SU680653A3 - Способ обработки порошкообразного поливинилхлорида - Google Patents
Способ обработки порошкообразного поливинилхлоридаInfo
- Publication number
- SU680653A3 SU680653A3 SU772489556A SU2489556A SU680653A3 SU 680653 A3 SU680653 A3 SU 680653A3 SU 772489556 A SU772489556 A SU 772489556A SU 2489556 A SU2489556 A SU 2489556A SU 680653 A3 SU680653 A3 SU 680653A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- polymer
- polymerization
- vinyl chloride
- water
- mixture
- Prior art date
Links
- 238000000034 method Methods 0.000 title description 15
- 238000012545 processing Methods 0.000 title description 10
- 229920000642 polymer Polymers 0.000 description 39
- BZHJMEDXRYGGRV-UHFFFAOYSA-N Vinyl chloride Chemical compound ClC=C BZHJMEDXRYGGRV-UHFFFAOYSA-N 0.000 description 27
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 26
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 24
- 239000000203 mixture Substances 0.000 description 22
- 238000006116 polymerization reaction Methods 0.000 description 18
- 238000010438 heat treatment Methods 0.000 description 17
- 239000004800 polyvinyl chloride Substances 0.000 description 16
- 229920000915 polyvinyl chloride Polymers 0.000 description 16
- 150000001875 compounds Chemical class 0.000 description 14
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 13
- 239000007789 gas Substances 0.000 description 10
- 238000011282 treatment Methods 0.000 description 10
- 239000000178 monomer Substances 0.000 description 9
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 8
- 238000012662 bulk polymerization Methods 0.000 description 8
- 125000004432 carbon atom Chemical group C* 0.000 description 8
- 229920001577 copolymer Polymers 0.000 description 8
- 239000000843 powder Substances 0.000 description 6
- 229920006395 saturated elastomer Polymers 0.000 description 6
- 239000000126 substance Substances 0.000 description 6
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 description 5
- 238000012360 testing method Methods 0.000 description 5
- -1 2-ethylhexoate Chemical compound 0.000 description 4
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 4
- 125000001931 aliphatic group Chemical group 0.000 description 4
- 230000007423 decrease Effects 0.000 description 4
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 4
- 229910052757 nitrogen Inorganic materials 0.000 description 4
- QYKIQEUNHZKYBP-UHFFFAOYSA-N Vinyl ether Chemical class C=COC=C QYKIQEUNHZKYBP-UHFFFAOYSA-N 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 229910052799 carbon Inorganic materials 0.000 description 3
- 230000000052 comparative effect Effects 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 229920000578 graft copolymer Polymers 0.000 description 3
- 239000012071 phase Substances 0.000 description 3
- UFTFJSFQGQCHQW-UHFFFAOYSA-N triformin Chemical compound O=COCC(OC=O)COC=O UFTFJSFQGQCHQW-UHFFFAOYSA-N 0.000 description 3
- OEPOKWHJYJXUGD-UHFFFAOYSA-N 2-(3-phenylmethoxyphenyl)-1,3-thiazole-4-carbaldehyde Chemical compound O=CC1=CSC(C=2C=C(OCC=3C=CC=CC=3)C=CC=2)=N1 OEPOKWHJYJXUGD-UHFFFAOYSA-N 0.000 description 2
- NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 description 2
- KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 2
- 239000005977 Ethylene Substances 0.000 description 2
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 2
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 2
- 150000007513 acids Chemical class 0.000 description 2
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 2
- 239000003570 air Substances 0.000 description 2
