CA1111182A - Methode d'amelioration des priorites du chlorure de polyvinyle en poudre - Google Patents

Methode d'amelioration des priorites du chlorure de polyvinyle en poudre

Info

Publication number: CA1111182A
Authority: CA; Canada
Prior art keywords: heat treatment; carried out; polymer; weight; vinyl chloride
Prior art date: 1976-06-04
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

CA279,785A

Other languages

English (en)

Inventor

Inge Konig

Ingolf Mielke

Ulrich Schwenk

Horst Streitberger

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Hoechst AG

Original Assignee

Hoechst AG

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1976-06-04

Filing date

1977-06-03

Publication date

1981-10-20

1977-06-03 Application filed by Hoechst AG filed Critical Hoechst AG

1981-10-20 Application granted granted Critical

1981-10-20 Publication of CA1111182A publication Critical patent/CA1111182A/fr

Status Expired legal-status Critical Current

Links

238000000034 method Methods 0.000 title claims description 40
230000008569 process Effects 0.000 title claims description 32
229920000915 polyvinyl chloride Polymers 0.000 title description 3
239000004800 polyvinyl chloride Substances 0.000 title description 3
BZHJMEDXRYGGRV-UHFFFAOYSA-N Vinyl chloride Chemical compound ClC=C BZHJMEDXRYGGRV-UHFFFAOYSA-N 0.000 claims abstract description 40
125000004432 carbon atom Chemical group C* 0.000 claims abstract description 15
125000002887 hydroxy group Chemical group [H]O* 0.000 claims abstract description 7
229920000642 polymer Polymers 0.000 claims description 73
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 37
238000010438 heat treatment Methods 0.000 claims description 30
239000000178 monomer Substances 0.000 claims description 30
239000000203 mixture Substances 0.000 claims description 27
150000001875 compounds Chemical class 0.000 claims description 16
239000007789 gas Substances 0.000 claims description 13
MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 claims description 10
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 6
125000001931 aliphatic group Chemical group 0.000 claims description 5
229920001577 copolymer Polymers 0.000 claims description 4
229920006395 saturated elastomer Polymers 0.000 claims description 4
ZIBGPFATKBEMQZ-UHFFFAOYSA-N triethylene glycol Chemical compound OCCOCCOCCO ZIBGPFATKBEMQZ-UHFFFAOYSA-N 0.000 claims description 4
ORTVZLZNOYNASJ-UPHRSURJSA-N (z)-but-2-ene-1,4-diol Chemical compound OC\C=C/CO ORTVZLZNOYNASJ-UPHRSURJSA-N 0.000 claims description 3
229920000578 graft copolymer Polymers 0.000 claims description 3
229910052757 nitrogen Inorganic materials 0.000 claims description 3
239000000843 powder Substances 0.000 abstract description 5
150000007824 aliphatic compounds Chemical class 0.000 abstract description 2
-1 vinyl halide Chemical class 0.000 description 20
239000002253 acid Substances 0.000 description 12
239000000047 product Substances 0.000 description 9
125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 8
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BVQVLAIMHVDZEL-UHFFFAOYSA-N 1-phenyl-1,2-propanedione Chemical group CC(=O)C(=O)C1=CC=CC=C1 BVQVLAIMHVDZEL-UHFFFAOYSA-N 0.000 description 2
NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 description 2
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125000000129 anionic group Chemical group 0.000 description 2
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JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 description 2
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ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 2
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239000000049 pigment Substances 0.000 description 2
QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 2
125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 2
230000001681 protective effect Effects 0.000 description 2
239000002904 solvent Substances 0.000 description 2
238000005507 spraying Methods 0.000 description 2
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DNIAPMSPPWPWGF-VKHMYHEASA-N (+)-propylene glycol Chemical compound C[C@H](O)CO DNIAPMSPPWPWGF-VKHMYHEASA-N 0.000 description 1
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OYHQOLUKZRVURQ-NTGFUMLPSA-N (9Z,12Z)-9,10,12,13-tetratritiooctadeca-9,12-dienoic acid Chemical compound C(CCCCCCC\C(=C(/C\C(=C(/CCCCC)\[3H])\[3H])\[3H])\[3H])(=O)O OYHQOLUKZRVURQ-NTGFUMLPSA-N 0.000 description 1
WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 1
BQCIDUSAKPWEOX-UHFFFAOYSA-N 1,1-Difluoroethene Chemical compound FC(F)=C BQCIDUSAKPWEOX-UHFFFAOYSA-N 0.000 description 1
WSLDOOZREJYCGB-UHFFFAOYSA-N 1,2-Dichloroethane Chemical group ClCCCl WSLDOOZREJYCGB-UHFFFAOYSA-N 0.000 description 1
LDVVTQMJQSCDMK-UHFFFAOYSA-N 1,3-dihydroxypropan-2-yl formate Chemical compound OCC(CO)OC=O LDVVTQMJQSCDMK-UHFFFAOYSA-N 0.000 description 1
YPFDHNVEDLHUCE-UHFFFAOYSA-N 1,3-propanediol Substances OCCCO YPFDHNVEDLHUCE-UHFFFAOYSA-N 0.000 description 1
ZFFMLCVRJBZUDZ-UHFFFAOYSA-N 2,3-dimethylbutane Chemical group CC(C)C(C)C ZFFMLCVRJBZUDZ-UHFFFAOYSA-N 0.000 description 1
SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 1
YDHPJFVXLJHHDQ-UHFFFAOYSA-N 2-ethenyl-11-methyldodecanoic acid Chemical class CC(C)CCCCCCCCC(C=C)C(O)=O YDHPJFVXLJHHDQ-UHFFFAOYSA-N 0.000 description 1
KGIGUEBEKRSTEW-UHFFFAOYSA-N 2-vinylpyridine Chemical compound C=CC1=CC=CC=N1 KGIGUEBEKRSTEW-UHFFFAOYSA-N 0.000 description 1
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NLZUEZXRPGMBCV-UHFFFAOYSA-N Butylhydroxytoluene Chemical compound CC1=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C1 NLZUEZXRPGMBCV-UHFFFAOYSA-N 0.000 description 1
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VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
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FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 description 1
FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 description 1
QSJXEFYPDANLFS-UHFFFAOYSA-N Diacetyl Chemical group CC(=O)C(C)=O QSJXEFYPDANLFS-UHFFFAOYSA-N 0.000 description 1
RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical class S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 1
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DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
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229920002451 polyvinyl alcohol Polymers 0.000 description 1
239000000376 reactant Substances 0.000 description 1
WBHHMMIMDMUBKC-XLNAKTSKSA-N ricinelaidic acid Chemical compound CCCCCC[C@@H](O)C\C=C\CCCCCCCC(O)=O WBHHMMIMDMUBKC-XLNAKTSKSA-N 0.000 description 1
229960003656 ricinoleic acid Drugs 0.000 description 1
FEUQNCSVHBHROZ-UHFFFAOYSA-N ricinoleic acid Natural products CCCCCCC(O[Si](C)(C)C)CC=CCCCCCCCC(=O)OC FEUQNCSVHBHROZ-UHFFFAOYSA-N 0.000 description 1
238000005096 rolling process Methods 0.000 description 1
XWGJFPHUCFXLBL-UHFFFAOYSA-M rongalite Chemical compound [Na+].OCS([O-])=O XWGJFPHUCFXLBL-UHFFFAOYSA-M 0.000 description 1
238000007790 scraping Methods 0.000 description 1
229910052709 silver Inorganic materials 0.000 description 1
239000004332 silver Substances 0.000 description 1
229910052708 sodium Inorganic materials 0.000 description 1
239000011734 sodium Substances 0.000 description 1
239000007787 solid Substances 0.000 description 1
239000000243 solution Substances 0.000 description 1
239000000600 sorbitol Substances 0.000 description 1
230000003019 stabilising effect Effects 0.000 description 1
238000003756 stirring Methods 0.000 description 1
150000003440 styrenes Chemical class 0.000 description 1
238000006467 substitution reaction Methods 0.000 description 1
150000005846 sugar alcohols Polymers 0.000 description 1
LSNNMFCWUKXFEE-UHFFFAOYSA-L sulfite Chemical class [O-]S([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-L 0.000 description 1
CIHOLLKRGTVIJN-UHFFFAOYSA-N tert‐butyl hydroperoxide Chemical compound CC(C)(C)OO CIHOLLKRGTVIJN-UHFFFAOYSA-N 0.000 description 1
238000012360 testing method Methods 0.000 description 1
150000004764 thiosulfuric acid derivatives Chemical class 0.000 description 1
VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
UBOXGVDOUJQMTN-UHFFFAOYSA-N trichloroethylene Natural products ClCC(Cl)Cl UBOXGVDOUJQMTN-UHFFFAOYSA-N 0.000 description 1
UFTFJSFQGQCHQW-UHFFFAOYSA-N triformin Chemical compound O=COCC(OC=O)COC=O UFTFJSFQGQCHQW-UHFFFAOYSA-N 0.000 description 1
235000021122 unsaturated fatty acids Nutrition 0.000 description 1
150000004670 unsaturated fatty acids Chemical class 0.000 description 1
JFALSRSLKYAFGM-UHFFFAOYSA-N uranium(0) Chemical compound [U] JFALSRSLKYAFGM-UHFFFAOYSA-N 0.000 description 1
229940117958 vinyl acetate Drugs 0.000 description 1
239000001993 wax Substances 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F6/00—Post-polymerisation treatments
- C08F6/26—Treatment of polymers prepared in bulk also solid polymers or polymer melts

