CR9805A - Proceso para la produccion de amidas - Google Patents

Proceso para la produccion de amidas

Info

Publication number
CR9805A
CR9805A CR9805A CR9805A CR9805A CR 9805 A CR9805 A CR 9805A CR 9805 A CR9805 A CR 9805A CR 9805 A CR9805 A CR 9805A CR 9805 A CR9805 A CR 9805A
Authority
CR
Costa Rica
Prior art keywords
formula
compound
reaction
amidas
production
Prior art date
Application number
CR9805A
Other languages
English (en)
Inventor
Hans Tobler
Harald Walter
Josef Ehrenfreund
Camilla Corsi
Fanny Giordano
Martin Zeller
Gottfried Seifert
Shailesh Shah
Neil George
Original Assignee
Syngenta Participations Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Syngenta Participations Ag filed Critical Syngenta Participations Ag
Publication of CR9805A publication Critical patent/CR9805A/es

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C211/00Compounds containing amino groups bound to a carbon skeleton
    • C07C211/43Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton
    • C07C211/57Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings being part of condensed ring systems of the carbon skeleton
    • C07C211/61Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings being part of condensed ring systems of the carbon skeleton with at least one of the condensed ring systems formed by three or more rings
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/48Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
    • A01N43/561,2-Diazoles; Hydrogenated 1,2-diazoles
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C205/00Compounds containing nitro groups bound to a carbon skeleton
    • C07C205/06Compounds containing nitro groups bound to a carbon skeleton having nitro groups bound to carbon atoms of six-membered aromatic rings
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/30Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds
    • C07C209/32Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds by reduction of nitro groups
    • C07C209/325Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds by reduction of nitro groups reduction by other means than indicated in C07C209/34 or C07C209/36
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/68Preparation of compounds containing amino groups bound to a carbon skeleton from amines, by reactions not involving amino groups, e.g. reduction of unsaturated amines, aromatisation, or substitution of the carbon skeleton
    • C07C209/70Preparation of compounds containing amino groups bound to a carbon skeleton from amines, by reactions not involving amino groups, e.g. reduction of unsaturated amines, aromatisation, or substitution of the carbon skeleton by reduction of unsaturated amines
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D231/00Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2603/00Systems containing at least three condensed rings
    • C07C2603/56Ring systems containing bridged rings
    • C07C2603/58Ring systems containing bridged rings containing three rings
    • C07C2603/60Ring systems containing bridged rings containing three rings containing at least one ring with less than six members
    • C07C2603/66Ring systems containing bridged rings containing three rings containing at least one ring with less than six members containing five-membered rings

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Plant Pathology (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Agronomy & Crop Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Hydrogenated Pyridines (AREA)

Abstract

Se refiere al proceso para la preparacion de compuestos de la formula en la cual R1 y R2 son cada uno independientes de los otros hidrogeno o C1-C5 alkilo y R3 es CF3 o CF2H por a) reaccion de un compuesto de la formula (II) en la cual R1 y R2 son como estan definidas para la formula (I) con al menos un agente reductor para formar un compuesto de formula (III) en el cual R1 y R2 son como estan definidas para la formula (I), y b) reaccion de ese compuesto con al menos un agente reductor para formar un compuesto de la formula (IV) en el cual R1 y R2, son como estan definidos en la formula (I) y (c) reaccion de ese compuesto con un compuesto de formula (V) en el cual Q es cloro, fluor, bromo, yodo, hidroxido o C1-C6 alkoxi y R3 es como se define en la formula (I) para formar el compuesto de la formula (I); y para intermediarios novedosos para utilizarse en ese proceso.
CR9805A 2005-09-16 2008-03-07 Proceso para la produccion de amidas CR9805A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH15202005 2005-09-16
CH2962006 2006-02-24

Publications (1)

Publication Number Publication Date
CR9805A true CR9805A (es) 2008-07-31

Family

ID=37467494

Family Applications (1)

Application Number Title Priority Date Filing Date
CR9805A CR9805A (es) 2005-09-16 2008-03-07 Proceso para la produccion de amidas

Country Status (18)

Country Link
US (3) US7994341B2 (es)
EP (3) EP2253623B1 (es)
JP (1) JP5118043B2 (es)
CN (5) CN101277938B (es)
AR (1) AR058050A1 (es)
AU (1) AU2006291419B2 (es)
BR (1) BRPI0616238B1 (es)
CA (1) CA2622097C (es)
CL (1) CL2011000514A1 (es)
CO (1) CO6382182A2 (es)
CR (1) CR9805A (es)
EA (2) EA013638B1 (es)
EC (1) ECSP088264A (es)
ES (1) ES2397932T3 (es)
IL (2) IL189757A (es)
SG (1) SG165380A1 (es)
TW (2) TWI436984B (es)
WO (1) WO2007031323A1 (es)