- 150000001298 alcohols Chemical class 0.000 description 2
- 150000001336 alkenes Chemical class 0.000 description 2
- 150000001735 carboxylic acids Chemical class 0.000 description 2
- 238000004587 chromatography analysis Methods 0.000 description 2
- JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 description 2
- ZSWFCLXCOIISFI-UHFFFAOYSA-N cyclopentadiene Chemical compound C1C=CC=C1 ZSWFCLXCOIISFI-UHFFFAOYSA-N 0.000 description 2
- 238000010790 dilution Methods 0.000 description 2
- 239000012895 dilution Substances 0.000 description 2
- 239000000839 emulsion Substances 0.000 description 2
- 150000002148 esters Chemical class 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 150000002334 glycols Chemical class 0.000 description 2
- 239000011261 inert gas Substances 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 229920000151 polyglycol Polymers 0.000 description 2
- 239000010695 polyglycol Substances 0.000 description 2
- 238000006884 silylation reaction Methods 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 238000010557 suspension polymerization reaction Methods 0.000 description 2
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 2
- ZIBGPFATKBEMQZ-UHFFFAOYSA-N triethylene glycol Chemical compound OCCOCCOCCO ZIBGPFATKBEMQZ-UHFFFAOYSA-N 0.000 description 2
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 2
- 229920002554 vinyl polymer Polymers 0.000 description 2
- BQCIDUSAKPWEOX-UHFFFAOYSA-N 1,1-Difluoroethene Chemical compound FC(F)=C BQCIDUSAKPWEOX-UHFFFAOYSA-N 0.000 description 1
- RZYHXKLKJRGJGP-UHFFFAOYSA-N 2,2,2-trifluoro-n,n-bis(trimethylsilyl)acetamide Chemical compound C[Si](C)(C)N([Si](C)(C)C)C(=O)C(F)(F)F RZYHXKLKJRGJGP-UHFFFAOYSA-N 0.000 description 1
- QRCSMPCUJFDIIM-UHFFFAOYSA-N 3-ethoxyoctane Chemical compound CCCCCC(CC)OCC QRCSMPCUJFDIIM-UHFFFAOYSA-N 0.000 description 1
- FERIUCNNQQJTOY-UHFFFAOYSA-N Butyric acid Chemical compound CCCC(O)=O FERIUCNNQQJTOY-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 101100518501 Mus musculus Spp1 gene Proteins 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 1
- XBDQKXXYIPTUBI-UHFFFAOYSA-M Propionate Chemical compound CCC([O-])=O XBDQKXXYIPTUBI-UHFFFAOYSA-M 0.000 description 1
- 150000008065 acid anhydrides Chemical class 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 239000012736 aqueous medium Substances 0.000 description 1
- 239000007900 aqueous suspension Substances 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- WERYXYBDKMZEQL-UHFFFAOYSA-N butane-1,4-diol Chemical compound OCCCCO WERYXYBDKMZEQL-UHFFFAOYSA-N 0.000 description 1
- 150000001721 carbon Chemical group 0.000 description 1
- 239000004359 castor oil Substances 0.000 description 1
- 235000019438 castor oil Nutrition 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000007872 degassing Methods 0.000 description 1
- 150000001993 dienes Chemical class 0.000 description 1
- 150000005690 diesters Chemical class 0.000 description 1
- HGQSXVKHVMGQRG-UHFFFAOYSA-N dioctyltin Chemical compound CCCCCCCC[Sn]CCCCCCCC HGQSXVKHVMGQRG-UHFFFAOYSA-N 0.000 description 1
- 238000010556 emulsion polymerization method Methods 0.000 description 1
- BPEQQKXOMYZIJU-UHFFFAOYSA-N ethenyl tridecanoate Chemical compound CCCCCCCCCCCCC(=O)OC=C BPEQQKXOMYZIJU-UHFFFAOYSA-N 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000011010 flushing procedure Methods 0.000 description 1
- 238000004817 gas chromatography Methods 0.000 description 1
- 239000007792 gaseous phase Substances 0.000 description 1
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 1
- 238000010559 graft polymerization reaction Methods 0.000 description 1
