CH641128A5 - Procede de fabrication en semi-continu de zeolithe a. - Google Patents

Procede de fabrication en semi-continu de zeolithe a. Download PDF

Info

Publication number: CH641128A5
Authority: CH; Switzerland
Prior art keywords: zeolite; solution; gel; prepared; particle size
Prior art date: 1978-12-15

Application number

CH1112679A

Other languages

English (en)

French (fr)

Inventor

Bernard Berger

Original Assignee

Ugine Kuhlmann

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1978-12-15

Filing date

1979-12-14

Publication date

1984-02-15

1979-12-14 Application filed by Ugine Kuhlmann filed Critical Ugine Kuhlmann

1984-02-15 Publication of CH641128A5 publication Critical patent/CH641128A5/fr

Links

238000004519 manufacturing process Methods 0.000 title description 13
239000010457 zeolite Substances 0.000 claims description 27
HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims description 26
229910021536 Zeolite Inorganic materials 0.000 claims description 25
PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 24
239000002245 particle Substances 0.000 claims description 12
238000000034 method Methods 0.000 claims description 11
238000002425 crystallisation Methods 0.000 claims description 9
230000008025 crystallization Effects 0.000 claims description 9
230000014759 maintenance of location Effects 0.000 claims description 7
238000002156 mixing Methods 0.000 claims description 7
150000004645 aluminates Chemical class 0.000 claims description 6
239000004115 Sodium Silicate Substances 0.000 claims description 5
NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims description 5
229910052911 sodium silicate Inorganic materials 0.000 claims description 5
ANBBXQWFNXMHLD-UHFFFAOYSA-N aluminum;sodium;oxygen(2-) Chemical compound [O-2].[O-2].[Na+].[Al+3] ANBBXQWFNXMHLD-UHFFFAOYSA-N 0.000 claims description 3
238000009826 distribution Methods 0.000 claims description 3
238000002360 preparation method Methods 0.000 claims description 3
229910001388 sodium aluminate Inorganic materials 0.000 claims description 3
150000002500 ions Chemical class 0.000 claims description 2
229920006395 saturated elastomer Polymers 0.000 claims 1
VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 32
239000011734 sodium Substances 0.000 description 25
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 24
239000000499 gel Substances 0.000 description 16
229910001868 water Inorganic materials 0.000 description 14
239000000047 product Substances 0.000 description 13
239000000377 silicon dioxide Substances 0.000 description 12
229910052681 coesite Inorganic materials 0.000 description 11
229910052906 cristobalite Inorganic materials 0.000 description 11
229910052682 stishovite Inorganic materials 0.000 description 11
229910052905 tridymite Inorganic materials 0.000 description 11
BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 10
239000011575 calcium Substances 0.000 description 8
230000005070 ripening Effects 0.000 description 6
229910004298 SiO 2 Inorganic materials 0.000 description 5
239000000203 mixture Substances 0.000 description 5
238000003756 stirring Methods 0.000 description 5
229910018072 Al 2 O 3 Inorganic materials 0.000 description 4
CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 4
238000001556 precipitation Methods 0.000 description 4
235000012239 silicon dioxide Nutrition 0.000 description 4
230000015572 biosynthetic process Effects 0.000 description 3
239000003599 detergent Substances 0.000 description 3
238000005342 ion exchange Methods 0.000 description 3
239000000843 powder Substances 0.000 description 3
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
IRPGOXJVTQTAAN-UHFFFAOYSA-N 2,2,3,3,3-pentafluoropropanal Chemical compound FC(F)(F)C(F)(F)C=O IRPGOXJVTQTAAN-UHFFFAOYSA-N 0.000 description 2
KLZUFWVZNOTSEM-UHFFFAOYSA-K Aluminum fluoride Inorganic materials F[Al](F)F KLZUFWVZNOTSEM-UHFFFAOYSA-K 0.000 description 2
238000004131 Bayer process Methods 0.000 description 2
KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 2
238000006243 chemical reaction Methods 0.000 description 2
238000001914 filtration Methods 0.000 description 2
239000007788 liquid Substances 0.000 description 2
239000011541 reaction mixture Substances 0.000 description 2
238000000926 separation method Methods 0.000 description 2
229910052708 sodium Inorganic materials 0.000 description 2
239000007787 solid Substances 0.000 description 2
239000000725 suspension Substances 0.000 description 2
