CS244802B2 - Copper catalysed reaction substance and method of its production - Google Patents

Copper catalysed reaction substance and method of its production Download PDF

Info

Publication number: CS244802B2
Authority: CS; Czechoslovakia
Prior art keywords: copper; silicon; reaction mass; mixture; less
Prior art date: 1979-10-24

Application number

CS807189A

Other languages

Czech (cs)

English (en)

Inventor

James H Downing

E James

Tom K Ioannou

Original Assignee

Elkem Metals

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1979-10-24

Filing date

1980-10-23

Publication date

1986-08-14

1980-10-23 Application filed by Elkem Metals filed Critical Elkem Metals

1986-08-14 Publication of CS244802B2 publication Critical patent/CS244802B2/cs

Links

RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 title claims abstract description 47
239000010949 copper Substances 0.000 title claims abstract description 43
229910052802 copper Inorganic materials 0.000 title claims abstract description 41
238000004519 manufacturing process Methods 0.000 title claims abstract description 15
238000000034 method Methods 0.000 title claims description 9
238000006555 catalytic reaction Methods 0.000 title claims 2
239000000126 substance Substances 0.000 title description 2
238000006243 chemical reaction Methods 0.000 claims abstract description 35
XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims abstract description 30
229910052710 silicon Inorganic materials 0.000 claims abstract description 27
239000010703 silicon Substances 0.000 claims abstract description 27
239000002245 particle Substances 0.000 claims abstract description 19
229910000676 Si alloy Inorganic materials 0.000 claims abstract description 10
WCCJDBZJUYKDBF-UHFFFAOYSA-N copper silicon Chemical compound [Si].[Cu] WCCJDBZJUYKDBF-UHFFFAOYSA-N 0.000 claims abstract description 9
239000000843 powder Substances 0.000 claims abstract description 8
230000003197 catalytic effect Effects 0.000 claims abstract description 3
239000003054 catalyst Substances 0.000 claims description 15
239000000203 mixture Substances 0.000 claims description 11
238000010438 heat treatment Methods 0.000 claims description 4
229910045601 alloy Inorganic materials 0.000 claims description 3
239000000956 alloy Substances 0.000 claims description 3
-1 methanol chlorosilanes Chemical class 0.000 claims description 2
238000002360 preparation method Methods 0.000 claims description 2
HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims 6
229910052725 zinc Inorganic materials 0.000 claims 4
239000011701 zinc Substances 0.000 claims 4
BERDEBHAJNAUOM-UHFFFAOYSA-N copper(I) oxide Inorganic materials [Cu]O[Cu] BERDEBHAJNAUOM-UHFFFAOYSA-N 0.000 claims 3
KRFJLUBVMFXRPN-UHFFFAOYSA-N cuprous oxide Chemical compound [O-2].[Cu+].[Cu+] KRFJLUBVMFXRPN-UHFFFAOYSA-N 0.000 claims 2
229940112669 cuprous oxide Drugs 0.000 claims 2
239000011541 reaction mixture Substances 0.000 claims 2
ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims 1
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims 1
229910052787 antimony Inorganic materials 0.000 claims 1
WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 claims 1
229910052785 arsenic Inorganic materials 0.000 claims 1
RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 claims 1
230000015572 biosynthetic process Effects 0.000 claims 1
229910052797 bismuth Inorganic materials 0.000 claims 1
JCXGWMGPZLAOME-UHFFFAOYSA-N bismuth atom Chemical compound [Bi] JCXGWMGPZLAOME-UHFFFAOYSA-N 0.000 claims 1
239000004568 cement Substances 0.000 claims 1
239000000460 chlorine Substances 0.000 claims 1
229910052801 chlorine Inorganic materials 0.000 claims 1
229940108928 copper Drugs 0.000 claims 1
239000001257 hydrogen Substances 0.000 claims 1
229910052739 hydrogen Inorganic materials 0.000 claims 1
239000012535 impurity Substances 0.000 claims 1
239000002184 metal Substances 0.000 claims 1
229910052751 metal Inorganic materials 0.000 claims 1
239000003595 mist Substances 0.000 claims 1
239000002105 nanoparticle Substances 0.000 claims 1
239000007921 spray Substances 0.000 claims 1
YGZSVWMBUCGDCV-UHFFFAOYSA-N chloro(methyl)silane Chemical compound C[SiH2]Cl YGZSVWMBUCGDCV-UHFFFAOYSA-N 0.000 abstract description 8
239000011856 silicon-based particle Substances 0.000 abstract description 5
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
NEHMKBQYUWJMIP-UHFFFAOYSA-N chloromethane Chemical compound ClC NEHMKBQYUWJMIP-UHFFFAOYSA-N 0.000 description 2
239000000178 monomer Substances 0.000 description 2
239000011863 silicon-based powder Substances 0.000 description 2
239000007787 solid Substances 0.000 description 2
239000004215 Carbon black (E152) Substances 0.000 description 1
239000004927 clay Substances 0.000 description 1
150000004820 halides Chemical class 0.000 description 1
229930195733 hydrocarbon Natural products 0.000 description 1
229940050176 methyl chloride Drugs 0.000 description 1
239000008188 pellet Substances 0.000 description 1
229920001296 polysiloxane Polymers 0.000 description 1
SBEQWOXEGHQIMW-UHFFFAOYSA-N silicon Chemical compound [Si].[Si] SBEQWOXEGHQIMW-UHFFFAOYSA-N 0.000 description 1
239000000377 silicon dioxide Substances 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
- C07F7/12—Organo silicon halides
- C07F7/16—Preparation thereof from silicon and halogenated hydrocarbons direct synthesis

