DD299288A5 - Verfahren zur herstellung eines kristallinen molekularsiebes - Google Patents

Verfahren zur herstellung eines kristallinen molekularsiebes Download PDF

Info

Publication number: DD299288A5
Authority: DD; German Democratic Republic
Prior art keywords: reaction mixture; molecular sieve; compound; hours; pore
Prior art date: 1989-07-07

Application number

DD89330566A

Other languages

German (de)

English (en)

Inventor

Elke Jahn

Rolf Fricke

Frank Neissendorfer

Juergen Richter-Mendau

Martin Buelow

Karl Becker

Peter Kraak

Rainer Schoedel

Original Assignee

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Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1989-07-07

Filing date

1989-07-07

Publication date

1992-04-09

1989-07-07 Application filed by ��@��@��@�K@��K@��@�K@��@�K@��@M��]k�� filed Critical ��@��@��@�K@��K@��@�K@��@�K@��@M��]k��

1989-07-07 Priority to DD89330566A priority Critical patent/DD299288A5/de

1990-07-05 Priority to DE59008225T priority patent/DE59008225D1/de

1990-07-05 Priority to EP90112879A priority patent/EP0406872B1/fr

1990-07-05 Priority to ES90112879T priority patent/ES2069633T3/es

1990-07-05 Priority to AT90112879T priority patent/ATE116951T1/de

1992-04-09 Publication of DD299288A5 publication Critical patent/DD299288A5/de

Links

238000004519 manufacturing process Methods 0.000 title abstract 2
239000002808 molecular sieve Substances 0.000 claims abstract description 20
URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 claims abstract description 20
238000000034 method Methods 0.000 claims abstract description 14
239000011148 porous material Substances 0.000 claims abstract description 11
239000011541 reaction mixture Substances 0.000 claims abstract description 9
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 8
239000000203 mixture Substances 0.000 claims description 9
NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 8
229910004298 SiO 2 Inorganic materials 0.000 claims description 8
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
WEHWNAOGRSTTBQ-UHFFFAOYSA-N dipropylamine Chemical compound CCCNCCC WEHWNAOGRSTTBQ-UHFFFAOYSA-N 0.000 claims description 6
229910018072 Al 2 O 3 Inorganic materials 0.000 claims description 5
-1 aluminum compound Chemical class 0.000 claims description 5
229910052698 phosphorus Inorganic materials 0.000 claims description 5
239000011574 phosphorus Substances 0.000 claims description 5
RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 claims description 5
229910000147 aluminium phosphate Inorganic materials 0.000 claims description 4
238000005216 hydrothermal crystallization Methods 0.000 claims description 4
238000002360 preparation method Methods 0.000 claims description 4
229910052782 aluminium Inorganic materials 0.000 claims description 3
150000001875 compounds Chemical class 0.000 claims description 3
229910002012 Aerosil® Inorganic materials 0.000 claims description 2
238000002441 X-ray diffraction Methods 0.000 claims description 2
150000003377 silicon compounds Chemical class 0.000 claims 4
150000001412 amines Chemical class 0.000 claims 2
229910001679 gibbsite Inorganic materials 0.000 claims 2
SMZOGRDCAXLAAR-UHFFFAOYSA-N aluminium isopropoxide Chemical compound [Al+3].CC(C)[O-].CC(C)[O-].CC(C)[O-] SMZOGRDCAXLAAR-UHFFFAOYSA-N 0.000 claims 1
230000011514 reflex Effects 0.000 claims 1
239000003054 catalyst Substances 0.000 abstract description 6
239000007787 solid Substances 0.000 abstract description 6
230000003197 catalytic effect Effects 0.000 abstract description 4
239000003463 adsorbent Substances 0.000 abstract description 3
229910000323 aluminium silicate Inorganic materials 0.000 abstract description 3
238000006243 chemical reaction Methods 0.000 abstract description 3
230000004048 modification Effects 0.000 abstract description 3
238000012986 modification Methods 0.000 abstract description 3
239000000377 silicon dioxide Substances 0.000 abstract description 3
239000010457 zeolite Substances 0.000 abstract description 3
HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 abstract description 2
239000000463 material Substances 0.000 abstract description 2
238000000926 separation method Methods 0.000 abstract description 2
229910021536 Zeolite Inorganic materials 0.000 abstract 1
229910052681 coesite Inorganic materials 0.000 abstract 1
229910052906 cristobalite Inorganic materials 0.000 abstract 1
238000002425 crystallisation Methods 0.000 abstract 1
239000011159 matrix material Substances 0.000 abstract 1
235000012239 silicon dioxide Nutrition 0.000 abstract 1
229910052682 stishovite Inorganic materials 0.000 abstract 1
229910052905 tridymite Inorganic materials 0.000 abstract 1
238000001816 cooling Methods 0.000 description 7
238000003756 stirring Methods 0.000 description 7
VXAUWWUXCIMFIM-UHFFFAOYSA-M aluminum;oxygen(2-);hydroxide Chemical compound [OH-].[O-2].[Al+3] VXAUWWUXCIMFIM-UHFFFAOYSA-M 0.000 description 4
239000000047 product Substances 0.000 description 4
239000013078 crystal Substances 0.000 description 3
239000012065 filter cake Substances 0.000 description 3
LGXAANYJEHLUEM-UHFFFAOYSA-N 1,2,3-tri(propan-2-yl)benzene Chemical compound CC(C)C1=CC=CC(C(C)C)=C1C(C)C LGXAANYJEHLUEM-UHFFFAOYSA-N 0.000 description 2
VXNZUUAINFGPBY-UHFFFAOYSA-N 1-Butene Chemical compound CCC=C VXNZUUAINFGPBY-UHFFFAOYSA-N 0.000 description 2
VQTUBCCKSQIDNK-UHFFFAOYSA-N Isobutene Chemical compound CC(C)=C VQTUBCCKSQIDNK-UHFFFAOYSA-N 0.000 description 2
OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 2
ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 2
QQONPFPTGQHPMA-UHFFFAOYSA-N Propene Chemical compound CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 2
238000010521 absorption reaction Methods 0.000 description 2
NNPPMTNAJDCUHE-UHFFFAOYSA-N isobutane Chemical compound CC(C)C NNPPMTNAJDCUHE-UHFFFAOYSA-N 0.000 description 2
239000000725 suspension Substances 0.000 description 2
241000269350 Anura Species 0.000 description 1
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
239000003513 alkali Substances 0.000 description 1
XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
239000011230 binding agent Substances 0.000 description 1
230000015572 biosynthetic process Effects 0.000 description 1
239000000470 constituent Substances 0.000 description 1
238000010586 diagram Methods 0.000 description 1
238000011049 filling Methods 0.000 description 1
238000010335 hydrothermal treatment Methods 0.000 description 1
239000001282 iso-butane Substances 0.000 description 1
150000002605 large molecules Chemical class 0.000 description 1
229920002521 macromolecule Polymers 0.000 description 1
150000002736 metal compounds Chemical class 0.000 description 1
IJDNQMDRQITEOD-UHFFFAOYSA-N n-butane Chemical compound CCCC IJDNQMDRQITEOD-UHFFFAOYSA-N 0.000 description 1
TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 1
239000001294 propane Substances 0.000 description 1
229910052710 silicon Inorganic materials 0.000 description 1
239000010703 silicon Substances 0.000 description 1
238000000547 structure data Methods 0.000 description 1
239000000126 substance Substances 0.000 description 1
238000003786 synthesis reaction Methods 0.000 description 1
230000009466 transformation Effects 0.000 description 1
238000000844 transformation Methods 0.000 description 1
239000011800 void material Substances 0.000 description 1

Classifications

- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J29/00—Catalysts comprising molecular sieves
- B01J29/82—Phosphates
- B01J29/84—Aluminophosphates containing other elements, e.g. metals, boron
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B37/00—Compounds having molecular sieve properties but not having base-exchange properties
- C01B37/04—Aluminophosphates [APO compounds]
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B37/00—Compounds having molecular sieve properties but not having base-exchange properties
- C01B37/06—Aluminophosphates containing other elements, e.g. metals, boron
- C01B37/08—Silicoaluminophosphates [SAPO compounds], e.g. CoSAPO