238000003786 synthesis reaction Methods 0.000 description 2
239000005995 Aluminium silicate Substances 0.000 description 1
BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 description 1
101100348017 Drosophila melanogaster Nazo gene Proteins 0.000 description 1
229910003638 H2SiF6 Inorganic materials 0.000 description 1
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
229910019142 PO4 Inorganic materials 0.000 description 1
229910000676 Si alloy Inorganic materials 0.000 description 1
XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
238000002441 X-ray diffraction Methods 0.000 description 1
239000002253 acid Substances 0.000 description 1
AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical class [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 description 1
229910052782 aluminium Inorganic materials 0.000 description 1
235000012211 aluminium silicate Nutrition 0.000 description 1
229910001570 bauxite Inorganic materials 0.000 description 1
229910001424 calcium ion Inorganic materials 0.000 description 1
230000015556 catabolic process Effects 0.000 description 1
150000001768 cations Chemical class 0.000 description 1
238000010908 decantation Methods 0.000 description 1
238000006731 degradation reaction Methods 0.000 description 1
238000010586 diagram Methods 0.000 description 1
238000001035 drying Methods 0.000 description 1
239000000835 fiber Substances 0.000 description 1
239000012467 final product Substances 0.000 description 1
239000007789 gas Substances 0.000 description 1
239000008233 hard water Substances 0.000 description 1
238000000265 homogenisation Methods 0.000 description 1
239000012535 impurity Substances 0.000 description 1
238000009776 industrial production Methods 0.000 description 1
230000000977 initiatory effect Effects 0.000 description 1
NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 1
229910052749 magnesium Inorganic materials 0.000 description 1
239000011777 magnesium Substances 0.000 description 1
239000012452 mother liquor Substances 0.000 description 1
238000005192 partition Methods 0.000 description 1
235000021317 phosphate Nutrition 0.000 description 1
150000003013 phosphoric acid derivatives Chemical class 0.000 description 1
239000011148 porous material Substances 0.000 description 1
239000002994 raw material Substances 0.000 description 1
230000001105 regulatory effect Effects 0.000 description 1
239000000741 silica gel Substances 0.000 description 1
229910002027 silica gel Inorganic materials 0.000 description 1
229910052710 silicon Inorganic materials 0.000 description 1
125000004436 sodium atom Chemical group 0.000 description 1
239000000126 substance Substances 0.000 description 1
ZEFWRWWINDLIIV-UHFFFAOYSA-N tetrafluorosilane;dihydrofluoride Chemical compound F.F.F[Si](F)(F)F ZEFWRWWINDLIIV-UHFFFAOYSA-N 0.000 description 1
239000004753 textile Substances 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/20—Silicates
- C01B33/26—Aluminium-containing silicates, i.e. silico-aluminates
- C01B33/28—Base exchange silicates, e.g. zeolites
- C01B33/2807—Zeolitic silicoaluminates with a tridimensional crystalline structure possessing molecular sieve properties; Isomorphous compounds wherein a part of the aluminium ore of the silicon present may be replaced by other elements such as gallium, germanium, phosphorus; Preparation of zeolitic molecular sieves from molecular sieves of another type or from preformed reacting mixtures
- C01B33/2815—Zeolitic silicoaluminates with a tridimensional crystalline structure possessing molecular sieve properties; Isomorphous compounds wherein a part of the aluminium ore of the silicon present may be replaced by other elements such as gallium, germanium, phosphorus; Preparation of zeolitic molecular sieves from molecular sieves of another type or from preformed reacting mixtures of type A (UNION CARBIDE trade name; corresponds to GRACE's types Z-12 or Z-12L)
- C01B33/2823—Zeolitic silicoaluminates with a tridimensional crystalline structure possessing molecular sieve properties; Isomorphous compounds wherein a part of the aluminium ore of the silicon present may be replaced by other elements such as gallium, germanium, phosphorus; Preparation of zeolitic molecular sieves from molecular sieves of another type or from preformed reacting mixtures of type A (UNION CARBIDE trade name; corresponds to GRACE's types Z-12 or Z-12L) from aqueous solutions of an alkali metal aluminate and an alkali metal silicate excluding any other source of alumina or silica