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Catalysts (AREA)
Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

CS807189A 1979-10-24 1980-10-23 Copper catalysed reaction substance and method of its production CS244802B2 (en)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
US06/087,798 US4314908A (en)	1979-10-24	1979-10-24	Preparation of reaction mass for the production of methylchlorosilane

Publications (1)

Publication Number	Publication Date
CS244802B2 true CS244802B2 (en)	1986-08-14

Family

ID=22207326

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CS807189A CS244802B2 (en)	1979-10-24	1980-10-23	Copper catalysed reaction substance and method of its production

Country Status (8)

Country	Link
US (1)	US4314908A (de)
EP (1)	EP0028009B1 (de)
JP (1)	JPS5948139B2 (de)
AT (1)	ATE13537T1 (de)
CA (1)	CA1158629A (de)
CS (1)	CS244802B2 (de)
DE (1)	DE3070708D1 (de)
SU (1)	SU1526580A3 (de)

Families Citing this family (37)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US4487950A (en) *	1982-04-16	1984-12-11	General Electric Company	Method for making methylchlorosilanes
GB2127032A (en) *	1982-09-17	1984-04-04	Gen Electric	A catalyst for a process for producing silicones
JPS5955891A (ja) *	1982-09-27	1984-03-31	ゼネラル・エレクトリツク・カンパニイ	改良触媒によるオルガノハロシランの製法
US4500724A (en) *	1983-07-28	1985-02-19	General Electric Company	Method for making alkylhalosilanes
USRE33452E (en) *	1983-07-28	1990-11-20	General Electric Company	Method for making alkylhalosilanes
US4504597A (en) *	1983-11-04	1985-03-12	Scm Corporation	Cupreous catalyst and process making same
GB2153697B (en) *	1984-02-13	1988-04-27	Gen Electric	Catalysts for the production of organohalosilanes
US4520130A (en) *	1984-05-08	1985-05-28	Scm Corporation	Halosilane catalyst and process for making same
US4593114A (en) *	1984-09-13	1986-06-03	Union Carbide Corporation	Direct process for preparing dimethylsiloxanes
US4864044A (en) *	1985-02-15	1989-09-05	Union Carbide Corporation	Tin containing activated silicon for the direct reaction
US4602101A (en) *	1985-11-12	1986-07-22	Dow Corning Corporation	Method of manufacturing alkylhalosilanes
US4762940A (en) *	1987-12-11	1988-08-09	Dow Corning Corporation	Method for preparation of alkylhalosilanes
US4973725A (en) *	1988-06-28	1990-11-27	Union Carbide Chemicals And Plastics Company Inc.	Direct synthesis process for organohalohydrosilanes
