CH373499A - Verfahren zur Herstellung metallhaltiger Azofarbstoffe - Google Patents

Verfahren zur Herstellung metallhaltiger Azofarbstoffe

Info

Publication number: CH373499A
Authority: CH; Switzerland
Prior art keywords: parts; dye; weight; metal; chromium
Prior art date: 1957-12-23

Application number

CH6707058A

Other languages

German (de)

English (en)

Inventor

Gerhard Dr Dittmar

Rolf Dr Puetter

Walter Dr Scholl

Fritz Dr Suckfuell

Original Assignee

Bayer Ag

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1957-12-23

Filing date

1958-12-08

Publication date

1963-11-30

1958-12-08 Application filed by Bayer Ag filed Critical Bayer Ag

1963-11-30 Publication of CH373499A publication Critical patent/CH373499A/de

Links

229910052751 metal Inorganic materials 0.000 title claims description 8
239000002184 metal Substances 0.000 title claims description 8
238000000034 method Methods 0.000 title claims description 6
239000000987 azo dye Substances 0.000 title claims description 4
238000004519 manufacturing process Methods 0.000 title claims description 3
239000000975 dye Substances 0.000 claims description 53
NYGZLYXAPMMJTE-UHFFFAOYSA-M metanil yellow Chemical group [Na+].[O-]S(=O)(=O)C1=CC=CC(N=NC=2C=CC(NC=3C=CC=CC=3)=CC=2)=C1 NYGZLYXAPMMJTE-UHFFFAOYSA-M 0.000 claims description 20
229940124530 sulfonamide Drugs 0.000 claims description 16
229910052804 chromium Inorganic materials 0.000 claims description 15
239000011651 chromium Substances 0.000 claims description 15
VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims description 14
230000002378 acidificating effect Effects 0.000 claims description 10
150000001875 compounds Chemical class 0.000 claims description 8
239000000203 mixture Substances 0.000 claims description 6
229910017052 cobalt Inorganic materials 0.000 claims description 5
239000010941 cobalt Substances 0.000 claims description 5
GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims description 5
125000000664 diazo group Chemical group [N-]=[N+]=[*] 0.000 claims description 5
125000001424 substituent group Chemical group 0.000 claims description 3
LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 claims description 2
125000002843 carboxylic acid group Chemical group 0.000 claims description 2
239000003795 chemical substances by application Substances 0.000 claims description 2
230000009918 complex formation Effects 0.000 claims description 2
238000001465 metallisation Methods 0.000 claims description 2
125000000217 alkyl group Chemical group 0.000 claims 1
150000003456 sulfonamides Chemical class 0.000 claims 1
125000001174 sulfone group Chemical group 0.000 claims 1
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 27
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 25
210000002268 wool Anatomy 0.000 description 12
235000002639 sodium chloride Nutrition 0.000 description 10
LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 9
FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 9
239000000843 powder Substances 0.000 description 9
239000011780 sodium chloride Substances 0.000 description 9
230000007935 neutral effect Effects 0.000 description 8
KMUONIBRACKNSN-UHFFFAOYSA-N potassium dichromate Chemical compound [K+].[K+].[O-][Cr](=O)(=O)O[Cr]([O-])(=O)=O KMUONIBRACKNSN-UHFFFAOYSA-N 0.000 description 7
238000006243 chemical reaction Methods 0.000 description 6
238000004043 dyeing Methods 0.000 description 4
239000011541 reaction mixture Substances 0.000 description 4
-1 1 , 4 - naphthoquinone methylene sulfone Chemical compound 0.000 description 3
238000003756 stirring Methods 0.000 description 3
229910021556 Chromium(III) chloride Inorganic materials 0.000 description 2
RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 2
238000009835 boiling Methods 0.000 description 2
QSWDMMVNRMROPK-UHFFFAOYSA-K chromium(3+) trichloride Chemical compound [Cl-].[Cl-].[Cl-].[Cr+3] QSWDMMVNRMROPK-UHFFFAOYSA-K 0.000 description 2
239000011636 chromium(III) chloride Substances 0.000 description 2
235000007831 chromium(III) chloride Nutrition 0.000 description 2
229940044175 cobalt sulfate Drugs 0.000 description 2