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Life Sciences & Earth Sciences (AREA)
General Life Sciences & Earth Sciences (AREA)
Geology (AREA)
Inorganic Chemistry (AREA)
Silicates, Zeolites, And Molecular Sieves (AREA)
Solid-Sorbent Or Filter-Aiding Compositions (AREA)

CH1112679A 1978-12-15 1979-12-14 Procede de fabrication en semi-continu de zeolithe a. CH641128A5 (fr)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
FR7835344A FR2444005A1 (fr)	1978-12-15	1978-12-15	Procede industriel de fabrication en semi-continu de zeolithe a

Publications (1)

Publication Number	Publication Date
CH641128A5 true CH641128A5 (fr)	1984-02-15

Family

ID=9216175

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CH1112679A CH641128A5 (fr)	1978-12-15	1979-12-14	Procede de fabrication en semi-continu de zeolithe a.

Country Status (21)

Country	Link
JP (1)	JPS5585416A (it)
BE (1)	BE880533A (it)
BR (1)	BR7908222A (it)
CA (1)	CA1142501A (it)
CH (1)	CH641128A5 (it)
DE (1)	DE2950086A1 (it)
DK (1)	DK532479A (it)
ES (1)	ES8101516A1 (it)
FI (1)	FI793923A7 (it)
FR (1)	FR2444005A1 (it)
GB (1)	GB2038301B (it)
GR (1)	GR66001B (it)
HU (1)	HU181898B (it)
IT (1)	IT1119601B (it)
LU (1)	LU81989A1 (it)
NO (1)	NO794092L (it)
PL (1)	PL125174B1 (it)
PT (1)	PT70474A (it)
RO (1)	RO78900A (it)
SE (1)	SE7910247L (it)
YU (1)	YU296179A (it)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS6049130B2 (ja) *	1980-12-27	1985-10-31	日本化学工業株式会社	Ａ型ゼオライトの製造法
DK164097C (da) *	1982-09-20	1992-10-05	Tosoh Corp	Fremgangsmaade til fremstilling af zeoliter
DE3926400A1 (de) *	1988-08-12	1990-02-22	Degussa	Zeolithpulver des typs naa fuer die verwendung in fluessigwaschmitteln
EP0490011B1 (en) *	1990-12-14	1994-09-07	Foret, S.A.	A process to obtain zeolite 4A starting from bauxite
SI2673237T2 (sl)	2011-02-11	2025-12-31	Zs Pharma, Inc	Uporaba cirkonijevega silikata v zdravljenju hiperkalemije
US9943637B2 (en)	2012-06-11	2018-04-17	ZS Pharma, Inc.	Microporous zirconium silicate and its method of production
CN104968336A (zh) *	2012-07-11	2015-10-07	Zs制药公司	用于治疗高钙血症患者高钾血症的微孔硅酸锆以及用于治疗高钾血症的改进的含钙组合物
US10695365B2 (en)	2012-10-22	2020-06-30	ZS Pharma, Inc.	Microporous zirconium silicate for the treatment of hyperkalemia
CN104797263B (zh)	2012-10-22	2018-02-09	Zs制药公司	用于治疗高钾血症的微孔硅酸锆
WO2016134277A1 (en) *	2015-02-20	2016-08-25	Usalco, Llc	Stable concentrated polyaluminum chlorosilicate solutions
US9592253B1 (en)	2015-10-14	2017-03-14	ZS Pharma, Inc.	Extended use zirconium silicate compositions and methods of use thereof

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
FR1280877A (fr) *	1961-01-14	1962-01-08	Socony Mobil Oil Co	Procédé de préparation de zéolithes cristallins
GB1115489A (en) *	1964-07-31	1968-05-29	Deputy Minister	A process to manufacture crystalline synthetic zeolites for use as molecular sieves
US3425800A (en) *	1967-10-05	1969-02-04	Aluminum Co Of America	Production of crystalline zeolites
AT322511B (de) *	1970-06-15	1975-05-26	Martinswerk G M B H Fuer Chem	Verfahren zur direktherstellung eines reinen kristallinen zeolithischen molekularsiebes mit einer porenweite von 4å.
DD107428B3 (de) *	1973-11-05	1992-12-10	Chemie Ag Bittrfeld Wolfen	Verfahren und vorrichtung zur herstellung synthetischer zeolithe
DE2447021C3 (de) *	1974-10-02	1984-03-22	Degussa Ag, 6000 Frankfurt	Kristallines Zeolithpulver des Typs A und das Verfahren zu seiner Herstellung
DE2651384C2 (de) *	1976-11-11	1984-03-15	Degussa Ag, 6000 Frankfurt	Verfahren zur Aufbereitung von Siliziumdioxid enthaltenden Abfallstäuben zu kristallinem zeolithischem Molekularsieb vom Typ A
DE2651445A1 (de) *	1976-11-11	1978-05-18	Degussa	Kristallines zeolithpulver des typs a ii

1978
- 1978-12-15 FR FR7835344A patent/FR2444005A1/fr active Granted
1979
- 1979-10-20 GR GR60306A patent/GR66001B/el unknown
- 1979-11-20 PT PT70474A patent/PT70474A/pt unknown
- 1979-11-26 GB GB7940829A patent/GB2038301B/en not_active Expired
- 1979-12-05 YU YU02961/79A patent/YU296179A/xx unknown
- 1979-12-11 BE BE0/198501A patent/BE880533A/fr not_active IP Right Cessation
- 1979-12-12 CA CA000341755A patent/CA1142501A/fr not_active Expired
- 1979-12-12 SE SE7910247A patent/SE7910247L/ not_active Application Discontinuation
- 1979-12-13 LU LU81989A patent/LU81989A1/fr unknown
- 1979-12-13 JP JP16090979A patent/JPS5585416A/ja active Pending
- 1979-12-13 DE DE19792950086 patent/DE2950086A1/de not_active Withdrawn
- 1979-12-14 ES ES486941A patent/ES8101516A1/es not_active Expired
- 1979-12-14 PL PL1979220420A patent/PL125174B1/pl unknown
- 1979-12-14 HU HU79KU550A patent/HU181898B/hu unknown
- 1979-12-14 RO RO7999542A patent/RO78900A/ro unknown
- 1979-12-14 BR BR7908222A patent/BR7908222A/pt unknown
- 1979-12-14 FI FI793923A patent/FI793923A7/fi not_active Application Discontinuation
- 1979-12-14 IT IT69413/79A patent/IT1119601B/it active
- 1979-12-14 NO NO794092A patent/NO794092L/no unknown
- 1979-12-14 CH CH1112679A patent/CH641128A5/fr not_active IP Right Cessation
- 1979-12-14 DK DK532479A patent/DK532479A/da unknown

