ES2105982A1 - Zeolita itq-1 - Google Patents

Zeolita itq-1

Info

Publication number
ES2105982A1
ES2105982A1 ES09502306A ES9502306A ES2105982A1 ES 2105982 A1 ES2105982 A1 ES 2105982A1 ES 09502306 A ES09502306 A ES 09502306A ES 9502306 A ES9502306 A ES 9502306A ES 2105982 A1 ES2105982 A1 ES 2105982A1
Authority
ES
Spain
Prior art keywords
preparation
equal
value smaller
chemical element
oxidation status
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
ES09502306A
Other languages
English (en)
Other versions
ES2105982B1 (es
Inventor
Cabanas M Jose Diaz
Fernandez Miguel Angel Camblor
Martires Catalina Corell
Camos Avelino Corma
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Consejo Superior de Investigaciones Cientificas CSIC
Universidad Politecnica de Valencia
Original Assignee
Consejo Superior de Investigaciones Cientificas CSIC
Universidad Politecnica de Valencia
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to ES09502306A priority Critical patent/ES2105982B1/es
Application filed by Consejo Superior de Investigaciones Cientificas CSIC, Universidad Politecnica de Valencia filed Critical Consejo Superior de Investigaciones Cientificas CSIC
Priority to AT96939937T priority patent/ATE206688T1/de
Priority to ES96939937T priority patent/ES2165531T3/es
Priority to PCT/ES1996/000218 priority patent/WO1997019021A1/es
Priority to EP96939937A priority patent/EP0818417B1/en
Priority to DK96939937T priority patent/DK0818417T3/da
Priority to US08/875,302 priority patent/US6077498A/en
Priority to DE69615830T priority patent/DE69615830T2/de
Publication of ES2105982A1 publication Critical patent/ES2105982A1/es
Application granted granted Critical
Publication of ES2105982B1 publication Critical patent/ES2105982B1/es
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G47/00—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions
    • C10G47/02—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions characterised by the catalyst used
    • C10G47/10—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions characterised by the catalyst used with catalysts deposited on a carrier
    • C10G47/12—Inorganic carriers
    • C10G47/16—Crystalline alumino-silicate carriers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/03—Catalysts comprising molecular sieves not having base-exchange properties
    • B01J29/035—Microporous crystalline materials not having base exchange properties, such as silica polymorphs, e.g. silicalites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B37/00—Compounds having molecular sieve properties but not having base-exchange properties
    • C01B37/005—Silicates, i.e. so-called metallosilicalites or metallozeosilites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B37/00—Compounds having molecular sieve properties but not having base-exchange properties
    • C01B37/02—Crystalline silica-polymorphs, e.g. silicalites dealuminated aluminosilicate zeolites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
    • C01B39/48—Other types characterised by their X-ray diffraction pattern and their defined composition using at least one organic template directing agent
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C4/00—Preparation of hydrocarbons from hydrocarbons containing a larger number of carbon atoms
    • C07C4/02—Preparation of hydrocarbons from hydrocarbons containing a larger number of carbon atoms by cracking a single hydrocarbon or a mixture of individually defined hydrocarbons or a normally gaseous hydrocarbon fraction
    • C07C4/06—Catalytic processes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C5/00—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms
    • C07C5/22—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms by isomerisation
    • C07C5/27—Rearrangement of carbon atoms in the hydrocarbon skeleton
    • C07C5/2767—Changing the number of side-chains
    • C07C5/277—Catalytic processes
    • C07C5/2775—Catalytic processes with crystalline alumino-silicates, e.g. molecular sieves
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/12—Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers
    • C07C7/13—Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers by molecular-sieve technique
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G11/00—Catalytic cracking, in the absence of hydrogen, of hydrocarbon oils
    • C10G11/02—Catalytic cracking, in the absence of hydrogen, of hydrocarbon oils characterised by the catalyst used
    • C10G11/04—Oxides
    • C10G11/05—Crystalline alumino-silicates, e.g. molecular sieves
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G45/00—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds
    • C10G45/58—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to change the structural skeleton of some of the hydrocarbon content without cracking the other hydrocarbons present, e.g. lowering pour point; Selective hydrocracking of normal paraffins
    • C10G45/60—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to change the structural skeleton of some of the hydrocarbon content without cracking the other hydrocarbons present, e.g. lowering pour point; Selective hydrocracking of normal paraffins characterised by the catalyst used
    • C10G45/64—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to change the structural skeleton of some of the hydrocarbon content without cracking the other hydrocarbons present, e.g. lowering pour point; Selective hydrocracking of normal paraffins characterised by the catalyst used containing crystalline alumino-silicates, e.g. molecular sieves
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2529/00—Catalysts comprising molecular sieves
    • C07C2529/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites, pillared clays
    • C07C2529/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • C07C2529/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups C07C2529/08 - C07C2529/65

