CH99680A - Process for the preparation of an azo dye. - Google Patents
Process for the preparation of an azo dye.Info
- Publication number
- CH99680A CH99680A CH99680DA CH99680A CH 99680 A CH99680 A CH 99680A CH 99680D A CH99680D A CH 99680DA CH 99680 A CH99680 A CH 99680A
- Authority
- CH
- Switzerland
- Prior art keywords
- azo dye
- preparation
- dye
- dyes
- produced
- Prior art date
Links
- 239000000987 azo dye Substances 0.000 title claims description 3
- 238000000034 method Methods 0.000 title claims description 3
- 238000002360 preparation method Methods 0.000 title description 2
- 239000000975 dye Substances 0.000 claims description 9
- 150000008049 diazo compounds Chemical class 0.000 claims description 3
- 239000000835 fiber Substances 0.000 claims description 2
- RGCKGOZRHPZPFP-UHFFFAOYSA-N alizarin Chemical compound C1=CC=C2C(=O)C3=C(O)C(O)=CC=C3C(=O)C2=C1 RGCKGOZRHPZPFP-UHFFFAOYSA-N 0.000 claims 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- WFNLHDJJZSJARK-UHFFFAOYSA-N 2-chloro-6-methylaniline Chemical compound CC1=CC=CC(Cl)=C1N WFNLHDJJZSJARK-UHFFFAOYSA-N 0.000 description 1
- 239000007900 aqueous suspension Substances 0.000 description 1
- 239000001054 red pigment Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
Landscapes
- Coloring (AREA)
Description
Verfahren zur Herstellung eines Azofarbstoffes. <B>in</B> E4 s wurde gefunden, dass man zu sehr bäuchechten Farbstoffen von Aliza,riiiiiuan- cen gelangt, wenn man die Diazoverbinclung von 6-Chlor-2-toluidin mit dem 4-Brom-3- toluidid der 2-3-Oxynaphto#s5,ure kuppelt.
Der Farbstoff kann für sich allein zwecks Verwendung als roter Pigmentfiarbstoff her gestellt werden, er kann aber aueli auf (ler vegetabilischen Faser erzeugt werden. Die Bäucheclitheit dieses Farbstoffes ist, im Gegensatz züi derjenigen ähnlich zusammen gesetzter Farbstoffe ganz überraschend.
<I>Beispiel:</I> Die aus 1.4,1 gr 6-Clilor-2-1,oliiidiii in<B>üb-</B> licher Weise dargestellte Diazoverbindung lässt man unter Rühren in eine wässerige Sus pension von<B>37</B> gr 2 -3-Oxviia,plitoUsäiire-4- Brom-3-toluidid einfliessen, bereitet durch Auflösen in Natronlauge und Wiederaus- fällen mit verdünnter Essigsäure. Der Farb stoff scheidet sieh in roten Flocken aus; ,darauf wird filtriert, gewaschen und ge trocknet.
Process for the preparation of an azo dye. <B> in </B> E4 s it was found that very stomach-fast dyes from Aliza, riiiiiuan- cen can be obtained if the diazo compound of 6-chloro-2-toluidine with the 4-bromo-3-toluidide of the 2 -3-Oxynaphto # s5, ure couples.
The dye can be produced on its own for the purpose of using it as a red pigment dye, but it can also be produced on (ler vegetable fiber. The bellicose clarity of this dye, in contrast to that of similarly composed dyes, is quite surprising.
<I> Example: </I> The diazo compound prepared from 1.4,1 gr 6-Clilor-2-1, oliiidiii in the usual way is left with stirring in an aqueous suspension of <B > 37 </B> gr 2 -3-Oxviia, plitoUsäiire-4-bromo-3-toluidide, prepared by dissolving in sodium hydroxide solution and reprecipitating with dilute acetic acid. The dye separates out in red flakes; , then it is filtered, washed and dried ge.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE99680X | 1921-09-21 | ||
| CH99284T | 1922-06-20 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH99680A true CH99680A (en) | 1923-06-16 |
Family
ID=25705534
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH99680D CH99680A (en) | 1921-09-21 | 1922-06-20 | Process for the preparation of an azo dye. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH99680A (en) |
-
1922
- 1922-06-20 CH CH99680D patent/CH99680A/en unknown
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