DK1506159T3 - Fremgangsmåde til fremstilling af 2-(4-N,N-diethylamino-2-hydroxybenzoyl)benzoesyre-n-hexyl-ester - Google Patents

Fremgangsmåde til fremstilling af 2-(4-N,N-diethylamino-2-hydroxybenzoyl)benzoesyre-n-hexyl-ester

Info

Publication number: DK1506159T3
Authority: DK; Denmark
Prior art keywords: hydroxybenzoyl; benzoic acid; dialkylamino; alcohol; formula
Prior art date: 2002-05-15

Application number

DK03720564T

Other languages

English (en)

Inventor

Thomas Heidenfelder

Karl Beck

Original Assignee

Basf Ag

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2002-05-15

Filing date

2003-05-12

Publication date

2007-12-27

2003-05-12 Application filed by Basf Ag filed Critical Basf Ag

2007-12-27 Application granted granted Critical

2007-12-27 Publication of DK1506159T3 publication Critical patent/DK1506159T3/da

Links

238000000034 method Methods 0.000 title abstract 2
UUGLJVMIFJNVFH-UHFFFAOYSA-N Hexyl benzoate Chemical compound CCCCCCOC(=O)C1=CC=CC=C1 UUGLJVMIFJNVFH-UHFFFAOYSA-N 0.000 title 1
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 4
WPYMKLBDIGXBTP-UHFFFAOYSA-N Benzoic acid Natural products OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 abstract 2
239000005711 Benzoic acid Substances 0.000 abstract 2
239000003377 acid catalyst Substances 0.000 abstract 2
WPYMKLBDIGXBTP-VQEHIDDOSA-N benzoic acid Chemical compound OC(=O)C1=CC=C[13CH]=C1 WPYMKLBDIGXBTP-VQEHIDDOSA-N 0.000 abstract 2
235000010233 benzoic acid Nutrition 0.000 abstract 2
150000001559 benzoic acids Chemical class 0.000 abstract 2
238000006243 chemical reaction Methods 0.000 abstract 2
125000004122 cyclic group Chemical group 0.000 abstract 2
125000000753 cycloalkyl group Chemical group 0.000 abstract 2
230000032050 esterification Effects 0.000 abstract 2
238000005886 esterification reaction Methods 0.000 abstract 2
150000002148 esters Chemical class 0.000 abstract 2
238000004519 manufacturing process Methods 0.000 abstract 2
LGRFSURHDFAFJT-UHFFFAOYSA-N phthalic anhydride Chemical compound C1=CC=C2C(=O)OC(=O)C2=C1 LGRFSURHDFAFJT-UHFFFAOYSA-N 0.000 abstract 2
239000003463 adsorbent Substances 0.000 abstract 1
125000000217 alkyl group Chemical group 0.000 abstract 1
238000004821 distillation Methods 0.000 abstract 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C227/38—Separation; Purification; Stabilisation; Use of additives
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C229/52—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to carbon atoms of six-membered aromatic rings of the same carbon skeleton

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

DK03720564T 2002-05-15 2003-05-12 Fremgangsmåde til fremstilling af 2-(4-N,N-diethylamino-2-hydroxybenzoyl)benzoesyre-n-hexyl-ester DK1506159T3 (da)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
DE10221805A DE10221805A1 (de)	2002-05-15	2002-05-15	Verfahren zur Herstellung von 2-(4-N,N-Dialkylamino-2-hydroxybenzoyl)benzoesäureestern
PCT/EP2003/004918 WO2003097578A1 (de)	2002-05-15	2003-05-12	Verfahren zur herstellung von 2-(4-n, n-dialkylamino-2-hydroxybenzoyl)benzoesäureestern

Publications (1)

Publication Number	Publication Date
DK1506159T3 true DK1506159T3 (da)	2007-12-27

Family

ID=29285465

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
DK03720564T DK1506159T3 (da)	2002-05-15	2003-05-12	Fremgangsmåde til fremstilling af 2-(4-N,N-diethylamino-2-hydroxybenzoyl)benzoesyre-n-hexyl-ester

Country Status (11)

Country	Link
US (1)	US20050165099A1 (da)
EP (1)	EP1506159B1 (da)
JP (1)	JP4472518B2 (da)
CN (1)	CN1653035A (da)
AT (1)	ATE373634T1 (da)
AU (1)	AU2003224156A1 (da)
DE (2)	DE10221805A1 (da)
DK (1)	DK1506159T3 (da)
ES (1)	ES2290452T3 (da)
PT (1)	PT1506159E (da)
WO (1)	WO2003097578A1 (da)