GB8910967D0 (en) *	1989-05-12	1989-06-28	Univ Leicester	Abstracting electronegative elements from heteromolecules
US5061672A (en) *	1990-01-30	1991-10-29	Elkem Metals Company	Active mass for making organohalosilanes
US5250716A (en) *	1992-05-28	1993-10-05	Mui Jeffrey Y P	Method for making a silicon/copper contact mass suitable for direct reaction
US5243061A (en) *	1992-12-09	1993-09-07	General Electric Company	Method for making organohalosilanes
US5281739A (en) *	1992-12-23	1994-01-25	Dow Corning Corporation	Process for manufacture of alkylhalosilanes
US5783720A (en)	1996-10-10	1998-07-21	Osi Specialties, Inc.	Surface-active additives in the direct synthesis of trialkoxysilanes
JPH1111926A (ja) *	1997-06-20	1999-01-19	Mitsui Chem Inc	銅−珪素合金が珪素粉末表面に高度に分散した珪素粉末及びその製造方法
US6156380A (en) *	1998-10-05	2000-12-05	Shin-Etsu Chemical Co., Ltd.	Method for preparing contact mass for organohalosilane synthesis
US6528674B1 (en)	2000-04-20	2003-03-04	General Electric Company	Method for preparing a contact mass
DE10044796A1 (de) *	2000-09-11	2002-04-04	Bayer Ag	Verfahren zur Herstellung von Chlorsilanen
JP4813545B2 (ja) *	2005-03-09	2011-11-09	アールイーシーシリコンインコーポレイテッド	ヒドロクロロシランの製造方法
KR20120124061A (ko)	2010-01-26	2012-11-12	다우 코닝 코포레이션	오가노할로실란의 제조 방법
US8722915B2 (en) *	2010-05-28	2014-05-13	Dow Corning Corporation	Preparation of organohalosilanes
KR101839585B1 (ko) *	2010-05-28	2018-03-16	다우 코닝 코포레이션	디오가노디할로실란의 제조 방법
US8765090B2 (en)	2010-09-08	2014-07-01	Dow Corning Corporation	Method for preparing a trihalosilane
JP2014501243A (ja)	2010-12-17	2014-01-20	ダウコーニングコーポレーション	ジオルガノジハロシランの製造方法
USRE46657E1 (en)	2010-12-17	2018-01-02	Dow Corning Corporation	Method of making a trihalosilane
AU2012209345A1 (en) *	2011-01-25	2013-06-13	Dow Corning Corporation	Method of preparing a diorganodihalosilane
KR101422080B1 (ko)	2011-09-06	2014-07-22	인스티튜트 오브 아이온-플라즈마엔드 레이저 테크놀러지스	트리알콕시실란의 제조방법
JP2015524824A (ja)	2012-08-13	2015-08-27	ダウコーニングコーポレーションＤｏｗＣｏｒｎｉｎｇＣｏｒｐｏｒａｔｉｏｎ	銅触媒上での２工程プロセスで水素、ハロシラン、及び有機ハロゲン化物を反応させることによって、オルガノハロシランを調製する方法
JP6125646B2 (ja)	2012-10-16	2017-05-10	ダウコーニングコーポレーションＤｏｗＣｏｒｎｉｎｇＣｏｒｐｏｒａｔｉｏｎ	ハロゲン化シラヒドロカルビレンの調製方法
CN105705507B (zh)	2013-11-12	2018-08-31	美国陶氏有机硅公司	制备卤代硅烷的方法
KR101616043B1 (ko)	2014-07-22	2016-04-27	한화케미칼 주식회사	삼염화실란의 제조방법
JP6725510B2 (ja)	2014-12-18	2020-07-22	ダウシリコーンズコーポレーション	アリール官能性シランの製造方法