- 229920001519 homopolymer Polymers 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 239000011976 maleic acid Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000002609 medium Substances 0.000 description 1
- 125000005395 methacrylic acid group Chemical group 0.000 description 1
- 239000003607 modifier Substances 0.000 description 1
- 125000001971 neopentyl group Chemical group [H]C([*])([H])C(C([H])([H])[H])(C([H])([H])[H])C([H])([H])[H] 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000000546 pharmaceutical excipient Substances 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 230000000379 polymerizing effect Effects 0.000 description 1
- 239000001294 propane Substances 0.000 description 1
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 1
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 1
- KOUKXHPPRFNWPP-UHFFFAOYSA-N pyrazine-2,5-dicarboxylic acid;hydrate Chemical compound O.OC(=O)C1=CN=C(C(O)=O)C=N1 KOUKXHPPRFNWPP-UHFFFAOYSA-N 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 125000001424 substituent group Chemical group 0.000 description 1
- 238000010558 suspension polymerization method Methods 0.000 description 1
- 229920001169 thermoplastic Polymers 0.000 description 1
- 239000004416 thermosoftening plastic Substances 0.000 description 1
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
- 238000003260 vortexing Methods 0.000 description 1
- 230000003245 working effect Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F6/00—Post-polymerisation treatments
- C08F6/26—Treatment of polymers prepared in bulk also solid polymers or polymer melts
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19762625167 DE2625167C3 (de) | 1976-06-04 | 1976-06-04 | Verfahren zur Verbesserung der Eigenschaften von pulverförmigem Polyvinylchlorid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU680653A3 true SU680653A3 (ru) | 1979-08-15 |
Family
ID=5979847
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU772489556A SU680653A3 (ru) | 1976-06-04 | 1977-06-03 | Способ обработки порошкообразного поливинилхлорида |
Country Status (13)
| Country | Link |
|---|---|
| JP (1) | JPS52148586A (fr) |
| BE (1) | BE855434A (fr) |
| CA (1) | CA1111182A (fr) |
| CH (1) | CH630100A5 (fr) |
| DE (1) | DE2625167C3 (fr) |
| ES (1) | ES459219A1 (fr) |
| FR (1) | FR2353570A1 (fr) |
| GB (1) | GB1560765A (fr) |
| IT (1) | IT1074531B (fr) |
| MX (1) | MX143249A (fr) |
| NL (1) | NL7705868A (fr) |
| SU (1) | SU680653A3 (fr) |
| YU (1) | YU137877A (fr) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE69330421T2 (de) * | 1992-12-10 | 2002-05-16 | Tosoh Corp., Shinnanyo | Verfahren zur Herstellung eines Polymeren vom Vinylchloridtyp |
| ATE291056T1 (de) * | 1999-03-19 | 2005-04-15 | Occidental Chem Co | Stabilisation von polymeren nach aussetzen von oxidation |
| JP5717452B2 (ja) * | 2010-01-15 | 2015-05-13 | 日本曹達株式会社 | 液状ポリブタジエン精製法 |
| EP2915821A1 (fr) | 2014-03-04 | 2015-09-09 | Synthomer Ltd. | Procédé de traitement d'une composition de poly(chlorure de vinyle) avec du dioxyde de carbone à phase dense |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DK120776A (da) * | 1975-03-20 | 1976-09-21 | Unilever Nv | Fremgangsmade til behandling af blandinger af vinylhalogenid-polymere og additiver |
| DE2518492B2 (de) * | 1975-04-25 | 1980-04-17 | Friedrich Horst 5840 Schwerte Papenmeier | Verfahren und Vorrichtung zum Aufbereiten von Polyvinylchlorid |
| DD126470A1 (fr) * | 1976-07-15 | 1977-07-20 |
-
1976
- 1976-06-04 DE DE19762625167 patent/DE2625167C3/de not_active Expired
-
1977
