CS246515B1 - Production method of dihydrate and/or waterless hydrogenphosphate - Google Patents

Production method of dihydrate and/or waterless hydrogenphosphate Download PDF

Info

Publication number: CS246515B1
Authority: CS; Czechoslovakia
Prior art keywords: ammonia; solution; ammonium; chloride; phosphate
Prior art date: 1984-05-25

Application number

CS393584A

Other languages

Czech (cs)

English (en)

Inventor

Vladimir Glaser

Jan Vidensky

Original Assignee

Vladimir Glaser

Jan Vidensky

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1984-05-25

Filing date

1984-05-25

Publication date

1986-10-16

1984-05-25 Application filed by Vladimir Glaser, Jan Vidensky filed Critical Vladimir Glaser

1984-05-25 Priority to CS393584A priority Critical patent/CS246515B1/cs

1985-04-15 Priority to BG6974985A priority patent/BG45758A1/xx

1985-04-17 Priority to DD27522285A priority patent/DD255443A3/de

1985-04-17 Priority to SU857773811A priority patent/SU1518298A1/ru

1985-05-08 Priority to NL8501303A priority patent/NL8501303A/nl

1985-05-15 Priority to DE19853517608 priority patent/DE3517608A1/de

1985-05-17 Priority to GB08512556A priority patent/GB2159510B/en

1985-05-20 Priority to FR8507570A priority patent/FR2564817B1/fr

1985-05-24 Priority to IT20868/85A priority patent/IT1183673B/it

1985-05-24 Priority to YU00875/85A priority patent/YU87585A/xx

1985-05-24 Priority to HU851997A priority patent/HU201496B/hu

1986-10-16 Publication of CS246515B1 publication Critical patent/CS246515B1/cs

Links

238000004519 manufacturing process Methods 0.000 title claims description 20
150000004683 dihydrates Chemical class 0.000 title claims description 6
NBIIXXVUZAFLBC-UHFFFAOYSA-L Phosphate ion(2-) Chemical compound OP([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-L 0.000 title description 2
QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 39
239000000243 solution Substances 0.000 claims description 29
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 24
229910021529 ammonia Inorganic materials 0.000 claims description 19
239000000047 product Substances 0.000 claims description 18
238000000034 method Methods 0.000 claims description 17
NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 claims description 14
UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 claims description 11
FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 10
239000002244 precipitate Substances 0.000 claims description 10
VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 claims description 9
239000000908 ammonium hydroxide Substances 0.000 claims description 9
239000001110 calcium chloride Substances 0.000 claims description 9
229910001628 calcium chloride Inorganic materials 0.000 claims description 9
239000002253 acid Substances 0.000 claims description 8
239000000203 mixture Substances 0.000 claims description 8
238000011084 recovery Methods 0.000 claims description 8
CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 7
235000019270 ammonium chloride Nutrition 0.000 claims description 7
NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 6
239000011780 sodium chloride Substances 0.000 claims description 5
239000000725 suspension Substances 0.000 claims description 5
FUFJGUQYACFECW-UHFFFAOYSA-L calcium hydrogenphosphate Chemical compound [Ca+2].OP([O-])([O-])=O FUFJGUQYACFECW-UHFFFAOYSA-L 0.000 claims description 4
239000001506 calcium phosphate Substances 0.000 claims description 4
235000019739 Dicalciumphosphate Nutrition 0.000 claims description 3
229910000147 aluminium phosphate Inorganic materials 0.000 claims description 3
NEFBYIFKOOEVPA-UHFFFAOYSA-K dicalcium phosphate Chemical compound [Ca+2].[Ca+2].[O-]P([O-])([O-])=O NEFBYIFKOOEVPA-UHFFFAOYSA-K 0.000 claims description 3
229910000390 dicalcium phosphate Inorganic materials 0.000 claims description 3
229940038472 dicalcium phosphate Drugs 0.000 claims description 3
239000003381 stabilizer Substances 0.000 claims description 3
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
229910019142 PO4 Inorganic materials 0.000 claims description 2
LFVGISIMTYGQHF-UHFFFAOYSA-N ammonium dihydrogen phosphate Chemical compound [NH4+].OP(O)([O-])=O LFVGISIMTYGQHF-UHFFFAOYSA-N 0.000 claims description 2
229910000387 ammonium dihydrogen phosphate Inorganic materials 0.000 claims description 2
229910000389 calcium phosphate Inorganic materials 0.000 claims description 2
230000018044 dehydration Effects 0.000 claims description 2
238000006297 dehydration reaction Methods 0.000 claims description 2
MNNHAPBLZZVQHP-UHFFFAOYSA-N diammonium hydrogen phosphate Chemical compound [NH4+].[NH4+].OP([O-])([O-])=O MNNHAPBLZZVQHP-UHFFFAOYSA-N 0.000 claims description 2
238000010790 dilution Methods 0.000 claims description 2
239000012895 dilution Substances 0.000 claims description 2
230000007062 hydrolysis Effects 0.000 claims description 2
238000006460 hydrolysis reaction Methods 0.000 claims description 2
