ECSP088264A - Proceso para la preparación de amidas - Google Patents
Proceso para la preparación de amidasInfo
- Publication number
- ECSP088264A ECSP088264A EC2008008264A ECSP088264A ECSP088264A EC SP088264 A ECSP088264 A EC SP088264A EC 2008008264 A EC2008008264 A EC 2008008264A EC SP088264 A ECSP088264 A EC SP088264A EC SP088264 A ECSP088264 A EC SP088264A
- Authority
- EC
- Ecuador
- Prior art keywords
- formula
- compound
- reaction
- preparation
- amidas
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 3
- 150000001875 compounds Chemical class 0.000 abstract 7
- 238000006243 chemical reaction Methods 0.000 abstract 4
- 239000003638 chemical reducing agent Substances 0.000 abstract 2
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical group [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 abstract 1
- PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical group FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 abstract 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 1
- 125000003545 alkoxy group Chemical group 0.000 abstract 1
- 125000000217 alkyl group Chemical group 0.000 abstract 1
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Chemical group BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 abstract 1
- 229910052794 bromium Inorganic materials 0.000 abstract 1
- 229910052801 chlorine Inorganic materials 0.000 abstract 1
- 239000000460 chlorine Substances 0.000 abstract 1
- 125000001309 chloro group Chemical group Cl* 0.000 abstract 1
- 229910052731 fluorine Inorganic materials 0.000 abstract 1
- 239000011737 fluorine Chemical group 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- LMBFAGIMSUYTBN-MPZNNTNKSA-N teixobactin Chemical compound C([C@H](C(=O)N[C@@H]([C@@H](C)CC)C(=O)N[C@@H](CO)C(=O)N[C@H](CCC(N)=O)C(=O)N[C@H]([C@@H](C)CC)C(=O)N[C@@H]([C@@H](C)CC)C(=O)N[C@@H](CO)C(=O)N[C@H]1C(N[C@@H](C)C(=O)N[C@@H](C[C@@H]2NC(=N)NC2)C(=O)N[C@H](C(=O)O[C@H]1C)[C@@H](C)CC)=O)NC)C1=CC=CC=C1 LMBFAGIMSUYTBN-MPZNNTNKSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C211/00—Compounds containing amino groups bound to a carbon skeleton
- C07C211/43—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton
- C07C211/57—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings being part of condensed ring systems of the carbon skeleton
- C07C211/61—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings being part of condensed ring systems of the carbon skeleton with at least one of the condensed ring systems formed by three or more rings
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
- A01N43/56—1,2-Diazoles; Hydrogenated 1,2-diazoles
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C205/00—Compounds containing nitro groups bound to a carbon skeleton
- C07C205/06—Compounds containing nitro groups bound to a carbon skeleton having nitro groups bound to carbon atoms of six-membered aromatic rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/30—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds
- C07C209/32—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds by reduction of nitro groups
- C07C209/325—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds by reduction of nitro groups reduction by other means than indicated in C07C209/34 or C07C209/36
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/68—Preparation of compounds containing amino groups bound to a carbon skeleton from amines, by reactions not involving amino groups, e.g. reduction of unsaturated amines, aromatisation, or substitution of the carbon skeleton
