double bonds the radical having only two carbon-to-carbon double bonds
    • C08F36/04Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, at least one having two or more carbon-to-carbon double bonds the radical having only two carbon-to-carbon double bonds conjugated
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/25Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
    • G01N21/31Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
    • G01N21/35Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
    • G01N21/3563Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light for analysing solids; Preparation of samples therefor
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/25Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
    • G01N21/31Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
    • G01N21/35Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
    • G01N21/3577Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light for analysing liquids, e.g. polluted water

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Investigating Or Analysing Materials By Optical Means (AREA)

Abstract

PROCESSO PARA A PURIFICAÇçO DE UMA SOLUÇçO DE HIDROCARBONETOS DERIVADA DA SÍNTESE DE UM CARBOXILATO DE LANTANÍDEO, MÉTODO PARA A DETERMINAÇçO DO TEOR DE ÁCIDO CARBOXÍLICO E/OU ÁGUA DE UMA SOLUÇçO DO CARBOXILATO DE LANTANÍDEO, SOLUÇçO DE HIDROCARBONETOS CONTENDO UM CARBOXILATO DE LANTANÍDEO, E, USO DA SOLUÇçO. É descrito um processo para a purificação de carboxilatos de lantanideo que é composto de uma etapa na qual a solução de hidrocarbonetos derivada da síntese de carboxilato de lantanídeo, contendo o referido carboxilato e impurezas do ácido carboxílico correspondente e/ou água, é tratado com uma solução aquosa de uma base para obter um pH na fase aquosa variando de 9,0 a 12,2 e/ou uma etapa na qual a solução de hidrocarbonetos contendo o carboxilato de lantanídeo é tratada com um sólido escolhido de Na~ 2~SO~ 4~, MgSO~ 4~, Mg(C1O~ 4~)~ 2~, peneiras moleculares 3<143>, peneiras moleculares 4<143>, peneiras moleculares 5<143> e peneiras moleculares 13 X. São também descritos métodos analíticos, que permitem que a pureza dos carboxilatos de lantanídeos seja medida não destrutivamente.
BRPI0704638A 2006-03-31 2007-03-30 processo para a purificação de uma solução de hidrocarbonetos derivada da síntese de um carboxilato de lantanídeo, método para a determinação do teor de ácido carboxílico e/ou água de uma solução do carboxilato de lantanídeo, solução de hidrocarbonetos contendo um carboxilato de lantanídeo, e, uso da solução BRPI0704638B1 (pt)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
IT000619A ITMI20060619A1 (it) 2006-03-31 2006-03-31 Processo per la purificazione di carbossilati lantanidi

Publications (2)

Publication Number Publication Date
BRPI0704638A2 true BRPI0704638A2 (pt) 2008-12-30
BRPI0704638B1 BRPI0704638B1 (pt) 2016-06-07

Family

ID=37075893

Family Applications (1)

Application Number Title Priority Date Filing Date
BRPI0704638A BRPI0704638B1 (pt) 2006-03-31 2007-03-30 processo para a purificação de uma solução de hidrocarbonetos derivada da síntese de um carboxilato de lantanídeo, método para a determinação do teor de ácido carboxílico e/ou água de uma solução do carboxilato de lantanídeo, solução de hidrocarbonetos contendo um carboxilato de lantanídeo, e, uso da solução

Country Status (13)

Country Link
US (1) US8188304B2 (pt)
EP (1) EP1840112B1 (pt)
KR (1) KR101488986B1 (pt)
CN (1) CN101139276B (pt)
BR (1) BRPI0704638B1 (pt)
CA (1) CA2581987C (pt)
ES (1) ES2557585T3 (pt)
HU (1) HUE028263T2 (pt)
IT (1) ITMI20060619A1 (pt)
MX (1) MX2007003931A (pt)
PL (1) PL1840112T3 (pt)
TW (1) TWI418538B (pt)
ZA (1) ZA200702543B (pt)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ITMI20080570A1 (it) * 2008-04-02 2009-10-03 Polimeri Europa Spa Procedimento per la preparazione di polibutadiene ramificato ad alto contenuto in unita' 1,4-cis

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0564081B1 (en) 1992-02-28 1997-04-23 Sentrachem Limited Production of an organic salt of a rare earth metal
US5783676C1 (en) 1996-03-29 2002-03-12 Rhodia Rare Earths Inc Synthesis of solid powdery rare earth carboxylates by a precipitation method
US6054563A (en) * 1997-03-05 2000-04-25 Rhodia Chimie Preparation of solid, powdery rare earth carboxylates by evaporation method
TW458964B (en) * 1998-03-03 2001-10-11 Chi Mei Corp Process for producing lanthanide series metal carboxylates
US6111082A (en) * 1998-04-17 2000-08-29 Rhodia Rare Earths Inc. Stable concentrated rare earth carboxylate liquids
AU2002300062B8 (en) * 2001-07-16 2010-04-15 Dudley Mills Pty Ltd Removal of Phosphate from Water

Also Published As

Publication number Publication date
US8188304B2 (en) 2012-05-29
EP1840112A1 (en) 2007-10-03
ZA200702543B (en) 2008-07-30
BRPI0704638B1 (pt) 2016-06-07
PL1840112T3 (pl) 2016-03-31
ITMI20060619A1 (it) 2007-10-01
TWI418538B (zh) 2013-12-11
EP1840112B1 (en) 2015-09-30
CN101139276B (zh) 2013-04-17
CA2581987C (en) 2014-02-25
CN101139276A (zh) 2008-03-12
KR101488986B1 (ko) 2015-02-02
CA2581987A1 (en) 2007-09-30
TW200745018A (en) 2007-12-16
US20070232794A1 (en) 2007-10-04
KR20070098731A (ko) 2007-10-05
ES2557585T3 (es) 2016-01-27
MX2007003931A (es) 2009-02-16
HUE028263T2 (hu) 2016-12-28

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Legal Events

Date Code Title Description
B03A Publication of a patent application or of a certificate of addition of invention [chapter 3.1 patent gazette]
B09A Decision: intention to grant [chapter 9.1 patent gazette]
B16A Patent or certificate of addition of invention granted

Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 30/03/2007, OBSERVADAS AS CONDICOES LEGAIS.