ES2032133T3 - Procedimiento y dispositivo de introduccion de tetracloruro de zirconio, tetracloruro de hafnio y sus mezclas en una columna de destilacion extractora en continuo y bajo presion de dichos cloruros. - Google Patents

Procedimiento y dispositivo de introduccion de tetracloruro de zirconio, tetracloruro de hafnio y sus mezclas en una columna de destilacion extractora en continuo y bajo presion de dichos cloruros.

Info

Publication number
ES2032133T3
ES2032133T3 ES198989420114T ES89420114T ES2032133T3 ES 2032133 T3 ES2032133 T3 ES 2032133T3 ES 198989420114 T ES198989420114 T ES 198989420114T ES 89420114 T ES89420114 T ES 89420114T ES 2032133 T3 ES2032133 T3 ES 2032133T3
Authority
ES
Spain
Prior art keywords
tetrachloride
procedure
chlorides
introduction
under pressure
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES198989420114T
Other languages
English (en)
Inventor
Pierre Brun
Jean Guerin
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Compagnie Europeenne du Zirconium Cezus SA
Original Assignee
Compagnie Europeenne du Zirconium Cezus SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Compagnie Europeenne du Zirconium Cezus SA filed Critical Compagnie Europeenne du Zirconium Cezus SA
Application granted granted Critical
Publication of ES2032133T3 publication Critical patent/ES2032133T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/40—Extractive distillation
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G25/00—Compounds of zirconium
    • C01G25/04—Halides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G27/00—Compounds of hafnium
    • C01G27/04—Halides
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S203/00—Distillation: processes, separatory
    • Y10S203/17—Saline water conversion

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Manufacture And Refinement Of Metals (AREA)

Abstract

EL PROCEDIMIENTO Y EL DISPOSITIVO DE LA INVENCION SE REFIEREN A LA INTRODUCCION CON UN CAUDAL ESTABLE Y CONOCIDO DE TETRACLORURO SUBLIMABLE EN UNA COLUMNA (7) DE DESTILACION EXTRACTIVA CONTINUA Y BAJO PRESION DE DICHOS CLORUROS. EL TETRACLORURO SUBLIMABLE ES DISUELTO EN UN DISOLVENTE DE CALOR (I) EN UN DISOLVENTE LIQUIDO COMO KAICI4, DESPUES EMPUJADO POR UNA BOMBA (5) CON UN CAUDAL ESTABLE Y CONOCIDO EN UN EVAPORADOR (6) UNIDO A LA COLUMNA (7). LA SOLUCION ES ENTONCES RECALENTADA EN EL EVAPORADOR (6) DE MANERA QUE SE SUBLIME LO ESENCIAL DEL PRODUCTO QUE CONTIENEN, LOS VAPORES SUBLIMADOS PASANDO ENTONCES CON UN CAUDAL ESTABLE Y CONOCIDO EN LA COLUMNA (7). EL PROCEDIMIENTO DE LA INVENCION SE APLICA EN PARTICULAR EN LAS UNIDADES DE FABRICACION DE ZRCL4 DE PUREZA NUCLEAR Y DE HFCL4.
ES198989420114T 1988-03-31 1989-03-29 Procedimiento y dispositivo de introduccion de tetracloruro de zirconio, tetracloruro de hafnio y sus mezclas en una columna de destilacion extractora en continuo y bajo presion de dichos cloruros. Expired - Lifetime ES2032133T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR8804731A FR2629360B1 (fr) 1988-03-31 1988-03-31 Procede et dispositif d'introduction de tetrachlorure de zirconium, de tetrachlorure de hafnium et de leurs melanges dans une colonne de distillation extractive en continu et sous pression desdits chlorures

Publications (1)

Publication Number Publication Date
ES2032133T3 true ES2032133T3 (es) 1993-01-01

Family

ID=9365155

Family Applications (1)

Application Number Title Priority Date Filing Date
ES198989420114T Expired - Lifetime ES2032133T3 (es) 1988-03-31 1989-03-29 Procedimiento y dispositivo de introduccion de tetracloruro de zirconio, tetracloruro de hafnio y sus mezclas en una columna de destilacion extractora en continuo y bajo presion de dichos cloruros.

