CH377844A - Verfahren zur Herstellung von 5-Aminomethyl-2-furfurylamin - Google Patents
Verfahren zur Herstellung von 5-Aminomethyl-2-furfurylaminInfo
- Publication number
- CH377844A CH377844A CH8209359A CH8209359A CH377844A CH 377844 A CH377844 A CH 377844A CH 8209359 A CH8209359 A CH 8209359A CH 8209359 A CH8209359 A CH 8209359A CH 377844 A CH377844 A CH 377844A
- Authority
- CH
- Switzerland
- Prior art keywords
- sep
- aminomethyl
- furfurylamine
- amination
- pressure
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 15
- 238000002360 preparation method Methods 0.000 title claims description 4
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 21
- 229910021529 ammonia Inorganic materials 0.000 claims description 8
- 238000005576 amination reaction Methods 0.000 claims description 7
- 239000003054 catalyst Substances 0.000 claims description 7
- 239000003960 organic solvent Substances 0.000 claims description 3
- 230000001419 dependent effect Effects 0.000 claims 2
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 9
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- 150000001414 amino alcohols Chemical class 0.000 description 4
- XTHFKEDIFFGKHM-UHFFFAOYSA-N Dimethoxyethane Chemical compound COCCOC XTHFKEDIFFGKHM-UHFFFAOYSA-N 0.000 description 3
- 239000007868 Raney catalyst Substances 0.000 description 3
- NPXOKRUENSOPAO-UHFFFAOYSA-N Raney nickel Chemical compound [Al].[Ni] NPXOKRUENSOPAO-UHFFFAOYSA-N 0.000 description 3
- 229910000564 Raney nickel Inorganic materials 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 239000000706 filtrate Substances 0.000 description 3
- XBOHKUPCELBZPH-UHFFFAOYSA-N furan-2,3-diamine Chemical compound NC=1C=COC=1N XBOHKUPCELBZPH-UHFFFAOYSA-N 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 229910052757 nitrogen Inorganic materials 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- 238000004821 distillation Methods 0.000 description 2
- 229910000069 nitrogen hydride Inorganic materials 0.000 description 2
- 238000005292 vacuum distillation Methods 0.000 description 2
- -1 5-aminomethyl-furfuryl Chemical group 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000012043 crude product Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000004508 fractional distillation Methods 0.000 description 1
- XPFVYQJUAUNWIW-UHFFFAOYSA-N furfuryl alcohol Substances OCC1=CC=CO1 XPFVYQJUAUNWIW-UHFFFAOYSA-N 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000012442 inert solvent Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 235000020075 ouzo Nutrition 0.000 description 1
- 229940075930 picrate Drugs 0.000 description 1
- OXNIZHLAWKMVMX-UHFFFAOYSA-M picrate anion Chemical compound [O-]C1=C([N+]([O-])=O)C=C([N+]([O-])=O)C=C1[N+]([O-])=O OXNIZHLAWKMVMX-UHFFFAOYSA-M 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000010926 purge Methods 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
- C07D307/52—Radicals substituted by nitrogen atoms not forming part of a nitro radical
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Furan Compounds (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US78369858A | 1958-12-30 | 1958-12-30 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH377844A true CH377844A (de) | 1964-05-31 |
Family
ID=25130142
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH8209359A CH377844A (de) | 1958-12-30 | 1959-12-21 | Verfahren zur Herstellung von 5-Aminomethyl-2-furfurylamin |
Country Status (4)
| Country | Link |
|---|---|
| BE (1) | BE585729A (es) |
| CH (1) | CH377844A (es) |
| ES (1) | ES254884A1 (es) |
| GB (1) | GB930506A (es) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FI783098A7 (fi) * | 1977-10-11 | 1979-04-12 | Glaxo Group Ltd | Farmakologiskt aktiva kompositioner |
-
1959
- 1959-12-11 GB GB4221759A patent/GB930506A/en not_active Expired
- 1959-12-16 BE BE585729A patent/BE585729A/fr unknown
- 1959-12-21 CH CH8209359A patent/CH377844A/de unknown
- 1959-12-23 ES ES0254884A patent/ES254884A1/es not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| GB930506A (en) | 1963-07-03 |
| BE585729A (fr) | 1960-06-16 |
| ES254884A1 (es) | 1960-04-01 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE2429935C3 (de) | Verfahren zur Herstellung von 2,2,6,6- Tetramethyl-4-oxopiperidin | |
| DE1768339C3 (de) | Verfahren zur Herstellung von Orthokieselsäuretetramethylester | |
| DE2149917A1 (de) | Verfahren zur Herstellung von 2-Pyrrolidinon | |
| DE880136C (de) | Verfahren zur Herstellung von Adipinsäuredinitril | |
| CH325080A (de) | Verfahren zur Herstellung von organischen Hydroxylaminverbindungen | |
| DE958649C (de) | Verfahren zur Herstellung von N-substituierten 6, 7-Dihydro-5 H-dibenz-(c,e)-azepinen | |
| DE2715518C2 (es) | ||
| DE2451473A1 (de) | Verfahren zur herstellung von formylpropylacetaten | |
| AT159575B (de) | Verfahren zum katalytischen Hydrieren von aliphatischen, niedrigmolekularen Oxyoxoverbindungen. | |
| DE823882C (de) | Verfahren zur Herstellung von aliphatischen Halogenoxyverbindungen | |
| DE861844C (de) | Verfahren zur Reduktion von organischen Verbindungen mit Hilfe von Formamid | |
| DE886447C (de) | Verfahren zur Herstellung von ªÏ,ªÏ'-Dicyandibutylaethern | |
| DE848952C (de) | Verfahren zur Herstellung von organischen Verbindungen | |
| DE939811C (de) | Verfahren zur Herstellung von ªÏ-Caprolactam und seinen Derivaten | |
| DE724297C (de) | Verfahren zur Aufarbeitung von Glycerinpechen | |
| CH311203A (de) | Verfahren zur Herstellung aromatischer Alkylamine. | |
| DE574834C (de) | Verfahren zur Herstellung von Alkoholen | |
| DE871005C (de) | Verfahren zur Herstellung von Butin-2-diol-1, 4 | |
| CH342554A (de) | Verfahren zur Herstellung von mehrwertigen Alkoholen, vorzugsweise 1,3-Propylenglykol, aus Hexiten | |
| DE1004155B (de) | Verfahren zur Herstellung von 1, 4-Dichlorbutan aus 1, 4-Dioxybutan | |
| DE1054996B (de) | Verfahren zur Herstellung von substituierten Pyrrolen | |
| DE1227450B (de) | Verfahren zur Herstellung von sekundaeren N-Alkyl-allylaminen | |
| DE1044085B (de) | Verfahren zur Herstellung von N-Methyl-ª-phenyl-ª-methylsuccinimid | |
| DE1080096B (de) | Verfahren zur Herstellung von olefinisch-ungesaettigten AEthern mit besonderer Riechstoffeigenschaften | |
| CH254446A (de) | Verfahren zur Herstellung eines neuen Oxyhydrophenanthren-Derivates. |