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KR20050037584A (ko) * 2002-08-22 2005-04-22 신젠타 파티서페이션즈 아게 살미생물성(예를 들어, 살진균성)1,2,3-트리아졸 유도체
RU2426312C2 (ru) * 2006-04-06 2011-08-20 Синджента Партисипейшнс Аг Фунгицидные композиции
BRPI0718222A2 (pt) 2006-11-03 2018-09-04 Basf Se processo para preparar compostos, e, composto.
US7994207B2 (en) * 2006-12-21 2011-08-09 Basf Se Process for preparing fluoromethyl-substituted heterocyclic compounds
JP5876209B2 (ja) * 2007-03-16 2016-03-02 シンジェンタ リミテッド 殺微生物剤の新規な固体形態
DK2164831T3 (da) 2007-06-01 2013-10-14 Basf Se Fremgangsmåde til fremstilling af n-substituerede (3-dihalomethyl-1-methyl-pyrazol-4-yl)carboxamider
MX2009013059A (es) 2007-06-15 2010-01-15 Basf Se Procedimientos para la preparacion de compuestos de pirazol sustituidos con difluorometilo.
EP2008996A1 (en) * 2007-06-27 2008-12-31 Syngeta Participations AG Process for the production of pyrazoles
WO2009106619A1 (en) 2008-02-29 2009-09-03 Basf Se Process for preparing alkyl 2-alkoxymethylene-4,4-difluoro-3-oxobutyrates
JP5602131B2 (ja) 2008-05-02 2014-10-08 ビーエーエスエフ ソシエタス・ヨーロピア ハロゲン置換2−(アミノメチリデン)−3−オキソ酪酸エステルの製造方法
WO2009133178A1 (de) 2008-05-02 2009-11-05 Basf Se Verfahren zur herstellung von 2-(aminomethyliden)-4,4-difluor-3-oxobuttersäureestern
AU2009243550B2 (en) 2008-05-05 2014-06-26 Basf Se Method for preparing 1,3,4-substituted pyrazol compounds
ES2409605T3 (es) 2008-05-08 2013-06-27 Basf Se Procedimiento para la producción de arilcarboxamidas
EP2280944A1 (en) * 2008-05-14 2011-02-09 Syngenta Limited Process for the preparation of amides
EP2307384B1 (en) 2008-07-21 2012-04-25 Basf Se Process for preparing 1,3-disubstituted pyrazolecarboxylic esters
MX2011003758A (es) * 2008-10-27 2011-04-27 Syngenta Participations Ag Proceso para la preparacion de benzonorbornenos.
MX2011006426A (es) * 2008-12-24 2011-07-20 Syngenta Ltd Metodos para la preparacion de arilamidas.
WO2011098386A1 (en) 2010-02-09 2011-08-18 Syngenta Participations Ag Process for the preparation of an anthranilic acid derivative
WO2011131543A1 (en) 2010-04-20 2011-10-27 Syngenta Participations Ag Process for the preparation of pyrazole carboxylic acid amides
KR20130119900A (ko) * 2010-06-07 2013-11-01 다우 아그로사이언시즈 엘엘씨 살진균제로서의 피라지닐 카르복스아미드
US8309747B2 (en) * 2010-07-06 2012-11-13 Chevron Phillips Chemical Company Lp Process for synthesizing bridged cyclopentadienyl-indenyl metallocenes
EP2632901B1 (en) 2010-10-27 2018-09-12 Solvay Sa Process for the preparation of pyrazole-4-carboxamides
CN107266368A (zh) * 2010-11-15 2017-10-20 拜耳知识产权有限责任公司 5‑卤代吡唑甲酰胺
BR112013032988A2 (pt) * 2011-06-21 2016-08-16 Bayer Ip Gmbh método para a produção de pirazolilcarboxanilidas
MX348274B (es) * 2012-05-14 2017-06-02 Bayer Cropscience Ag Procedimiento de preparacion de cloruros de 1-alquil-3-fluoroalqui l-1h-pirazol-4-carbonilo.
WO2013188403A1 (en) * 2012-06-11 2013-12-19 Syngenta Participations Ag Producing solids and related mother liquors
CN104649973B (zh) 2013-11-25 2017-02-15 沈阳中化农药化工研发有限公司 一种吡唑酰胺类化合物及其用途
GB201403438D0 (en) * 2014-02-27 2014-04-16 Syngenta Participations Ag Polymorphs
EP2980078A1 (en) 2014-07-29 2016-02-03 Solvay SA Process for the preparation of pyrazole-4-carboxamides
WO2016177318A1 (zh) 2015-05-06 2016-11-10 沈阳中化农药化工研发有限公司 一种酰胺类化合物及其制备方法和用途
KR20180108695A (ko) 2016-01-28 2018-10-04 솔베이(소시에떼아노님) 할로겐 치환된 디케톤, 피라졸 화합물 및 피라졸 화합물의 제조 방법
EP3455211A1 (en) 2016-05-10 2019-03-20 Solvay SA Composition comprising 3-(haloalkyl or formyl)-1h-pyrazole-4-carboxylic acids or esters, its manufacture and its use for the preparation of carboxamides
WO2018024644A1 (en) 2016-08-02 2018-02-08 Solvay Sa Manufacture of hydrazinyl compounds useful in the manufacture of pyrazole carboxylic acid and derivatives, hydrazinyl compounds and their use
CN106279025B (zh) * 2016-08-15 2017-10-10 浙江永太科技股份有限公司 一种含吡唑环的二酯化合物及其制备方法
CN106045910B (zh) * 2016-08-15 2017-10-10 浙江永太科技股份有限公司 一种3‑(二氟甲基)‑1‑甲基‑1h‑吡唑‑4‑羧酸的合成方法
US20190276409A1 (en) 2016-11-07 2019-09-12 Solvay Sa Process for the manufacture of carboxylic acids or carboxylic acid derivatives
WO2018201272A1 (en) 2017-05-02 2018-11-08 Solvay Fluor Gmbh Process for the manufacture of carboxylic acids or carboxylic acid derivatives
US20200181091A1 (en) 2017-08-28 2020-06-11 Japan Finechem Company, Inc. Production method for pyrazole-4-carboxamide derivative
EP3495351A1 (en) 2017-12-08 2019-06-12 Solvay Sa Oxidation of a pyrazolyl ketone compound to the corresponding carboxylic acid
WO2019122164A1 (en) 2017-12-22 2019-06-27 Solvay Sa Process for the manufacture of pyrazole carboxylic derivatives and precursors thereof
CN111454157B (zh) * 2020-05-14 2022-07-22 利民化学有限责任公司 一种3-硝基苯炔的制备方法
CN112174891B (zh) * 2020-11-02 2022-02-01 浙江省农业科学院 一种氟唑菌苯胺代谢物的制备方法