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Inorganic Chemistry (AREA)
Engineering & Computer Science (AREA)
Materials Engineering (AREA)
Chemical Kinetics & Catalysis (AREA)
Silicates, Zeolites, And Molecular Sieves (AREA)
Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Catalysts (AREA)
Compounds Of Unknown Constitution (AREA)
Medicines Containing Material From Animals Or Micro-Organisms (AREA)

DD89330566A 1989-07-07 1989-07-07 Verfahren zur herstellung eines kristallinen molekularsiebes DD299288A5 (de)

Priority Applications (5)

Application Number	Priority Date	Filing Date	Title
DD89330566A DD299288A5 (de)	1989-07-07	1989-07-07	Verfahren zur herstellung eines kristallinen molekularsiebes
DE59008225T DE59008225D1 (de)	1989-07-07	1990-07-05	Verfahren zur Herstellung eines weitporigen kristallinen Molekularsiebes.
EP90112879A EP0406872B1 (fr)	1989-07-07	1990-07-05	Procédé de préparation d'un tamis moléculaire cristallin à grands pores
ES90112879T ES2069633T3 (es)	1989-07-07	1990-07-05	Procedimiento para la fabricacion de un tamiz molecular cristalino de poro ancho.
AT90112879T ATE116951T1 (de)	1989-07-07	1990-07-05	Verfahren zur herstellung eines weitporigen kristallinen molekularsiebes.

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
DD89330566A DD299288A5 (de)	1989-07-07	1989-07-07	Verfahren zur herstellung eines kristallinen molekularsiebes

Publications (1)

Publication Number	Publication Date
DD299288A5 true DD299288A5 (de)	1992-04-09

Family

ID=5610706

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
DD89330566A DD299288A5 (de)	1989-07-07	1989-07-07	Verfahren zur herstellung eines kristallinen molekularsiebes

Country Status (5)

Country	Link
EP (1)	EP0406872B1 (fr)
AT (1)	ATE116951T1 (fr)
DD (1)	DD299288A5 (fr)
DE (1)	DE59008225D1 (fr)
ES (1)	ES2069633T3 (fr)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE4138272A1 (de) *	1991-11-21	1993-07-01	Vaw Ver Aluminium Werke Ag	Katalysatormaterial, seine verwendung sowie ein verfahren zur hydrodehalogenierung von organischen halogenverbindungen
DE4331116C2 (de) *	1993-09-14	1998-09-03	Alsi Penta Zeolithe Gmbh	Verfahren zur Herstellung von Dimeren des alpha-Methylstyrols
US6379646B1 (en) *	1997-06-17	2002-04-30	Chevron U.S.A. Inc.	Crystalline phosphorus-containing molecular sieves
DE19805572A1 (de) *	1998-02-12	1999-08-19	Beiersdorf Ag	Intercalationsverbindungen und Stabilisierung oxidations- und/oder UV-empfindlicher Wirkstoffe
ES2601799T3 (es)	2009-06-12	2017-02-16	Albemarle Europe Sprl.	Catalizadores de tamiz molecular SAPO y su preparación y usos
CN111099603B (zh)	2018-10-25	2022-12-09	中国石油化工股份有限公司	Scm-18分子筛及其制备方法

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
NZ210467A (en) *	1983-12-19	1988-06-30	Mobil Oil Corp	Crystalline silicophosphoaluminate material and its use as a catalyst
JPH03505720A (ja) *	1987-08-28	1991-12-12	ザ　ダウ　ケミカル　カンパニー	結晶性アルミニウムホスフェート組成物
AU2924089A (en) *	1987-12-21	1989-07-19	Mobil Oil Corporation	Crystalline molecular sieve

1989
- 1989-07-07 DD DD89330566A patent/DD299288A5/de not_active IP Right Cessation
1990
- 1990-07-05 AT AT90112879T patent/ATE116951T1/de not_active IP Right Cessation
- 1990-07-05 DE DE59008225T patent/DE59008225D1/de not_active Expired - Fee Related
- 1990-07-05 ES ES90112879T patent/ES2069633T3/es not_active Expired - Lifetime
- 1990-07-05 EP EP90112879A patent/EP0406872B1/fr not_active Expired - Lifetime