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US2380996A (en) *	1941-09-26	1945-08-07	Gen Electric	Preparation of organosilicon halides
US2449821A (en) *	1945-12-08	1948-09-21	Gen Electric	Method for preparing organosilicon compounds
US2686194A (en) *	1951-05-31	1954-08-10	Kellogg M W Co	Organosilicon compounds
US3069452A (en) *	1959-01-26	1962-12-18	Goldschmidt Ag Th	Process for the production of a silane mixture
FR1545407A (fr) *	1966-11-28	1968-11-08	Midland Silicones Ltd	Procédé de préparation d'organohalosilanes

1979
- 1979-10-24 US US06/087,798 patent/US4314908A/en not_active Expired - Lifetime
1980
- 1980-08-22 CA CA000358871A patent/CA1158629A/en not_active Expired
- 1980-10-23 CS CS807189A patent/CS244802B2/cs unknown
- 1980-10-23 SU SU802998452A patent/SU1526580A3/ru active
- 1980-10-23 JP JP55148867A patent/JPS5948139B2/ja not_active Expired
- 1980-10-23 AT AT80106464T patent/ATE13537T1/de not_active IP Right Cessation
- 1980-10-23 DE DE8080106464T patent/DE3070708D1/de not_active Expired
- 1980-10-23 EP EP80106464A patent/EP0028009B1/de not_active Expired

Also Published As

Publication number	Publication date
EP0028009A2 (de)	1981-05-06
ATE13537T1 (de)	1985-06-15
CA1158629A (en)	1983-12-13
EP0028009B1 (de)	1985-05-29
JPS5673544A (en)	1981-06-18
JPS5948139B2 (ja)	1984-11-24
EP0028009A3 (en)	1982-05-26
SU1526580A3 (ru)	1989-11-30
DE3070708D1 (en)	1985-07-04
US4314908A (en)	1982-02-09

Publication	Publication Date	Title
CS244802B2 (en)	1986-08-14	Copper catalysed reaction substance and method of its production
US6057469A (en)	2000-05-02	Process for manufacturing active silicon powder for the preparation of alkyl- or aryl-halosilanes
EP0223447B1 (de)	1994-02-09	Verfahren zur Herstellung von Alkylhalosilanen
FI77460C (fi)	1989-03-10	Foerfarande och alkali som tillsatsmedel innehaollande katalysator foer direkt syntes av dimetyl-diklorsilan.
EP0273635B1 (de)	1993-02-10	Verfahren zur Herstellung von Alkylhalosilanen
CA1310466C (en)	1992-11-24	Method of direct process performance improvement via control of silicon manufacture
KR20020093931A (ko)	2002-12-16	접촉괴의 제조방법
EP0411645B1 (de)	1995-05-31	Verfahren zur Herstellung von Organohalogensilanen
JPH0480740B2 (de)	1992-12-21
CN1834098B (zh)	2010-06-16	有机卤代硅烷的制备
JP3775467B2 (ja)	2006-05-17	オルガノハロシランの製造方法
US4487950A (en)	1984-12-11	Method for making methylchlorosilanes
JPH04305582A (ja)	1992-10-28	メチルジクロロシランの収率増加方法
US6423860B1 (en)	2002-07-23	Method for promoting dialkyldihalosilane formation during direct method alkylhalosilane production
TW200400157A (en)	2004-01-01	Method for preparing a contact mass
JPH11228580A (ja)	1999-08-24	アルキルまたはアリール・ハロシランの調製のための活性珪素粉末及びその製造方法
KR100785673B1 (ko)	2007-12-14	알킬할로게노실란의 직접 합성을 위한 촉매 시스템 및 방법
Luo et al.	2006	Effect of copper content on the direct process of organosilane synthesis from silicon and methyl chloride
JP2000226208A (ja)	2000-08-15	アルキル―またはアリル―ハロゲンシランの調製のための活性珪素粉末及びその製造方法
JPH04297483A (ja)	1992-10-21	オルガノハロシラン類の調製方法
KR100785674B1 (ko)	2007-12-14	알킬할로실란의 직접 합성을 위한 구리, 인 및 알칼리 금속기재 촉매 조성물
EP0514034B1 (de)	1996-02-28	Silan-Verbindungen aus der Reaktion von festem Siliziummonoxid mit aromatischen Halogenverbindungen