- C07C209/70—Preparation of compounds containing amino groups bound to a carbon skeleton from amines, by reactions not involving amino groups, e.g. reduction of unsaturated amines, aromatisation, or substitution of the carbon skeleton by reduction of unsaturated amines
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
- C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
- C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2603/00—Systems containing at least three condensed rings
- C07C2603/56—Ring systems containing bridged rings
- C07C2603/58—Ring systems containing bridged rings containing three rings
- C07C2603/60—Ring systems containing bridged rings containing three rings containing at least one ring with less than six members
- C07C2603/66—Ring systems containing bridged rings containing three rings containing at least one ring with less than six members containing five-membered rings
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Agronomy & Crop Science (AREA)
- General Health & Medical Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Hydrogenated Pyridines (AREA)
Abstract
La presente invención se refiere a un proceso para la preparación de compuestos de fórmula I (I),donde R1 y R2 son cada uno de modo independiente del otro hidrógeno o alquilo C1C5 y R3 es CF3 o CF2H, mediantea) la reacción de un compuesto de fórmula II (II),donde R1 y R2 son tal como se define para la fórmula I, con al menos un agente reductor para formar un compuesto de fórmula III (III),donde R1 y R2 son tal como se define para la fórmula I; y(b) la reacción de ese compuesto con al menos un agente reductor para formar un compuesto de fórmula IV (IV),donde R1 y R2 son tal como se define para la fórmula I; y(c) la conversión de ese compuesto en el compuesto de fórmula I por medio de la reacción con un compuesto de fórmula V (V),donde Q es cloro, flúor, bromo, yodo, hidroxi o alcoxi C1C6 y R3 es como se define en la fórmula I.y a nuevos intermediarios para su uso en ese proceso.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH15202005 | 2005-09-16 | ||
| CH2962006 | 2006-02-24 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ECSP088264A true ECSP088264A (es) | 2008-04-28 |
Family
ID=37467494
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| EC2008008264A ECSP088264A (es) | 2005-09-16 | 2008-03-12 | Proceso para la preparación de amidas |
Country Status (18)
| Country | Link |
|---|---|
| US (3) | US7994341B2 (es) |
| EP (3) | EP2253623B1 (es) |
| JP (1) | JP5118043B2 (es) |
| CN (5) | CN101277938B (es) |
| AR (1) | AR058050A1 (es) |
| AU (1) | AU2006291419B2 (es) |
| BR (1) | BRPI0616238B1 (es) |
| CA (1) | CA2622097C (es) |
| CL (1) | CL2011000514A1 (es) |
| CO (1) | CO6382182A2 (es) |
| CR (1) | CR9805A (es) |
| EA (2) | EA013638B1 (es) |
| EC (1) | ECSP088264A (es) |
| ES (1) | ES2397932T3 (es) |
| IL (2) | IL189757A (es) |
| SG (1) | SG165380A1 (es) |
| TW (2) | TWI436984B (es) |
| WO (1) | WO2007031323A1 (es) |
Families Citing this family (42)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20050037584A (ko) * | 2002-08-22 | 2005-04-22 | 신젠타 파티서페이션즈 아게 | 살미생물성（예를 들어, 살진균성）1,2,3-트리아졸 유도체 |
| RU2426312C2 (ru) * | 2006-04-06 | 2011-08-20 | Синджента Партисипейшнс Аг | Фунгицидные композиции |
| BRPI0718222A2 (pt) | 2006-11-03 | 2018-09-04 | Basf Se | processo para preparar compostos, e, composto. |
| US7994207B2 (en) * | 2006-12-21 | 2011-08-09 | Basf Se | Process for preparing fluoromethyl-substituted heterocyclic compounds |
| JP5876209B2 (ja) * | 2007-03-16 | 2016-03-02 | シンジェンタ リミテッド | 殺微生物剤の新規な固体形態 |
| DK2164831T3 (da) | 2007-06-01 | 2013-10-14 | Basf Se | Fremgangsmåde til fremstilling af n-substituerede (3-dihalomethyl-1-methyl-pyrazol-4-yl)carboxamider |