Also Published As

Publication number	Publication date
GR66001B (it)	1981-01-13
FI793923A7 (fi)	1981-01-01
GB2038301A (en)	1980-07-23
DE2950086A1 (de)	1980-06-19
BE880533A (fr)	1980-06-11
PL125174B1 (en)	1983-04-30
BR7908222A (pt)	1980-07-22
IT1119601B (it)	1986-03-10
ES486941A0 (es)	1980-12-16
IT7969413A0 (it)	1979-12-14
FR2444005A1 (fr)	1980-07-11
YU296179A (en)	1983-01-21
DK532479A (da)	1980-06-16
LU81989A1 (fr)	1981-07-23
PL220420A1 (it)	1980-10-06
CA1142501A (fr)	1983-03-08
RO78900A (ro)	1982-12-06
GB2038301B (en)	1983-02-09
HU181898B (en)	1983-11-28
SE7910247L (sv)	1980-06-16
ES8101516A1 (es)	1980-12-16
NO794092L (no)	1980-06-17
FR2444005B1 (it)	1984-05-11
PT70474A (fr)	1979-12-01
JPS5585416A (en)	1980-06-27

Legal Events

Date	Code	Title	Description
1986-08-29	PL	Patent ceased
2024-10-31	PL	Patent ceased

Publication	Publication Date	Title
CH634282A5 (fr)	1983-01-31	Procede de preparation en continu de zeolithe a.
CA1082161A (en)	1980-07-22	Crystalline type-a zeolite powder
JP2523433B2 (ja)	1996-08-07	Ｐ型ゼオライトを製造する方法
NO150114B (no)	1984-05-14	Fremgangsmaate ved fremstilling av krystallinske ionebyttematerialer av alkalimetallaluminiumsilikat
CH641128A5 (fr)	1984-02-15	Procede de fabrication en semi-continu de zeolithe a.
FR2629444A1 (fr)	1989-10-06	Zeolites a base de silice et d'oxyde de germanium et procede de synthese de celles-ci
CH631682A5 (fr)	1982-08-31	Procede de fabrication d'un silico-aluminate de sodium cristallin de la variete 4a.
JPH1171108A (ja)	1999-03-16	合成ケイ酸マグネシウム
BE1001314A4 (fr)	1989-09-26	Procede de production d'alumines hydratees, et procede de traitement de rejets acides.
CN111559750A (zh)	2020-08-21	一种高效连续电子级氟化锂生产工艺
US3549317A (en)	1970-12-22	Process for utilizing fluorosilicic acid
CA1150711A (fr)	1983-07-26	Cristallisation de la zeolithe a lors des procedes industriels de fabrication
CN111186852A (zh)	2020-05-22	利用副产氟硅酸提纯石英物料及制备氟化铝和高纯度白炭黑的工艺
CN1043635C (zh)	1999-06-16	沸石p－型碱金属硅铝酸盐的制备方法
FR2543939A1 (fr)	1984-10-12	Procede de fabrication de zeolite a et produits obtenus
FR2552418A1 (fr)	1985-03-29	Procede de fabrication de zeolithe du type zsm-5
US8734750B2 (en)	2014-05-27	Sodium silicate solutions
JP3442120B2 (ja)	2003-09-02	シリカヒドロゲルを洗浄する方法
RU2808413C1 (ru)	2023-11-28	Способ получения жидкого стекла
CN107777690A (zh)	2018-03-09	一种纯化硅源的方法
SU882929A1 (ru)	1981-11-23	Способ получени фторалюминатов
JPS62132726A (ja)	1987-06-16	Ｌ型ゼオライトの製造法
EP0784594A1 (fr)	1997-07-23	Procede de fabrication de sels alcalins phosphates, sels et silices obtenus, ainsi que detergent ou produit alimentaire contenant ces sels
JPS6025368B2 (ja)	1985-06-18	粒状無定形アルミノ珪酸塩の連続製造方法
EP0485262A1 (fr)	1992-05-13	Procédé de préparation de zéolithe 4A cristallisée