ES2080575T3 - Procedimiento para la fabricacion de resina de organopolisiloxano. - Google Patents
Procedimiento para la fabricacion de resina de organopolisiloxano.Info
- Publication number
- ES2080575T3 ES2080575T3 ES93120313T ES93120313T ES2080575T3 ES 2080575 T3 ES2080575 T3 ES 2080575T3 ES 93120313 T ES93120313 T ES 93120313T ES 93120313 T ES93120313 T ES 93120313T ES 2080575 T3 ES2080575 T3 ES 2080575T3
- Authority
- ES
- Spain
- Prior art keywords
- water
- place
- mass
- organopolisiloxane
- acids
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- 239000011347 resin Substances 0.000 title abstract 2
- 229920005989 resin Polymers 0.000 title abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 4
- 239000002253 acid Substances 0.000 abstract 3
- 150000007513 acids Chemical class 0.000 abstract 3
- 238000004821 distillation Methods 0.000 abstract 2
- 239000003960 organic solvent Substances 0.000 abstract 2
- XLYOFNOQVPJJNP-PWCQTSIFSA-N Tritiated water Chemical compound [3H]O[3H] XLYOFNOQVPJJNP-PWCQTSIFSA-N 0.000 abstract 1
- KPUWHANPEXNPJT-UHFFFAOYSA-N disiloxane Chemical class [SiH3]O[SiH3] KPUWHANPEXNPJT-UHFFFAOYSA-N 0.000 abstract 1
- 230000003472 neutralizing effect Effects 0.000 abstract 1
- 210000000056 organ Anatomy 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D19/00—Degasification of liquids
- B01D19/02—Foam dispersion or prevention
- B01D19/04—Foam dispersion or prevention by addition of chemical substances
- B01D19/0404—Foam dispersion or prevention by addition of chemical substances characterised by the nature of the chemical substance
- B01D19/0409—Foam dispersion or prevention by addition of chemical substances characterised by the nature of the chemical substance compounds containing Si-atoms
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/06—Preparatory processes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H19/00—Coated paper; Coating material
- D21H19/10—Coatings without pigments
- D21H19/14—Coatings without pigments applied in a form other than the aqueous solution defined in group D21H19/12
- D21H19/24—Coatings without pigments applied in a form other than the aqueous solution defined in group D21H19/12 comprising macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D21H19/32—Coatings without pigments applied in a form other than the aqueous solution defined in group D21H19/12 comprising macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds obtained by reactions forming a linkage containing silicon in the main chain of the macromolecule
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03G—ELECTROGRAPHY; ELECTROPHOTOGRAPHY; MAGNETOGRAPHY
- G03G9/00—Developers
- G03G9/08—Developers with toner particles
- G03G9/087—Binders for toner particles
- G03G9/08742—Binders for toner particles comprising macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- G03G9/08773—Polymers having silicon in the main chain, with or without sulfur, oxygen, nitrogen or carbon only
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Spectroscopy & Molecular Physics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Toxicology (AREA)