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DE10228103A1 (de) 2002-06-24 2004-01-15 Bayer Cropscience Ag Fungizide Wirkstoffkombinationen
KR20050037584A (ko) * 2002-08-22 2005-04-22 신젠타 파티서페이션즈 아게 살미생물성(예를 들어, 살진균성)1,2,3-트리아졸 유도체
GB0224316D0 (en) * 2002-10-18 2002-11-27 Syngenta Participations Ag Chemical compounds
GB0422401D0 (en) * 2004-10-08 2004-11-10 Syngenta Participations Ag Fungicidal compositions
EA014297B1 (ru) * 2005-10-25 2010-10-29 Зингента Партисипейшнс Аг Гетероциклические амиды, применимые в качестве микробиоцидов

Also Published As

Publication number Publication date
EP1928838A1 (en) 2008-06-11
EP2253622A1 (en) 2010-11-24
JP5118043B2 (ja) 2013-01-16
CO6382182A2 (es) 2012-02-15
AU2006291419A1 (en) 2007-03-22
EP2253623B1 (en) 2013-10-23
EA013638B1 (ru) 2010-06-30
SG165380A1 (en) 2010-10-28
CN101979374A (zh) 2011-02-23
ES2397932T3 (es) 2013-03-12
WO2007031323A1 (en) 2007-03-22
CN101277938A (zh) 2008-10-01
BRPI0616238B1 (pt) 2016-01-19
JP2009509935A (ja) 2009-03-12
IL189757A (en) 2013-08-29
AU2006291419B2 (en) 2012-06-14
TWI436984B (zh) 2014-05-11
TW201247628A (en) 2012-12-01
CN101962364B (zh) 2013-01-09
US20130253225A1 (en) 2013-09-26
CN101979375A (zh) 2011-02-23
IL217212A0 (en) 2012-01-31
CN101962364A (zh) 2011-02-02
TW200804292A (en) 2008-01-16
CL2011000514A1 (es) 2011-05-06
CA2622097A1 (en) 2007-03-22
US7994341B2 (en) 2011-08-09
US8680337B2 (en) 2014-03-25
CN101277938B (zh) 2012-01-11
US20090163569A1 (en) 2009-06-25
EA201000345A1 (ru) 2010-06-30
US20120065239A1 (en) 2012-03-15
EP1928838B1 (en) 2012-10-24
EP2253623A1 (en) 2010-11-24
US8436037B2 (en) 2013-05-07
IL189757A0 (en) 2008-08-07
ECSP088264A (es) 2008-04-28
CA2622097C (en) 2014-04-15
BRPI0616238A2 (pt) 2011-06-14
CN101962363A (zh) 2011-02-02
EA200800840A1 (ru) 2008-08-29
AR058050A1 (es) 2008-01-23

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