- 1977-05-27 NL NL7705868A patent/NL7705868A/xx not_active Application Discontinuation
- 1977-05-27 ES ES459219A patent/ES459219A1/es not_active Expired
- 1977-06-01 CH CH671977A patent/CH630100A5/de not_active IP Right Cessation
- 1977-06-02 IT IT2433377A patent/IT1074531B/it active
- 1977-06-02 MX MX16931977A patent/MX143249A/es unknown
- 1977-06-02 YU YU137877A patent/YU137877A/xx unknown
- 1977-06-03 CA CA279,785A patent/CA1111182A/fr not_active Expired
- 1977-06-03 SU SU772489556A patent/SU680653A3/ru active
- 1977-06-03 JP JP6498177A patent/JPS52148586A/ja active Pending
- 1977-06-06 FR FR7717206A patent/FR2353570A1/fr active Granted
- 1977-06-06 BE BE178235A patent/BE855434A/fr not_active IP Right Cessation
- 1977-06-08 GB GB2390577A patent/GB1560765A/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| DE2625167C3 (de) | 1980-01-31 |
| FR2353570B1 (fr) | 1982-09-10 |
| YU137877A (en) | 1982-06-30 |
| IT1074531B (it) | 1985-04-20 |
| BE855434A (fr) | 1977-12-06 |
| FR2353570A1 (fr) | 1977-12-30 |
| DE2625167A1 (de) | 1977-12-22 |
| DE2625167B2 (de) | 1979-05-31 |
| JPS52148586A (en) | 1977-12-09 |
| CH630100A5 (en) | 1982-05-28 |
| NL7705868A (nl) | 1977-12-06 |
| ES459219A1 (es) | 1978-03-01 |
| CA1111182A (fr) | 1981-10-20 |
| GB1560765A (en) | 1980-02-06 |
| MX143249A (es) | 1981-04-06 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US2716638A (en) | Divinyltetramethyldisiloxane and polymers therefrom | |
| US3069401A (en) | Copolymers of hexafluoropropylene vinylidene fluoride and aliphatic, chain transfer agents | |
| US3629214A (en) | Process for the copolymerization of vinyltrialkoxysilanes | |
| SU680653A3 (ru) | Способ обработки порошкообразного поливинилхлорида | |
| SU776563A3 (ru) | Полимерна композици | |
| FI83090B (fi) | Foerfarande foer bildande av en loesning av en vatten loeslig polymer, vilken innehaoller sura grupper, i en blandning av ett polart loesningsmedel, vatten och bas. | |
| US2651627A (en) | Process for polymerizing phenyltrifluoroethylene | |
| JPH0629317B2 (ja) | 酸素脱着によるポリエステルの色改善法 | |
| EP1421124A1 (fr) | Regulation du poids moleculaire de copolymeres greffes au moyen d'agents de migration de chaine polymerisables | |
| EP0445839A1 (fr) | Elastomères fluorés à base de fluorure de vinylidène, hexafluoropropène et tétrafluoroéthylène | |
| US4122249A (en) | Solvent removal from chlorinated polymers | |
| EP0107895A2 (fr) | Procédé d'élimination | |
| US3357964A (en) | Process for the polymerization of vinyl aromatic compounds | |
| US4104459A (en) | Treating polyvinyl chloride resins | |
| US3271432A (en) | Process for the manufacture of polybasic araliphatic carboxylic acids and products thereof | |
| Yano et al. | Effects of peroxide bonds and their degradation products on the dielectric relaxations of polystyrene | |
| CA1109193A (fr) | Methode de degazage de polymeres et de copolymeres prepares par polymerisation en bloc d'un melange monomere a base de chlorure de vinyle | |
| US2751372A (en) | Highly unsaturated polymers derived from polymeric isopropenyl acylates | |
| Brepoels et al. | Kinetics of block polymerizations | |
| IE42687B1 (en) | Process for the continuous manufacture of polymers and copolymers of vinyl chloride | |
| US2196714A (en) | Rubberlike polymer and method of making the same | |
| RU2026307C1 (ru) | Способ получения сополимеров изобутилена и полярного винилового мономера | |
| US3477987A (en) | Protection of olefinic polymers | |
| US3796694A (en) | Process for the preparation of cyclic acid anhydrides | |
| DE3122614A1 (de) | "verfahren zur polymerisation von vinylchlorid in der masse" |