Landscapes

Chemical & Material Sciences (AREA)
Health & Medical Sciences (AREA)
Chemical Kinetics & Catalysis (AREA)
Medicinal Chemistry (AREA)
Polymers & Plastics (AREA)
Organic Chemistry (AREA)
Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)

CA279,785A 1976-06-04 1977-06-03 Methode d'amelioration des priorites du chlorure de polyvinyle en poudre Expired CA1111182A (fr)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
DE19762625167 DE2625167C3 (de)	1976-06-04	1976-06-04	Verfahren zur Verbesserung der Eigenschaften von pulverförmigem Polyvinylchlorid
DEP2625167.2		1976-06-04

Publications (1)

Publication Number	Publication Date
CA1111182A true CA1111182A (fr)	1981-10-20

Family

ID=5979847

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA279,785A Expired CA1111182A (fr)	1976-06-04	1977-06-03	Methode d'amelioration des priorites du chlorure de polyvinyle en poudre

Country Status (13)

Country	Link
JP (1)	JPS52148586A (fr)
BE (1)	BE855434A (fr)
CA (1)	CA1111182A (fr)
CH (1)	CH630100A5 (fr)
DE (1)	DE2625167C3 (fr)
ES (1)	ES459219A1 (fr)
FR (1)	FR2353570A1 (fr)
GB (1)	GB1560765A (fr)
IT (1)	IT1074531B (fr)
MX (1)	MX143249A (fr)
NL (1)	NL7705868A (fr)
SU (1)	SU680653A3 (fr)
YU (1)	YU137877A (fr)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE69330421T2 (de) *	1992-12-10	2002-05-16	Tosoh Corp., Shinnanyo	Verfahren zur Herstellung eines Polymeren vom Vinylchloridtyp
ATE291056T1 (de) *	1999-03-19	2005-04-15	Occidental Chem Co	Stabilisation von polymeren nach aussetzen von oxidation
JP5717452B2 (ja) *	2010-01-15	2015-05-13	日本曹達株式会社	液状ポリブタジエン精製法
EP2915821A1 (fr)	2014-03-04	2015-09-09	Synthomer Ltd.	Procédé de traitement d'une composition de poly(chlorure de vinyle) avec du dioxyde de carbone à phase dense

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DK120776A (da) *	1975-03-20	1976-09-21	Unilever Nv	Fremgangsmade til behandling af blandinger af vinylhalogenid-polymere og additiver
DE2518492B2 (de) *	1975-04-25	1980-04-17	Friedrich Horst 5840 Schwerte Papenmeier	Verfahren und Vorrichtung zum Aufbereiten von Polyvinylchlorid
DD126470A1 (fr) *	1976-07-15	1977-07-20

1976
- 1976-06-04 DE DE19762625167 patent/DE2625167C3/de not_active Expired
1977
- 1977-05-27 NL NL7705868A patent/NL7705868A/xx not_active Application Discontinuation
- 1977-05-27 ES ES459219A patent/ES459219A1/es not_active Expired
- 1977-06-01 CH CH671977A patent/CH630100A5/de not_active IP Right Cessation
- 1977-06-02 IT IT2433377A patent/IT1074531B/it active
- 1977-06-02 MX MX16931977A patent/MX143249A/es unknown
- 1977-06-02 YU YU137877A patent/YU137877A/xx unknown
- 1977-06-03 CA CA279,785A patent/CA1111182A/fr not_active Expired
- 1977-06-03 SU SU772489556A patent/SU680653A3/ru active
- 1977-06-03 JP JP6498177A patent/JPS52148586A/ja active Pending
- 1977-06-06 FR FR7717206A patent/FR2353570A1/fr active Granted
- 1977-06-06 BE BE178235A patent/BE855434A/fr not_active IP Right Cessation
- 1977-06-08 GB GB2390577A patent/GB1560765A/en not_active Expired

