CH184540A - Process for the preparation of a mixture of quaternary ammonium compounds. - Google Patents
Process for the preparation of a mixture of quaternary ammonium compounds.Info
- Publication number
- CH184540A CH184540A CH184540DA CH184540A CH 184540 A CH184540 A CH 184540A CH 184540D A CH184540D A CH 184540DA CH 184540 A CH184540 A CH 184540A
- Authority
- CH
- Switzerland
- Prior art keywords
- mixture
- quaternary ammonium
- ammonium compounds
- preparation
- water
- Prior art date
Links
- 239000000203 mixture Substances 0.000 title claims description 8
- 238000000034 method Methods 0.000 title claims description 7
- 150000003856 quaternary ammonium compounds Chemical class 0.000 title claims description 5
- 238000002360 preparation method Methods 0.000 title description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 4
- AGEZXYOZHKGVCM-UHFFFAOYSA-N benzyl bromide Chemical compound BrCC1=CC=CC=C1 AGEZXYOZHKGVCM-UHFFFAOYSA-N 0.000 claims description 3
- 238000006243 chemical reaction Methods 0.000 claims description 3
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 3
- 239000003925 fat Substances 0.000 claims description 3
- 229930195729 fatty acid Natural products 0.000 claims description 3
- 239000000194 fatty acid Substances 0.000 claims description 3
- 150000004665 fatty acids Chemical class 0.000 claims description 3
- 150000001412 amines Chemical class 0.000 claims description 2
- 125000003277 amino group Chemical group 0.000 claims description 2
- 230000000249 desinfective effect Effects 0.000 claims description 2
- 238000005187 foaming Methods 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims description 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 2
- 238000007127 saponification reaction Methods 0.000 claims description 2
- ROSDSFDQCJNGOL-UHFFFAOYSA-N Dimethylamine Chemical compound CNC ROSDSFDQCJNGOL-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- KCXMKQUNVWSEMD-UHFFFAOYSA-N benzyl chloride Chemical compound ClCC1=CC=CC=C1 KCXMKQUNVWSEMD-UHFFFAOYSA-N 0.000 description 1
- 229940073608 benzyl chloride Drugs 0.000 description 1
- 238000010531 catalytic reduction reaction Methods 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000012749 thinning agent Substances 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
Verfahren zur Herstellung eines Gemisches von quaternären Ammoniumverbindungen. Gegenstand des Hauptpatentes ist ein Verfahren zur Herstellung einer quaternären Ammoniumverbindung durch Einwirkenlassen voll Benzylchlorid auf Diätbyldodecylamin.
Gegenstand des vorliegenden Patentes ist ein Verfahren zur Herstellung eines Ge- tnisches von quaternären Ammoniumverbin- dungen. Das Verfahren ist dadurch gekenn zeichnet, dass man auf ein Gemisch von Dimethylalkylaminen, wie es durch Um wandlung der bei der Verseifung von natür lichen Fetten entstehenden Fettsäuren in die entsprechenden Amine unter Einführung von zwei Methylgruppen in die Aminogruppe erhältlich ist, Benzylbromid einwirken lässt.
Die Reaktion erfolgt zweckmässig unter Er wärmen und kann in Gegenwart eines Ver- dünnemittels, wie Wasser oder Alkohol, durchgeführt werden. Das bei der Reaktion entstandene Produkt bildet eine zähe; gelb liche Masse, die in Wasser zu einer klaren, stark schäumenden Lösung löslich ist.
Es hat netzende und desinfizierende Eigenschaf ten und soll für Desinfektionszwecke Ver- wendung-finden. <I>Beispiel:</I> Zu 240 Gewichtsteilen eines Gemisches voll Dimethylalkylaminen, wie es beispiels weise durch katalytische Reduktion natür licher Fette, bezw. der daraus erhältlichen Fettsäureamide bei Gegenwart von Dimethyl- amin gewonnen wird, fügt man 171 Ge wichtsteile Benzylbromid und erwärmt das Gemisch unter Rühren 12 Stunden im Dampf bad.
Nach dem Erkalten bildet das Reak tionsprodukt eine zähe gelbliche Masse, die sich klar in Wasser löst und dessen wässrige Lösungen stark schäumen.
Process for the preparation of a mixture of quaternary ammonium compounds. The subject of the main patent is a process for the preparation of a quaternary ammonium compound by exposing dietbyldodecylamine to full benzyl chloride.
The subject of the present patent is a process for the production of a mixture of quaternary ammonium compounds. The process is characterized in that benzyl bromide is allowed to act on a mixture of dimethylalkylamines such as can be obtained by converting the fatty acids formed during the saponification of natural fats into the corresponding amines by introducing two methyl groups into the amino group.
The reaction is expediently carried out with heating and can be carried out in the presence of a thinning agent such as water or alcohol. The product resulting from the reaction forms a tough one; yellowish mass that is soluble in water to form a clear, strongly foaming solution.
It has wetting and disinfecting properties and should be used for disinfection purposes. <I> Example: </I> To 240 parts by weight of a mixture full of dimethylalkylamines, such as, for example, by catalytic reduction of natural fats, respectively. the fatty acid amide obtainable therefrom is obtained in the presence of dimethylamine, 171 parts by weight of benzyl bromide are added and the mixture is heated in a steam bath for 12 hours while stirring.
After cooling, the reaction product forms a viscous yellowish mass that dissolves clearly in water and its aqueous solutions foam strongly.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE184540X | 1933-04-13 | ||
| CH175812T | 1934-04-03 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH184540A true CH184540A (en) | 1936-05-31 |
Family
ID=25719752
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH184540D CH184540A (en) | 1933-04-13 | 1934-04-03 | Process for the preparation of a mixture of quaternary ammonium compounds. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH184540A (en) |
-
1934
- 1934-04-03 CH CH184540D patent/CH184540A/en unknown
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