235000019837 monoammonium phosphate Nutrition 0.000 claims description 2
NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims description 2
239000010452 phosphate Substances 0.000 claims description 2
238000000746 purification Methods 0.000 claims description 2
VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims 2
229910000019 calcium carbonate Inorganic materials 0.000 claims 1
235000011010 calcium phosphates Nutrition 0.000 claims 1
229910052588 hydroxylapatite Inorganic materials 0.000 claims 1
XYJRXVWERLGGKC-UHFFFAOYSA-D pentacalcium;hydroxide;triphosphate Chemical compound [OH-].[Ca+2].[Ca+2].[Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O XYJRXVWERLGGKC-UHFFFAOYSA-D 0.000 claims 1
238000002360 preparation method Methods 0.000 claims 1
QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 claims 1
238000001556 precipitation Methods 0.000 description 5
239000002699 waste material Substances 0.000 description 5
239000000654 additive Substances 0.000 description 3
238000001914 filtration Methods 0.000 description 3
238000010438 heat treatment Methods 0.000 description 3
TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 description 2
ARLZGEXVMUDUQZ-UHFFFAOYSA-N O.O.[Ca] Chemical compound O.O.[Ca] ARLZGEXVMUDUQZ-UHFFFAOYSA-N 0.000 description 2
230000000996 additive effect Effects 0.000 description 2
238000009835 boiling Methods 0.000 description 2
239000002537 cosmetic Substances 0.000 description 2
238000005516 engineering process Methods 0.000 description 2
239000000706 filtrate Substances 0.000 description 2
235000013305 food Nutrition 0.000 description 2
235000008733 Citrus aurantifolia Nutrition 0.000 description 1
OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
235000011941 Tilia x europaea Nutrition 0.000 description 1
230000015572 biosynthetic process Effects 0.000 description 1
239000006227 byproduct Substances 0.000 description 1
YYRMJZQKEFZXMX-UHFFFAOYSA-L calcium bis(dihydrogenphosphate) Chemical compound [Ca+2].OP(O)([O-])=O.OP(O)([O-])=O YYRMJZQKEFZXMX-UHFFFAOYSA-L 0.000 description 1
229940062672 calcium dihydrogen phosphate Drugs 0.000 description 1
AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 1
XAAHAAMILDNBPS-UHFFFAOYSA-L calcium hydrogenphosphate dihydrate Chemical compound O.O.[Ca+2].OP([O-])([O-])=O XAAHAAMILDNBPS-UHFFFAOYSA-L 0.000 description 1
239000000920 calcium hydroxide Substances 0.000 description 1
229910001861 calcium hydroxide Inorganic materials 0.000 description 1
BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 1
239000000292 calcium oxide Substances 0.000 description 1
ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 1
238000005119 centrifugation Methods 0.000 description 1
238000006243 chemical reaction Methods 0.000 description 1
150000001875 compounds Chemical class 0.000 description 1
238000001816 cooling Methods 0.000 description 1
235000019700 dicalcium phosphate Nutrition 0.000 description 1
229940095079 dicalcium phosphate anhydrous Drugs 0.000 description 1
BNIILDVGGAEEIG-UHFFFAOYSA-L disodium hydrogen phosphate Chemical compound [Na+].[Na+].OP([O-])([O-])=O BNIILDVGGAEEIG-UHFFFAOYSA-L 0.000 description 1
229910000397 disodium phosphate Inorganic materials 0.000 description 1
235000019800 disodium phosphate Nutrition 0.000 description 1
230000000694 effects Effects 0.000 description 1
238000000227 grinding Methods 0.000 description 1
239000012535 impurity Substances 0.000 description 1
239000004571 lime Substances 0.000 description 1
229910001629 magnesium chloride Inorganic materials 0.000 description 1
239000008267 milk Substances 0.000 description 1
210000004080 milk Anatomy 0.000 description 1
235000013336 milk Nutrition 0.000 description 1
235000019691 monocalcium phosphate Nutrition 0.000 description 1
239000002245 particle Substances 0.000 description 1
239000011574 phosphorus Substances 0.000 description 1
229910052698 phosphorus Inorganic materials 0.000 description 1
230000008929 regeneration Effects 0.000 description 1
238000011069 regeneration method Methods 0.000 description 1
238000000926 separation method Methods 0.000 description 1
FQENQNTWSFEDLI-UHFFFAOYSA-J sodium diphosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])([O-])=O FQENQNTWSFEDLI-UHFFFAOYSA-J 0.000 description 1
239000001488 sodium phosphate Substances 0.000 description 1
229910000162 sodium phosphate Inorganic materials 0.000 description 1
235000011008 sodium phosphates Nutrition 0.000 description 1
229940048086 sodium pyrophosphate Drugs 0.000 description 1
HUAUNKAZQWMVFY-UHFFFAOYSA-M sodium;oxocalcium;hydroxide Chemical compound [OH-].[Na+].[Ca]=O HUAUNKAZQWMVFY-UHFFFAOYSA-M 0.000 description 1
239000007858 starting material Substances 0.000 description 1
235000019818 tetrasodium diphosphate Nutrition 0.000 description 1
239000001577 tetrasodium phosphonato phosphate Substances 0.000 description 1
RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 description 1
238000005406 washing Methods 0.000 description 1