| MX2009013059A (es) | 2007-06-15 | 2010-01-15 | Basf Se | Procedimientos para la preparacion de compuestos de pirazol sustituidos con difluorometilo. |
| EP2008996A1 (en) * | 2007-06-27 | 2008-12-31 | Syngeta Participations AG | Process for the production of pyrazoles |
| WO2009106619A1 (en) | 2008-02-29 | 2009-09-03 | Basf Se | Process for preparing alkyl 2-alkoxymethylene-4,4-difluoro-3-oxobutyrates |
| JP5602131B2 (ja) | 2008-05-02 | 2014-10-08 | ビーエーエスエフ ソシエタス・ヨーロピア | ハロゲン置換２−（アミノメチリデン）−３−オキソ酪酸エステルの製造方法 |
| WO2009133178A1 (de) | 2008-05-02 | 2009-11-05 | Basf Se | Verfahren zur herstellung von 2-(aminomethyliden)-4,4-difluor-3-oxobuttersäureestern |
| AU2009243550B2 (en) | 2008-05-05 | 2014-06-26 | Basf Se | Method for preparing 1,3,4-substituted pyrazol compounds |
| ES2409605T3 (es) | 2008-05-08 | 2013-06-27 | Basf Se | Procedimiento para la producción de arilcarboxamidas |
| EP2280944A1 (en) * | 2008-05-14 | 2011-02-09 | Syngenta Limited | Process for the preparation of amides |
| EP2307384B1 (en) | 2008-07-21 | 2012-04-25 | Basf Se | Process for preparing 1,3-disubstituted pyrazolecarboxylic esters |
| MX2011003758A (es) * | 2008-10-27 | 2011-04-27 | Syngenta Participations Ag | Proceso para la preparacion de benzonorbornenos. |
| MX2011006426A (es) * | 2008-12-24 | 2011-07-20 | Syngenta Ltd | Metodos para la preparacion de arilamidas. |
| WO2011098386A1 (en) | 2010-02-09 | 2011-08-18 | Syngenta Participations Ag | Process for the preparation of an anthranilic acid derivative |
| WO2011131543A1 (en) | 2010-04-20 | 2011-10-27 | Syngenta Participations Ag | Process for the preparation of pyrazole carboxylic acid amides |
| KR20130119900A (ko) * | 2010-06-07 | 2013-11-01 | 다우 아그로사이언시즈 엘엘씨 | 살진균제로서의 피라지닐 카르복스아미드 |
| US8309747B2 (en) * | 2010-07-06 | 2012-11-13 | Chevron Phillips Chemical Company Lp | Process for synthesizing bridged cyclopentadienyl-indenyl metallocenes |
| EP2632901B1 (en) | 2010-10-27 | 2018-09-12 | Solvay Sa | Process for the preparation of pyrazole-4-carboxamides |
| CN107266368A (zh) * | 2010-11-15 | 2017-10-20 | 拜耳知识产权有限责任公司 | 5‑卤代吡唑甲酰胺 |
| BR112013032988A2 (pt) * | 2011-06-21 | 2016-08-16 | Bayer Ip Gmbh | método para a produção de pirazolilcarboxanilidas |
| MX348274B (es) * | 2012-05-14 | 2017-06-02 | Bayer Cropscience Ag | Procedimiento de preparacion de cloruros de 1-alquil-3-fluoroalqui l-1h-pirazol-4-carbonilo. |
| WO2013188403A1 (en) * | 2012-06-11 | 2013-12-19 | Syngenta Participations Ag | Producing solids and related mother liquors |
| CN104649973B (zh) | 2013-11-25 | 2017-02-15 | 沈阳中化农药化工研发有限公司 | 一种吡唑酰胺类化合物及其用途 |
| GB201403438D0 (en) * | 2014-02-27 | 2014-04-16 | Syngenta Participations Ag | Polymorphs |
| EP2980078A1 (en) | 2014-07-29 | 2016-02-03 | Solvay SA | Process for the preparation of pyrazole-4-carboxamides |
| WO2016177318A1 (zh) | 2015-05-06 | 2016-11-10 | 沈阳中化农药化工研发有限公司 | 一种酰胺类化合物及其制备方法和用途 |
| KR20180108695A (ko) | 2016-01-28 | 2018-10-04 | 솔베이(소시에떼아노님) | 할로겐 치환된 디케톤, 피라졸 화합물 및 피라졸 화합물의 제조 방법 |
| EP3455211A1 (en) | 2016-05-10 | 2019-03-20 | Solvay SA | Composition comprising 3-(haloalkyl or formyl)-1h-pyrazole-4-carboxylic acids or esters, its manufacture and its use for the preparation of carboxamides |
| WO2018024644A1 (en) | 2016-08-02 | 2018-02-08 | Solvay Sa | Manufacture of hydrazinyl compounds useful in the manufacture of pyrazole carboxylic acid and derivatives, hydrazinyl compounds and their use |
| CN106279025B (zh) * | 2016-08-15 | 2017-10-10 | 浙江永太科技股份有限公司 | 一种含吡唑环的二酯化合物及其制备方法 |
| CN106045910B (zh) * | 2016-08-15 | 2017-10-10 | 浙江永太科技股份有限公司 | 一种3‑(二氟甲基)‑1‑甲基‑1h‑吡唑‑4‑羧酸的合成方法 |