229910000361 cobalt sulfate Inorganic materials 0.000 description 2
KTVIXTQDYHMGHF-UHFFFAOYSA-L cobalt(2+) sulfate Chemical compound [Co+2].[O-]S([O-])(=O)=O KTVIXTQDYHMGHF-UHFFFAOYSA-L 0.000 description 2
238000004040 coloring Methods 0.000 description 2
UFWIBTONFRDIAS-UHFFFAOYSA-N naphthalene-acid Natural products C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 description 2
USFZMSVCRYTOJT-UHFFFAOYSA-N Ammonium acetate Chemical compound N.CC(O)=O USFZMSVCRYTOJT-UHFFFAOYSA-N 0.000 description 1
239000005695 Ammonium acetate Substances 0.000 description 1
NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonium chloride Substances [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 1
VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 1
VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Chemical compound OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
241001366278 Leptotes marina Species 0.000 description 1
ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Natural products OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
239000004952 Polyamide Substances 0.000 description 1
150000001447 alkali salts Chemical class 0.000 description 1
229940043376 ammonium acetate Drugs 0.000 description 1
235000019257 ammonium acetate Nutrition 0.000 description 1
235000011114 ammonium hydroxide Nutrition 0.000 description 1
150000001720 carbohydrates Chemical class 0.000 description 1
235000014633 carbohydrates Nutrition 0.000 description 1
239000000460 chlorine Substances 0.000 description 1
229910052801 chlorine Inorganic materials 0.000 description 1
ZCDOYSPFYFSLEW-UHFFFAOYSA-N chromate(2-) Chemical class [O-][Cr]([O-])(=O)=O ZCDOYSPFYFSLEW-UHFFFAOYSA-N 0.000 description 1
230000008878 coupling Effects 0.000 description 1
238000010168 coupling process Methods 0.000 description 1
238000005859 coupling reaction Methods 0.000 description 1
239000010985 leather Substances 0.000 description 1
239000000463 material Substances 0.000 description 1
239000000434 metal complex dye Substances 0.000 description 1
150000007524 organic acids Chemical class 0.000 description 1
229920002647 polyamide Polymers 0.000 description 1
229920006306 polyurethane fiber Polymers 0.000 description 1
150000003839 salts Chemical class 0.000 description 1
125000000565 sulfonamide group Chemical group 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B45/00—Complex metal compounds of azo dyes
- C09B45/02—Preparation from dyes containing in o-position a hydroxy group and in o'-position hydroxy, alkoxy, carboxyl, amino or keto groups
- C09B45/14—Monoazo compounds
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B45/00—Complex metal compounds of azo dyes
- C09B45/02—Preparation from dyes containing in o-position a hydroxy group and in o'-position hydroxy, alkoxy, carboxyl, amino or keto groups
- C09B45/14—Monoazo compounds
- C09B45/18—Monoazo compounds containing copper
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B45/00—Complex metal compounds of azo dyes
- C09B45/02—Preparation from dyes containing in o-position a hydroxy group and in o'-position hydroxy, alkoxy, carboxyl, amino or keto groups
- C09B45/14—Monoazo compounds
- C09B45/22—Monoazo compounds containing other metals
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B45/00—Complex metal compounds of azo dyes
- C09B45/02—Preparation from dyes containing in o-position a hydroxy group and in o'-position hydroxy, alkoxy, carboxyl, amino or keto groups
- C09B45/24—Disazo or polyazo compounds

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Coloring (AREA)

CH6707058A 1957-12-23 1958-12-08 Verfahren zur Herstellung metallhaltiger Azofarbstoffe CH373499A (de)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
DEF24678A DE1220063B (de)	1957-12-23	1957-12-23	Verfahren zur Herstellung metallhaltiger Azofarbstoffe

Publications (1)

Publication Number	Publication Date
CH373499A true CH373499A (de)	1963-11-30

Family

ID=7091321

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CH6707058A CH373499A (de)	1957-12-23	1958-12-08	Verfahren zur Herstellung metallhaltiger Azofarbstoffe