Also Published As

Publication number	Publication date
ES2069633T3 (es)	1995-05-16
ATE116951T1 (de)	1995-01-15
DE59008225D1 (de)	1995-02-23
EP0406872B1 (fr)	1995-01-11
EP0406872A3 (en)	1992-01-02
EP0406872A2 (fr)	1991-01-09

Legal Events

Date	Code	Title	Description
1996-06-20	RPI	Change in the person, name or address of the patentee (searches according to art. 11 and 12 extension act)
2001-04-12	ENJ	Ceased due to non-payment of renewal fee

Publication	Publication Date	Title
DE60006765T2 (de)	2004-05-19	Verfahren zur Herstellung von Zeolith des MTT-Typs mittels spezifischen Vorläufern des Strukturbildners
DE69727395T2 (de)	2004-11-04	Verfahren zur olefinisomerisierung
DE60310898T2 (de)	2007-10-11	Chabazit mit hohem gehalt an siliciumdioxid, dessen synthese und verwendung zur umwandlung von sauerstoffverbindungen zu olefinen
DE69520208T3 (de)	2007-12-27	Herstellung von nicht-zeolithischen molekularsieben
DE2507426C2 (de)	1986-08-07	Verfahren zur Herstellung des Zeolithen Ferrierit
DE60036508T2 (de)	2008-06-26	Formling aus binderfreien Zeolith , Verfahren zu seiner Herstellung und seine Verwendung
DE3021580A1 (de)	1981-12-24	Verfahren zur herstellung von zeolithen und verwendung derselben als katalysatoren
DE69805013T2 (de)	2002-12-05	Verfahren zur Synthese von Silikatmolekularsiebe mit hohem Siliziumdioxydgehalte
EP0761598B1 (fr)	1999-07-14	Procédé de préparation de zéolithe Y
EP0464249B1 (fr)	1994-01-05	Procédé pour préparer des tamis moléculaires cristallins à grands pores
DE69510550T2 (de)	2000-01-20	Verfahren zur herstellung eines kristallinen mikroporösen körpers
EP0532993B1 (fr)	1995-04-19	Procédé de préparation d'alumino- et de silicoaluminophosphates de structure AEL par utilisation de 1,2-bis(4-pyridyl)éthane
ATE86948T1 (de)	1993-04-15	Synthetisches kristallines aluminiumsilikat und verfahren zu seiner herstellung.
EP0406872B1 (fr)	1995-01-11	Procédé de préparation d'un tamis moléculaire cristallin à grands pores
DE112012000587B4 (de)	2019-03-28	Verfahren zur Herstellung von MTW-Typ-Zeolith
EP0007098B1 (fr)	1981-09-09	Procédé pour la préparation de zéolites d'aluminosilicates cristallins
DE3037415A1 (de)	1982-05-27	Verfahren zur herstellung eines zeoliths vom strukturtyp des ferrierit
DD207186B1 (de)	1988-01-06	Verfahren zur herstellung von hochkieselsaeurehaltigen zeolithen des typs zsm-5
KR20010079999A (ko)	2001-08-22	거대 공극의 알루미노포스페이트인 이씨알-40 조성물 및그의 제조 방법
DE3215841A1 (de)	1982-11-11	Kristalline silikatteilchen, verfahren zu ihrer herstellung und ihre verwendung
EP0534200A1 (fr)	1993-03-31	Procédé de préparation de cristaux de borosilicate à structure zéolitique essentiellement exempts de métaux alcalins
DD296426A5 (de)	1991-12-05	Oekonomisches und umweltfreundliches verfahren zur herstellung eines weitporigen kristallinen molekularsiebes
EP0423532B1 (fr)	1994-03-09	Procédé de préparation de silicates de métaux finement cristallisés synthétiques
DE3137729A1 (de)	1982-06-16	Polymorphe kristalline kieselsaeuren
AT399107B (de)	1995-03-27	Verfahren zur herstellung eines aluminium-bor-silikat-katalysators