| US20190276409A1 (en) | 2016-11-07 | 2019-09-12 | Solvay Sa | Process for the manufacture of carboxylic acids or carboxylic acid derivatives |
| WO2018201272A1 (en) | 2017-05-02 | 2018-11-08 | Solvay Fluor Gmbh | Process for the manufacture of carboxylic acids or carboxylic acid derivatives |
| US20200181091A1 (en) | 2017-08-28 | 2020-06-11 | Japan Finechem Company, Inc. | Production method for pyrazole-4-carboxamide derivative |
| EP3495351A1 (en) | 2017-12-08 | 2019-06-12 | Solvay Sa | Oxidation of a pyrazolyl ketone compound to the corresponding carboxylic acid |
| WO2019122164A1 (en) | 2017-12-22 | 2019-06-27 | Solvay Sa | Process for the manufacture of pyrazole carboxylic derivatives and precursors thereof |
| CN111454157B (zh) * | 2020-05-14 | 2022-07-22 | 利民化学有限责任公司 | 一种3-硝基苯炔的制备方法 |
| CN112174891B (zh) * | 2020-11-02 | 2022-02-01 | 浙江省农业科学院 | 一种氟唑菌苯胺代谢物的制备方法 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE10228103A1 (de) | 2002-06-24 | 2004-01-15 | Bayer Cropscience Ag | Fungizide Wirkstoffkombinationen |
| KR20050037584A (ko) * | 2002-08-22 | 2005-04-22 | 신젠타 파티서페이션즈 아게 | 살미생물성（예를 들어, 살진균성）1,2,3-트리아졸 유도체 |
| GB0224316D0 (en) * | 2002-10-18 | 2002-11-27 | Syngenta Participations Ag | Chemical compounds |
| GB0422401D0 (en) * | 2004-10-08 | 2004-11-10 | Syngenta Participations Ag | Fungicidal compositions |
| EA014297B1 (ru) * | 2005-10-25 | 2010-10-29 | Зингента Партисипейшнс Аг | Гетероциклические амиды, применимые в качестве микробиоцидов |
-
2006
- 2006-09-14 EA EA200800840A patent/EA013638B1/ru not_active IP Right Cessation
- 2006-09-14 CN CN2006800365540A patent/CN101277938B/zh not_active Expired - Fee Related
- 2006-09-14 EP EP10175067.7A patent/EP2253623B1/en not_active Not-in-force
- 2006-09-14 TW TW101130220A patent/TWI436984B/zh not_active IP Right Cessation
- 2006-09-14 CN CN2010105057332A patent/CN101979374A/zh active Pending
- 2006-09-14 CN CN2010105057313A patent/CN101962363A/zh active Pending
- 2006-09-14 EP EP06805725A patent/EP1928838B1/en not_active Not-in-force
- 2006-09-14 SG SG201006670-2A patent/SG165380A1/en unknown
- 2006-09-14 CN CN2010105056984A patent/CN101979375A/zh active Pending
- 2006-09-14 CA CA2622097A patent/CA2622097C/en not_active Expired - Fee Related
- 2006-09-14 TW TW095133966A patent/TW200804292A/zh unknown
- 2006-09-14 US US12/066,683 patent/US7994341B2/en active Active
- 2006-09-14 ES ES06805725T patent/ES2397932T3/es active Active
- 2006-09-14 BR BRPI0616238A patent/BRPI0616238B1/pt not_active IP Right Cessation
- 2006-09-14 EP EP10175064A patent/EP2253622A1/en not_active Withdrawn
- 2006-09-14 AU AU2006291419A patent/AU2006291419B2/en not_active Ceased
- 2006-09-14 WO PCT/EP2006/008982 patent/WO2007031323A1/en not_active Ceased
- 2006-09-14 CN CN2010105057366A patent/CN101962364B/zh not_active Expired - Fee Related
- 2006-09-14 EA EA201000345A patent/EA201000345A1/ru unknown
- 2006-09-14 JP JP2008530418A patent/JP5118043B2/ja not_active Expired - Fee Related
- 2006-09-15 AR ARP060104046A patent/AR058050A1/es not_active Application Discontinuation
-
2008
- 2008-02-25 IL IL189757A patent/IL189757A/en not_active IP Right Cessation
- 2008-03-07 CR CR9805A patent/CR9805A/es unknown
- 2008-03-12 EC EC2008008264A patent/ECSP088264A/es unknown
- 2008-04-16 CO CO08038479A patent/CO6382182A2/es not_active Application Discontinuation
-
2011
- 2011-03-10 CL CL2011000514A patent/CL2011000514A1/es unknown
- 2011-08-05 US US13/198,739 patent/US8436037B2/en not_active Expired - Fee Related
- 2011-12-26 IL IL217212A patent/IL217212A0/en unknown
-
2013
- 2013-05-07 US US13/889,041 patent/US8680337B2/en active Active
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