Country Status (3)

Country	Link
BE (1)	BE574117A (fr)
CH (1)	CH373499A (fr)
DE (1)	DE1220063B (fr)

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE937367C (de) *	1951-08-17	1956-01-05	Ciba Geigy	Verfahren zur Herstellung chrom- oder kobalthaltiger Azofarbstoffe
FR1073177A (fr) *	1952-03-24	1954-09-20	Ciba Geigy	Nouveaux colorants azoïques métallifères, leur préparation et leur emploi
DE940483C (de) *	1952-12-04	1956-03-22	Bayer Ag	Verfahren zur Herstellung von metallkomplexbildenden Azofarbstoffen

1957
- 1957-12-23 DE DEF24678A patent/DE1220063B/de active Pending
1958
- 1958-12-08 CH CH6707058A patent/CH373499A/de unknown
- 1958-12-22 BE BE574117A patent/BE574117A/fr unknown

Also Published As

Publication number	Publication date
DE1220063B (de)	1966-06-30
BE574117A (fr)	1959-06-22

Publication	Publication Date	Title
DE751343C (de)	1953-05-04	Verfahren zur Herstellung von Disazofarbstoffen
DE821977C (de)	1951-11-22	Verfahren zur Herstellung von Azofarbstoffen
DE2704364C2 (fr)	1988-04-14
DE899537C (de)	1953-12-14	Verfahren zur Herstellung von 0-Oxy-0'-caboxy-azofarbstoffen
CH373499A (de)	1963-11-30	Verfahren zur Herstellung metallhaltiger Azofarbstoffe
DE955800C (de)	1957-01-10	Verfahren zur Herstellung chromhaltiger Azofarbstoffe der Pyrazolonreihe
DE951946C (de)	1956-11-08	Verfahren zur Herstellung von o,o'-Dioxyazofarbstoffen bzw. deren Metallkomplexverbindungen
DE953827C (de)	1956-12-06	Verfahren zur Herstellung metallhaltiger Azofarbstoffe
DE889338C (de)	1953-09-10	Verfahren zur Herstellung von Disazofarbstoffen
DE937367C (de)	1956-01-05	Verfahren zur Herstellung chrom- oder kobalthaltiger Azofarbstoffe
DE951471C (de)	1956-10-31	Verfahren zur Herstellung metallhaltiger Monoazofarbstoffe
DE818669C (de)	1951-10-25	Verfahren zur Herstellung von neuen Disazofarbstoffen
DE629743C (de)	1936-05-16	Verfahren zur Herstellung von Trisazofarbstoffen
CH386591A (de)	1965-01-15	Verfahren zur Herstellung von Azofarbstoffen
DE896187C (de)	1953-11-09	Verfahren zur Herstellung echter Faerbungen
DE1011100B (de)	1957-06-27	Verfahren zur Herstellung von Monoazofarbstoffen bzw. deren Metallkomplexverbindungen
CH355548A (de)	1961-07-15	Verfahren zur Herstellung von Monoazofarbstoffen und deren Metallkomplexverbindungen
DE1007902B (de)	1957-05-09	Verfahren zur Herstellung metallhaltiger Monoazofarbstoffe
DE836221C (de)	1952-04-10	Verfahren zur Herstellung von wasserloeslichen metallhaltigen Azofarbstoffen
AT165532B (de)	1950-03-10	Verfahren zur Herstellung neuer Azofarbstoffe
DE844771C (de)	1952-07-24	Verfahren zur Herstellung metallhaltiger Azofarbstoffe
CH413166A (de)	1966-05-15	Verfahren zur Herstellung von metallhaltigen Monoazofarbstoffen
CH358173A (de)	1961-11-15	Verfahren zur Herstellung von Dioxyazofarbstoffen
DE1007903B (de)	1957-05-09	Verfahren zur Herstellung von Monoazofarbstoffen bzw. deren Metallkomplexverbindungen
DE1007901B (de)	1957-05-09	Verfahren zur Herstellung von wasserloeslichen chromhaltigen Farbstoffen