Country Status (14)

Country Link
US (1) US4917773A (es)
EP (1) EP0340119B1 (es)
JP (1) JPH0637301B2 (es)
KR (1) KR930012027B1 (es)
CN (1) CN1020674C (es)
AR (1) AR243092A1 (es)
AU (1) AU605736B2 (es)
BR (1) BR8901486A (es)
CA (1) CA1336944C (es)
DE (1) DE68901633D1 (es)
ES (1) ES2032133T3 (es)
FR (1) FR2629360B1 (es)
RU (1) RU2036151C1 (es)
ZA (1) ZA892354B (es)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4243995C2 (de) * 1992-12-23 1996-07-25 Gore W L & Ass Gmbh Permanente hydrophile Modifizierung für Fluorpolymere und Verfahren zur Erzeugung der Modifizierung
FR2823740B1 (fr) * 2001-04-18 2004-02-06 Cezus Co Europ Zirconium Procede de separation des tetrachlorures de zirconium et de hafnium
FR2872811B1 (fr) 2004-07-09 2006-10-06 Cie Europ Du Zirconium Cezus S Procede de separation et purification du hafnium et du zirconium
RU2329951C2 (ru) * 2006-07-12 2008-07-27 Лев Александрович Нисельсон Способ разделения тетрахлоридов циркония и гафния ректификацией
EP2060315A3 (en) 2007-11-15 2009-08-12 DSMIP Assets B.V. High performance membrane
RU2431700C1 (ru) * 2010-06-21 2011-10-20 Учреждение Российской академии наук Институт высокотемпературной электрохимии Уральского отделения РАН Способ приготовления расплава хлоралюмината калия для разделения хлоридов циркония и гафния
RU2567430C2 (ru) * 2013-12-04 2015-11-10 Открытое акционерное общество "Чепецкий механический завод" (ОАО ЧМЗ) Способ коррозионной защиты оборудования, работающего в среде расплава хлоралюмината калия.
CN103725901B (zh) * 2013-12-12 2015-10-28 上海哈峰新材料科技有限公司 氧化锆/氧化铪混合物的火法分离方法
RU2689744C1 (ru) * 2018-02-13 2019-05-28 Акционерное общество "Чепецкий механический завод" Способ очистки смеси тетрахлоридов циркония и гафния от примесей
CN110747357B (zh) * 2019-11-12 2021-06-25 济南大学 一种双磷酸萃取剂用于萃取分离锆铪的方法
CN113772724A (zh) * 2021-10-20 2021-12-10 辽宁华锆新材料有限公司 一种熔盐提纯法制备精四氯化锆的方法及设备
CN119215462B (zh) * 2024-09-30 2025-09-19 有研资源环境技术研究院(北京)有限公司 一种锆铪四氯化物的熔盐萃取精馏分离装置

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2816814A (en) * 1953-08-20 1957-12-17 William K Plucknett Separation of zirconium and hafnium halides
US2852446A (en) * 1956-12-07 1958-09-16 Du Pont Purification of zirconium tetrachlorides by fractional distillation
US3098722A (en) * 1959-01-16 1963-07-23 Nat Distillers Chem Corp Purification of metal halides
JPS5025413B1 (es) * 1969-01-11 1975-08-23
US4021531A (en) * 1973-11-14 1977-05-03 Ugine Aciers Process for the separation of zirconium and hafnium tetrachlorides from mixtures thereof
US3966458A (en) * 1974-09-06 1976-06-29 Amax Speciality Metal Corporation Separation of zirconium and hafnium
CA1171664A (en) * 1980-07-30 1984-07-31 Hiroshi Ishizuka Process for separation of zirconium- and hafnium tetrachlorides from a mixture comprising such chlorides and apparatus therefor
FR2543162A1 (fr) * 1983-03-24 1984-09-28 Cezus Co Europ Zirconium Procede de separation de zrcl4 d'avec hfcl4 par distillation extractive permettant d'eliminer l'aluminium apporte par le solvant
US4737244A (en) * 1986-12-18 1988-04-12 Westinghouse Electric Corp. Zirconium and hafnium tetrachloride separation by extractive distillation with molten zinc chloride lead chloride solvent
US4749448A (en) * 1986-12-18 1988-06-07 Westinghouse Electric Corp. Zirconium and hafnium tetrachloride separation by extractive distillation with molten zinc chloride calcium and/or magnesium chloride solvent

Also Published As

Publication number Publication date
EP0340119B1 (fr) 1992-05-27
BR8901486A (pt) 1989-11-14
RU2036151C1 (ru) 1995-05-27
CA1336944C (fr) 1995-09-12
JPH01298024A (ja) 1989-12-01
DE68901633D1 (de) 1992-07-02
AU3224589A (en) 1989-10-05
FR2629360A1 (fr) 1989-10-06
CN1036706A (zh) 1989-11-01
JPH0637301B2 (ja) 1994-05-18
FR2629360B1 (fr) 1991-01-11
KR890014144A (ko) 1989-10-23
AR243092A1 (es) 1993-07-30
ZA892354B (en) 1989-12-27
CN1020674C (zh) 1993-05-19
KR930012027B1 (ko) 1993-12-23
AU605736B2 (en) 1991-01-17
EP0340119A1 (fr) 1989-11-02
US4917773A (en) 1990-04-17

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