CS199722B2 - Způsob výroby tetrabromdianu - Google Patents

Způsob výroby tetrabromdianu Download PDF

Info

Publication number: CS199722B2
Authority: CS; Czechoslovakia
Prior art keywords: bromine; hydroxyphenyl; propane; reaction; solvent
Prior art date: 1977-03-28

Application number

CS172778A

Other languages

Czech (cs)

English (en)

Inventor

Alina Kowalska-Kiedik

Zdzislaw Janowski

Edward Grzywa

Zenon Schneider

Maciej Kiedik

Gerhard Bekierz

Marian Sosnowski

Original Assignee

Inst Ciezkiej Syntezy Orga

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1977-03-28

Filing date

1978-03-17

Publication date

1980-07-31

1978-03-17 Application filed by Inst Ciezkiej Syntezy Orga filed Critical Inst Ciezkiej Syntezy Orga

1980-07-31 Publication of CS199722B2 publication Critical patent/CS199722B2/cs

Links

238000004519 manufacturing process Methods 0.000 title claims description 4
WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 claims description 27
GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 claims description 27
229910052794 bromium Inorganic materials 0.000 claims description 27
239000002904 solvent Substances 0.000 claims description 23
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 18
238000006243 chemical reaction Methods 0.000 claims description 16
VEORPZCZECFIRK-UHFFFAOYSA-N 3,3',5,5'-tetrabromobisphenol A Chemical compound C=1C(Br)=C(O)C(Br)=CC=1C(C)(C)C1=CC(Br)=C(O)C(Br)=C1 VEORPZCZECFIRK-UHFFFAOYSA-N 0.000 claims description 15
238000000034 method Methods 0.000 claims description 15
239000000203 mixture Substances 0.000 claims description 14
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 12
RWYFURDDADFSHT-RBBHPAOJSA-N diane Chemical compound OC1=CC=C2[C@H]3CC[C@](C)([C@](CC4)(O)C#C)[C@@H]4[C@@H]3CCC2=C1.C1=C(Cl)C2=CC(=O)[C@@H]3CC3[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@@](C(C)=O)(OC(=O)C)[C@@]1(C)CC2 RWYFURDDADFSHT-RBBHPAOJSA-N 0.000 claims description 10
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
239000011541 reaction mixture Substances 0.000 claims description 6
ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims description 5
230000015572 biosynthetic process Effects 0.000 claims description 5
230000031709 bromination Effects 0.000 claims description 5
238000005893 bromination reaction Methods 0.000 claims description 5
239000007787 solid Substances 0.000 claims description 5
238000003786 synthesis reaction Methods 0.000 claims description 5
239000007800 oxidant agent Substances 0.000 claims description 4
239000006227 byproduct Substances 0.000 claims description 3
239000000047 product Substances 0.000 description 18
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 14
ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 9
239000000460 chlorine Substances 0.000 description 9
229910052801 chlorine Inorganic materials 0.000 description 9
ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 6
239000012452 mother liquor Substances 0.000 description 6
229960000583 acetic acid Drugs 0.000 description 5
239000004033 plastic Substances 0.000 description 3
229920003023 plastic Polymers 0.000 description 3
239000001294 propane Substances 0.000 description 3
239000012209 synthetic fiber Substances 0.000 description 3
229920002994 synthetic fiber Polymers 0.000 description 3
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
239000000654 additive Substances 0.000 description 2
230000000996 additive effect Effects 0.000 description 2
IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 2
-1 bromo hydrogen Chemical compound 0.000 description 2
IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 2
229910000041 hydrogen chloride Inorganic materials 0.000 description 2
238000006386 neutralization reaction Methods 0.000 description 2
238000000926 separation method Methods 0.000 description 2
FNAKEOXYWBWIRT-UHFFFAOYSA-N 2,3-dibromophenol Chemical class OC1=CC=CC(Br)=C1Br FNAKEOXYWBWIRT-UHFFFAOYSA-N 0.000 description 1
125000004203 4-hydroxyphenyl group Chemical group [H]OC1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
238000010521 absorption reaction Methods 0.000 description 1
125000001246 bromo group Chemical class Br* 0.000 description 1
125000004432 carbon atom Chemical group C* 0.000 description 1
239000003795 chemical substances by application Substances 0.000 description 1
238000005660 chlorination reaction Methods 0.000 description 1
238000002485 combustion reaction Methods 0.000 description 1
230000000052 comparative effect Effects 0.000 description 1
238000004821 distillation Methods 0.000 description 1
239000000706 filtrate Substances 0.000 description 1
238000001914 filtration Methods 0.000 description 1
239000012467 final product Substances 0.000 description 1
239000012362 glacial acetic acid Substances 0.000 description 1
239000001257 hydrogen Substances 0.000 description 1
229910052739 hydrogen Inorganic materials 0.000 description 1
239000011261 inert gas Substances 0.000 description 1
238000011835 investigation Methods 0.000 description 1
238000000746 purification Methods 0.000 description 1
230000035484 reaction time Effects 0.000 description 1
238000001953 recrystallisation Methods 0.000 description 1
238000003756 stirring Methods 0.000 description 1
239000000725 suspension Substances 0.000 description 1

Landscapes

Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

CS172778A 1977-03-28 1978-03-17 Způsob výroby tetrabromdianu CS199722B2 (cs)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
PL19697677A PL112444B1 (en)	1977-03-28	1977-03-28	Method of tetrabromodian preparation

Publications (1)

Publication Number	Publication Date
CS199722B2 true CS199722B2 (cs)	1980-07-31

Family

ID=19981645

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CS172778A CS199722B2 (cs)	1977-03-28	1978-03-17	Způsob výroby tetrabromdianu

Country Status (3)

Country	Link
CS (1)	CS199722B2 (pl)
DD (1)	DD134515A5 (pl)
PL (1)	PL112444B1 (pl)

1977
- 1977-03-28 PL PL19697677A patent/PL112444B1/pl not_active IP Right Cessation
1978
- 1978-03-17 CS CS172778A patent/CS199722B2/cs unknown
- 1978-03-23 DD DD20438078A patent/DD134515A5/xx unknown

Also Published As

Publication number	Publication date
PL196976A1 (pl)	1978-12-04
DD134515A5 (de)	1979-03-07
PL112444B1 (en)	1980-10-31

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