- Dispersion Chemistry (AREA)
- Silicon Polymers (AREA)
Abstract
SE TRATA DE UN PROCESO PARA LA PRODUCCION DE RESINAS DE ORGANOPOLISILOXANO, CARACTERIZADO EN UN PRIMER PASO, POR QUE POR LO MENOS SE INTRODUZCA UN SILANO DE LA FORMULA DONDE A, R Y R , RECIBEN SU SIGNIFICADO EN EL APARTADO 1, Y/O SU HIDROLIZADO PARCIAL, CON LA SALVEDAD, DE QUE AL MENOS UN SILANO DE LA FORMULA 1 CON A IGUAL A 0 O A 1 Y/O SU HIDROLIZADO PARCIAL, ASI COMO DADO EL CASO SE TRANSFORME EL ORGANO(POLI)SILOXANO CON AGUA EN PRESENCIA DE ACIDOS POLIPROTONICOS Y DADO EL CASO DE OTROS PRODUCTOS, NEUTRALIZANDO A CONTINUACION LOS ACIDOS PARCIALMENTE CON EL AÑADIDO DE BASES Y SEPARANDO PARCIALMENTE POR DESTILACION EL ENLACE R1OH OBTENIDO. SI HUBIERA LUGAR A ELLO, SE TRANSFORMA EN UN SEGUNDO PASO LA MASA DE REACCION HOMOGENEA OBTENIDA EN EL APARTADO 1 EN PRESENCIA DE BASES ASI COMO DE DISOLVENTE ORGANICO NO SOLUBLE EN AGUA, Y SE SEPARAN POR DESTILACION PARCIALMENTE EL AGUA Y LOS ENLACES R1OH. SI HUBIERA LUGAR A ELLO, EN UN TERCER PASO LA MASA DE REACCION OBTENIDA ENE LE PASO 2, SE DEPOSITAJUNTO A ACIDOS POLIPROTONICOS Y/O SUS SALES MEDIANTE ALMACENAMIENTO CON UN VALOR DE PH ENTRE 6 Y 8, MIENTRAS QUE EL AGUA Y LOS ENLACES R1OH QUE AUN QUEDEN SE VUELVEN A SEPARAR POR DESTILACION PARCIALMENTE Y LA SAL RESULTANTE SE FILTRA. SI HUBIERA LUGAR A ELLO, EN UN CUARTO PASO LA MASA DE REACCION OBTENIDA EN EL PASO 3 DE LIBERA MEDIANTE UN DISOLVENTE ORGANICO NO SOLUBLE EN AGUA.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE4243895A DE4243895A1 (de) | 1992-12-23 | 1992-12-23 | Verfahren zur Herstellung von Organopolysiloxanharz |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2080575T3 true ES2080575T3 (es) | 1996-02-01 |
Family
ID=6476431
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES93120313T Expired - Lifetime ES2080575T3 (es) | 1992-12-23 | 1993-12-16 | Procedimiento para la fabricacion de resina de organopolisiloxano. |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US5401821A (es) |
| EP (1) | EP0604847B1 (es) |
| JP (1) | JP2596706B2 (es) |
| CA (1) | CA2111728C (es) |
| DE (2) | DE4243895A1 (es) |
| ES (1) | ES2080575T3 (es) |
| FI (1) | FI935632A7 (es) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5548053A (en) * | 1992-05-15 | 1996-08-20 | Wacker-Chemie Gmbh | Process for the preparation of organopolysiloxane resin |
| CN1125481A (zh) * | 1994-03-11 | 1996-06-26 | 川崎制铁株式会社 | 评价用于形成绝缘膜的硅氧烷的方法、形成绝缘膜的涂布液及其制备方法、半导体器件用绝缘膜成型方法以及采用绝缘膜成膜法制备半导体器件的方法 |
| DE19639782A1 (de) * | 1996-09-27 | 1998-04-02 | Huels Chemische Werke Ag | Glycidether-, Acryl- und/oder Methacryl-funktionelle Organopolysiloxan-haltige Zusammensetzungen auf Wasser-Basis, Verfahren zu deren Herstellung sowie deren Verwendung |
| DE19800021A1 (de) | 1998-01-02 | 1999-07-08 | Huels Silicone Gmbh | Verfahren zur Herstellung von Polyorganosiloxanharzen, die mono- und tetrafunktionelle Einheiten enthalten |
| DE19857348A1 (de) * | 1998-12-11 | 2000-06-15 | Wacker Chemie Gmbh | Organopolysiloxanharze |