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Inorganic Chemistry (AREA)
  • Materials Engineering (AREA)
  • General Chemical & Material Sciences (AREA)
  • Geology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Water Supply & Treatment (AREA)
  • Analytical Chemistry (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Saccharide Compounds (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)

Abstract

ZEOLITA ITQ-1. LA PRESENTE INVENCION SE REFIERE A UN MATERIAL CRISTALINO MICROPOROSO DE NATURALEZA ZEOLITICA DENOMINADO ITQ-1, AL PROCEDIMIENTO DE SU PREPARACION Y A SU UTILIZACION EN PROCESOS DE SEPARACION Y TRANSFORMACION DE COMPUESTOS ORGANICOS. EL ESTADO CALCINADO Y ANHIDRO, LA COMPOSICION QUIMICA DEL MATERIAL CORRESPONDE A LA FORMULA EMPIRICA: X(M1/NXO2): Y YO2:SIO2 DONDE X POSEE UN VALOR INFERIOR A 0,02, PUDIENDO SER IGUAL A CERO; Y TIENE UN VALOR INFERIOR A 0,04, PUDIENDO SER IGUAL A CERO; M ES H+ O UN CATION INORGANICO DE CARGA +N; X ES UN ELEMENTO QUIMICO DE ESTADO DE OXIDACION +3 (AL, GA, B, CR) E Y ES UN ELEMENTO QUIMICO CON ESTADO DE OXIDACION +4 (TI, GE, V). CUANDO X = 0 E Y =0 EL MATERIAL PUEDE DESCRIBIRSE COMO UNA NUEVA FORMA POLIMORFICA DE LA SILICE DE CARACTER MICROPOROSO. EL MATERIAL DE ESTA INVENCION SE CARACTERIZA TAMBIEN POR SU PATRON DE DIFRACCION DE RAYOS X. EL PROCESO DE PREPARACION SE CARACTERIZA POR EL USO DE UNO O VARIOS ADITIVOS ORGANICOS A UNA MEZCLA DE REACCIONQUE SE HACE CRISTALIZAR MEDIANTE CALENTAMIENTO.
ES09502306A 1995-11-23 1995-11-23 Zeolita itq-1 Expired - Fee Related ES2105982B1 (es)

Priority Applications (8)

Application Number Priority Date Filing Date Title
ES09502306A ES2105982B1 (es) 1995-11-23 1995-11-23 Zeolita itq-1
ES96939937T ES2165531T3 (es) 1995-11-23 1996-11-19 Zeolita itq-1.
PCT/ES1996/000218 WO1997019021A1 (es) 1995-11-23 1996-11-19 Zeolita itq-1
EP96939937A EP0818417B1 (en) 1995-11-23 1996-11-19 Zeolite itq-1
AT96939937T ATE206688T1 (de) 1995-11-23 1996-11-19 Zeolith itq-1
DK96939937T DK0818417T3 (da) 1995-11-23 1996-11-19 Zeolit
US08/875,302 US6077498A (en) 1995-11-23 1996-11-19 Zeolite ITQ-1
DE69615830T DE69615830T2 (de) 1995-11-23 1996-11-19 Zeolith itq-1

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
ES09502306A ES2105982B1 (es) 1995-11-23 1995-11-23 Zeolita itq-1

Publications (2)

Publication Number Publication Date
ES2105982A1 true ES2105982A1 (es) 1997-10-16
ES2105982B1 ES2105982B1 (es) 1998-07-01

Family

ID=8292268

Family Applications (2)

Application Number Title Priority Date Filing Date
ES09502306A Expired - Fee Related ES2105982B1 (es) 1995-11-23 1995-11-23 Zeolita itq-1
ES96939937T Expired - Lifetime ES2165531T3 (es) 1995-11-23 1996-11-19 Zeolita itq-1.

Family Applications After (1)

Application Number Title Priority Date Filing Date
ES96939937T Expired - Lifetime ES2165531T3 (es) 1995-11-23 1996-11-19 Zeolita itq-1.

Country Status (7)

Country Link
US (1) US6077498A (es)
EP (1) EP0818417B1 (es)
AT (1) ATE206688T1 (es)
DE (1) DE69615830T2 (es)
DK (1) DK0818417T3 (es)
ES (2) ES2105982B1 (es)
WO (1) WO1997019021A1 (es)

Families Citing this family (285)

* Cited by examiner, † Cited by third party
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US6077498A (en) 2000-06-20
ES2165531T3 (es) 2002-03-16
ES2105982B1 (es) 1998-07-01
ATE206688T1 (de) 2001-10-15
WO1997019021A1 (es) 1997-05-29
DE69615830T2 (de) 2002-04-25
EP0818417B1 (en) 2001-10-10
DE69615830D1 (de) 2001-11-15
DK0818417T3 (da) 2002-02-04

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