Also Published As

Publication number	Publication date
DE2625167C3 (de)	1980-01-31
FR2353570B1 (fr)	1982-09-10
YU137877A (en)	1982-06-30
IT1074531B (it)	1985-04-20
BE855434A (fr)	1977-12-06
FR2353570A1 (fr)	1977-12-30
DE2625167A1 (de)	1977-12-22
DE2625167B2 (de)	1979-05-31
JPS52148586A (en)	1977-12-09
CH630100A5 (en)	1982-05-28
SU680653A3 (ru)	1979-08-15
NL7705868A (nl)	1977-12-06
ES459219A1 (es)	1978-03-01
GB1560765A (en)	1980-02-06
MX143249A (es)	1981-04-06

Legal Events

Date	Code	Title	Description
1998-10-20	MKEX	Expiry

Publication	Publication Date	Title
EP0469759B1 (fr)	1996-01-31	Stabilisation de fluoropolymères
JP2636277B2 (ja)	1997-07-30	凝固分散物グレードのテトラフルオロエチレン・ホモ−またはコポリマーの製法
JPH082929B2 (ja)	1996-01-17	残留モノマー含量の少ない超吸収剤ポリアクリレートの製造法
CA1111182A (fr)	1981-10-20	Methode d'amelioration des priorites du chlorure de polyvinyle en poudre
US2476474A (en)	1949-07-19	Polymerization of vinyl compounds in an aqueous dispersion
SK278977B6 (sk)	1998-05-06	Spôsob výroby termoplastických hmôt na báze homopo
CA1039888A (fr)	1978-10-03	Procede de production de copolymeres avec greffes de chlorure de polyvinyle
DE3505238C2 (fr)	1989-12-07
KR100932452B1 (ko)	2009-12-17	비닐 클로라이드 단량체 중합 반응에서 압력 강하 중에유기 개시제의 첨가 방법
USRE32813E (en)	1988-12-27	Method for the suspension polymerization of vinyl chloride monomer
US3842056A (en)	1974-10-15	Method for producing polyvinyl chloride
US4207412A (en)	1980-06-10	Aftertreatment of spray dried, powdered vinyl chloride emulsion polymerizates
US4115640A (en)	1978-09-19	Aftertreatment of spray dried, powdered vinyl chloride emulsion polymerizates
EP0051945B1 (fr)	1986-04-30	Procédé de suspension pour la polymérisation du monomère de chlorure de vinyle
US3591567A (en)	1971-07-06	Method for producing internally plasticized copolymer of vinyl chloride and a higher alkyl ester of crotonic acid
DE2645918A1 (de)	1978-04-13	Verfahren zum entfernen von monomerem vinylchlorid aus polymerisaten des vinylchlorids
CN120040674B (zh)	2025-07-15	一种高耐候pvc抗冲改性剂的制备方法
DE2457667A1 (de)	1976-06-10	Verfahren zur herstellung von vinylchloridpolymerisaten
JPS6268807A (ja)	1987-03-28	セルロ−ス系グラフト共重合体の製造方法
DE69330421T2 (de)	2002-05-16	Verfahren zur Herstellung eines Polymeren vom Vinylchloridtyp
CA1137688A (fr)	1982-12-14	Procede d'abaissement de la teneur en monomeres residuels de dispersions polymeriques de chlorure de vinyle sensibles au cisaillement ou a la chaleur
US2470910A (en)	1949-05-24	Preparation of granular polymers of vinyl halides
DE1076373B (de)	1960-02-25	Verfahren zur Herstellung von Polyvinylchlorid-Dispersionen
US2492086A (en)	1949-12-20	Preparation of granular copolymers of vinyl chloride-diethyl maleate
DE2629741A1 (de)	1978-01-12	Verfahren zur verbesserung der eigenschaften von pulverfoermigen vinylchlorid-polymerisaten