| JP3705333B2 (ja) * | 1999-05-12 | 2005-10-12 | 信越化学工業株式会社 | シラノール基を有する有機けい素化合物の製造方法 |
| US6131312A (en) * | 1999-07-13 | 2000-10-17 | Hung; Cheng-Che | Safety shoe with detachable steel toe box |
| DE10242418A1 (de) * | 2002-09-12 | 2004-03-25 | Wacker-Chemie Gmbh | Verfahren zur Herstellung von Organopolysiloxanharz |
| US7413657B1 (en) * | 2003-12-02 | 2008-08-19 | Porous Media Ltd. | Method for selective extraction |
| DE102011078544A1 (de) * | 2011-07-01 | 2013-01-03 | Wacker Chemie Ag | Verfahren zur Herstellung von Organopolysiloxanen |
| JP6788862B2 (ja) * | 2016-01-12 | 2020-11-25 | 東レ・ファインケミカル株式会社 | シリコーン重合体の製造方法 |
| CN115894925B (zh) * | 2021-09-22 | 2024-04-02 | 深圳市埃派尔贸易有限公司 | 高沸硅油及其生产方法 |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3395117A (en) * | 1966-04-27 | 1968-07-30 | Owens Illinois Inc | Organopolysiloxane compositions and processes for the preparation of the same |
| US4218354A (en) * | 1974-03-22 | 1980-08-19 | Stauffer Chemical Company | Binder composition and coating containing the same |
| JPS5964671A (ja) * | 1982-10-05 | 1984-04-12 | Kansai Paint Co Ltd | 無機質塗膜の形成方法 |
| US4605446A (en) * | 1983-12-01 | 1986-08-12 | Kansai Paint Company, Limited | Process for preparing organosilicon high condensation products |
| JPS61195129A (ja) * | 1985-02-22 | 1986-08-29 | Toray Silicone Co Ltd | 有機けい素重合体の製造方法 |
| JPH078913B2 (ja) * | 1987-06-03 | 1995-02-01 | 信越化学工業株式会社 | オルガノポリシロキサンの製造方法 |
| JPH0633335B2 (ja) * | 1990-05-29 | 1994-05-02 | 信越化学工業株式会社 | オルガノポリシロキサンの製造方法 |
| DE4132697A1 (de) * | 1991-10-01 | 1993-04-08 | Wacker Chemie Gmbh | Verfahren zur herstellung von organopolysiloxanharz |
| US5210168A (en) * | 1992-04-02 | 1993-05-11 | Dow Corning Corporation | Process for forming siloxane bonds |
| US5548053A (en) * | 1992-05-15 | 1996-08-20 | Wacker-Chemie Gmbh | Process for the preparation of organopolysiloxane resin |
-
1992
- 1992-12-23 DE DE4243895A patent/DE4243895A1/de not_active Withdrawn
-
1993
- 1993-12-13 US US08/165,788 patent/US5401821A/en not_active Expired - Fee Related
- 1993-12-15 FI FI935632A patent/FI935632A7/fi unknown
- 1993-12-16 EP EP93120313A patent/EP0604847B1/de not_active Expired - Lifetime
- 1993-12-16 DE DE59301108T patent/DE59301108D1/de not_active Expired - Fee Related
- 1993-12-16 ES ES93120313T patent/ES2080575T3/es not_active Expired - Lifetime
- 1993-12-17 CA CA002111728A patent/CA2111728C/en not_active Expired - Fee Related
- 1993-12-22 JP JP5324499A patent/JP2596706B2/ja not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| CA2111728A1 (en) | 1994-06-24 |
| DE4243895A1 (de) | 1994-06-30 |
| US5401821A (en) | 1995-03-28 |
| DE59301108D1 (de) | 1996-01-18 |
| JP2596706B2 (ja) | 1997-04-02 |
| EP0604847B1 (de) | 1995-12-06 |
| FI935632A7 (fi) | 1994-06-24 |
| JPH06220196A (ja) | 1994-08-09 |
| CA2111728C (en) | 1997-11-25 |
| EP0604847A1 (de) | 1994-07-06 |
| FI935632A0 (fi) | 1993-12-15 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG2A | Definitive protection |
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