Families Citing this family (22)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE10328547A1 (de) *	2003-06-24	2005-01-13	Basf Ag	Mischung bestehend aus einem UV-A- und einem UV-B-Filter
WO2008135360A1 (de) *	2007-05-02	2008-11-13	Basf Se	Verfahren zur kristallisation von 2-(4-n,n-diethylamino-2-hydroxybenzoyl)-benzoesäure-n-hexylester
US20090258309A1 (en)	2008-04-15	2009-10-15	Konica Minolta Business Technologies, Inc.	Toner for electrostatic charge image development and method for producing the same
CN105339344B (zh) *	2013-06-27	2018-04-20	帝斯曼知识产权资产管理有限公司	生产2‑(4‑n,n‑二烷基氨基‑2‑羟基苯甲酰基)苯甲酸酯的方法
MX368523B (es) *	2013-06-27	2019-10-07	Dsm Ip Assets Bv	Metodo para producir benzoatos de 2-(4-n, n-dialquilamino-2-hidrox ibenzoilo).
CN105801830B (zh) *	2016-05-03	2018-01-19	中国航空工业集团公司北京航空材料研究院	一种耐高温聚碳酸酯及其制备方法
KR102179649B1 (ko) *	2019-10-11	2020-11-18	(주)에이에스텍	디에틸아미노하이드록시벤조일헥실벤조에이트의 제조 방법
JP2023515198A (ja) *	2020-02-27	2023-04-12	ビーエーエスエフソシエタス・ヨーロピア	２－（４’－ジエチルアミノ－２’－ヒドロキシベンゾイル）安息香酸ヘキシルエステルを単離する方法
WO2021233805A1 (en)	2020-05-19	2021-11-25	Basf Se	Process for purifying 2-(4'-diethylamino-2'-hydroxybenzoyl)benzoic acid hexyl ester
CN111499529B (zh) *	2020-06-08	2021-01-15	湖北师范大学	一种紫外线吸收剂UVA Plus的合成方法
CN112010771B (zh) *	2020-09-08	2023-05-02	河北建新化工股份有限公司	一种2-（4-二乙氨基-2-羟基苯甲酰基）苯甲酸正己酯的制备方法
EP4015500A1 (en)	2020-12-18	2022-06-22	Basf Se	Process of manufacturing 2-(4 -diethylamino-2 -hydroxybenzoyl)benzoic acid hexyl ester
EP4263490B1 (en) *	2020-12-18	2025-06-04	Basf Se	Method for obtaining crystalline diethylamino hydroxybenzoyl hexyl benzoate
CN115703715A (zh) *	2021-08-16	2023-02-17	马鞍山科思化学有限公司	一种防晒剂A-Plus的中控及成品分析方法
CN114276260B (zh) *	2021-11-11	2023-11-10	马鞍山科思化学有限公司	一种防晒剂UV A Plus的制备方法
CN114149339B (zh) *	2021-12-28	2023-01-31	黄冈美丰化工科技有限公司	一种紫外线吸收剂、组合物、化妆品及配制化妆品的工艺
WO2023242181A1 (en)	2022-06-17	2023-12-21	Basf Se	Method for obtaining crystalline diethylamino hydroxybenzoyl hexyl benzoate
CN115010615B (zh) *	2022-07-14	2023-12-08	四川沃肯精细化工有限公司	一种二乙氨基羟苯甲酰基苯甲酸正己酯的制备方法
KR102633630B1 (ko)	2023-05-22	2024-02-05	주식회사 디제이씨	n-헥실-2-(4-N,N-디에틸아미노-2-하이드록시벤조일)벤조에이트의 제조 방법
CN117658836A (zh) *	2023-11-07	2024-03-08	利安隆（中卫）新材料有限公司	二乙基氨基羟基苯甲酰基苯甲酸己酯的制备方法
KR102943266B1 (ko)	2024-02-23	2026-03-24	(주)젠퓨어	신규한 중간체로부터의 디에칠아미노하이드록시벤조일헥실벤조에이트 제조 방법
CN118724710B (zh) *	2024-06-07	2025-06-03	宜都市华阳化工有限责任公司	一种2-(4-n,n-二乙基氨基-2-羟基苯甲酰基)苯甲酸己酯的合成工艺

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS61151158A (ja) *	1984-12-26	1986-07-09	Taoka Chem Co Ltd	ベンゾイル安息香酸誘導体及びその製造法
DE19917906A1 (de) *	1999-04-20	2000-10-26	Basf Ag	Verwendung von aminosubstituierten Hydroxybenzophenonen als photostabile UV-Filter in kosmetischen und pharmazeutischen Zubereitungen

2002
- 2002-05-15 DE DE10221805A patent/DE10221805A1/de not_active Withdrawn
2003
- 2003-05-12 CN CNA038110008A patent/CN1653035A/zh active Pending
- 2003-05-12 DK DK03720564T patent/DK1506159T3/da active
- 2003-05-12 DE DE50308226T patent/DE50308226D1/de not_active Expired - Lifetime
- 2003-05-12 US US10/514,410 patent/US20050165099A1/en not_active Abandoned
- 2003-05-12 JP JP2004505312A patent/JP4472518B2/ja not_active Expired - Lifetime
- 2003-05-12 ES ES03720564T patent/ES2290452T3/es not_active Expired - Lifetime
- 2003-05-12 EP EP03720564A patent/EP1506159B1/de not_active Expired - Lifetime
- 2003-05-12 WO PCT/EP2003/004918 patent/WO2003097578A1/de not_active Ceased
- 2003-05-12 AU AU2003224156A patent/AU2003224156A1/en not_active Abandoned
- 2003-05-12 AT AT03720564T patent/ATE373634T1/de not_active IP Right Cessation
- 2003-05-12 PT PT03720564T patent/PT1506159E/pt unknown

Also Published As

Publication number	Publication date
ATE373634T1 (de)	2007-10-15
EP1506159A1 (de)	2005-02-16
EP1506159B1 (de)	2007-09-19
DE50308226D1 (de)	2007-10-31
ES2290452T3 (es)	2008-02-16
DE10221805A1 (de)	2003-11-27
JP2005533764A (ja)	2005-11-10
JP4472518B2 (ja)	2010-06-02
WO2003097578A1 (de)	2003-11-27
AU2003224156A1 (en)	2003-12-02
PT1506159E (pt)	2007-10-29
CN1653035A (zh)	2005-08-10
US20050165099A1 (en)	2005-07-28

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