Landscapes

Cosmetics (AREA)
Coloring Foods And Improving Nutritive Qualities (AREA)
Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

CS393584A 1984-05-25 1984-05-25 Production method of dihydrate and/or waterless hydrogenphosphate CS246515B1 (en)

Priority Applications (11)

Application Number	Priority Date	Filing Date	Title
CS393584A CS246515B1 (en)	1984-05-25	1984-05-25	Production method of dihydrate and/or waterless hydrogenphosphate
BG6974985A BG45758A1 (en)	1984-05-25	1985-04-15	Method for preparing of dihydrate and/or waterless hydrogenphosphate of calcium
DD27522285A DD255443A3 (de)	1984-05-25	1985-04-17	Verfahren zur gewinnung von calciumhydrogenphosphat-2-wasser oder/und wasserfreiem calciumhydrogenphosphat
SU857773811A SU1518298A1 (ru)	1984-05-25	1985-04-17	Способ получени гидрогенфосфата кальци
NL8501303A NL8501303A (nl)	1984-05-25	1985-05-08	Werkwijze voor de bereiding van calciumwaterstoffosfaatdihydraat en/of de watervrije vorm hiervan.
DE19853517608 DE3517608A1 (de)	1984-05-25	1985-05-15	Verfahren zur herstellung von calciumhydrogenphosphat-dihydrat und/oder dessen wasserfreier formen
GB08512556A GB2159510B (en)	1984-05-25	1985-05-17	Process for the production of anhydrous calcium hydrogen phosphates
FR8507570A FR2564817B1 (fr)	1984-05-25	1985-05-20	Procede pour la fabrication de phosphate hydrogene de calcium et/ou de sa forme anhydre
IT20868/85A IT1183673B (it)	1984-05-25	1985-05-24	Processo per la produzione di idrogenofosfato di calcio biidrato e/o idrogenofosfato di calcio anidro
YU00875/85A YU87585A (en)	1984-05-25	1985-05-24	Process for obtaining calcium-biophosphate dihydrate and/or anhydrated calcium-biophosphate
HU851997A HU201496B (en)	1984-05-25	1985-05-24	Process for producing calcium-hydrogen-phosphate-dihydtrate and-or calcium-hydrogen-phosphate siccum

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
CS393584A CS246515B1 (en)	1984-05-25	1984-05-25	Production method of dihydrate and/or waterless hydrogenphosphate

Publications (1)

Publication Number	Publication Date
CS246515B1 true CS246515B1 (en)	1986-10-16

Family

ID=5380856

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CS393584A CS246515B1 (en)	1984-05-25	1984-05-25	Production method of dihydrate and/or waterless hydrogenphosphate

Country Status (4)

Country	Link
BG (1)	BG45758A1 (de)
CS (1)	CS246515B1 (de)
DD (1)	DD255443A3 (de)
SU (1)	SU1518298A1 (de)

1984
- 1984-05-25 CS CS393584A patent/CS246515B1/cs unknown
1985
- 1985-04-15 BG BG6974985A patent/BG45758A1/xx unknown
- 1985-04-17 SU SU857773811A patent/SU1518298A1/ru active
- 1985-04-17 DD DD27522285A patent/DD255443A3/de not_active IP Right Cessation

Also Published As

Publication number	Publication date
BG45758A1 (en)	1989-08-15
DD255443A3 (de)	1988-04-06
SU1518298A1 (ru)	1989-10-30

Publication	Publication Date	Title
CS246515B1 (en)	1986-10-16	Production method of dihydrate and/or waterless hydrogenphosphate
CS247512B1 (en)	1987-01-15	Method of dihydrate or/and anhydrous hydrogen calcium phosphate production
JPS5921510A (ja)	1984-02-03	リン酸一水素カルシウム二水化物の製法
CS244246B1 (cs)	1986-07-17	Způsob výroby dihydrátu nebo/a bezvodého hydrogenfosforečnanu vápenatého
CS244247B1 (cs)	1986-07-17	) Způsob výroby dihydrátu nebo/a bezvodého hydrogenfosforečnanu vápenatého
CS242974B1 (cs)	1986-05-15	Způsob výroby dihydrátu nebo/a bezvodého hydrogenfosforečnanu vápenatého
CS236292B1 (cs)	1985-05-15	Způsob výroby směsi dihydrátu a bezvodého hydrogenfosforečnanu vápenatého
CS240739B1 (cs)	1986-02-13	Způsob výroby hydrogenfosforečnanu vápenatého
CS243309B1 (cs)	1986-06-12	Způsob výroby dihydrátu nebo/a bezvodého hydrogenfosforečnanu vápenatého
CS250189B1 (cs)	1987-04-16	Způsob výroby dihydrátu nebo/a bezvodého hydrogenfosforečnanú vápenatého
CS234950B1 (cs)	1985-04-16	Způsob výroby směsi dihydrátu a bezvqdého hydrogonfosforeůnauu vápenatého
CS234945B1 (cs)	1985-04-16	Způsob výroby směsi dihydrátu a bezvodého hydrogenřosforečnanu vápenatého
CS234949B1 (cs)	1985-04-16	Způsob výroby bezvodého hydrogenfosforečnanu vápenatého
CS235638B1 (cs)	1985-05-15	Způsob výroby směsi dihydrátu a bezvodého hydrogénfosforečnanu vápenatého
CS234682B1 (cs)	1985-04-16	Způsob výroby dihydrátu hydrogénfosforečnanu vápenatého
CS234943B1 (cs)	1985-04-16	Způsob výroby dihydrátu hydrogenfosforečnanu vápenatého
CS250187B1 (cs)	1987-04-16	Způsob výroby směsi dihydrátu a bezvodého hydrogenfosforečnanu vápenatého a chloridu amonného
CS243258B1 (cs)	1986-06-12	Způsob výroby hydrogenfosforečnanu vápenatého
CS242722B1 (cs)	1986-05-15	Způsob výroby dihydrátu nebo/a bezvodého hydrogenfosforečnanu vápenatého a amonné soli
CS235639B1 (cs)	1985-05-15	Způsob výroby bezvodého hydrogenfosforečnanu vápenatého
CS234932B1 (cs)	1985-04-16	Způsob výroby směsi dihydráíu a bezvodého hydrogenfosforečnanu vápenatého
CS247432B1 (en)	1986-12-18	Method of dihydrate or/and anhydrous calcium hydrogen phosphate production
CS235648B1 (cs)	1985-05-15	Způsob výroby směsi dihydrátu a bezvodého hydrogenfosforečnanu vápenatého
CS243257B1 (cs)	1986-06-12	Způsob výroby dihydrátu nebp/a bezvodého hydrogenfosforečnanu vápenatého
CS250188B1 (cs)	1987-04-16	Způsob výroby dihydrátu nebo/a bezvodého hydrogenfosforečnanu vápenatého