JPH01108123A - ハロゲン化銀乳剤の製造方法 - Google Patents

ハロゲン化銀乳剤の製造方法

Info

Publication number: JPH01108123A
Authority: JP; Japan
Prior art keywords: group; silver halide; oxidizing agent; silver; emulsion
Prior art date: 1987-10-19
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Granted

Application number

JP26332387A

Other languages

English (en)

Japanese (ja)

Other versions

JPH0563411B2 (2

Inventor

Yoshihiro Takagi

良博高木

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Fujifilm Holdings Corp

Original Assignee

Fuji Photo Film Co Ltd

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1987-10-19

Filing date

1987-10-19

Publication date

1989-04-25

1987-10-19 Application filed by Fuji Photo Film Co Ltd filed Critical Fuji Photo Film Co Ltd

1987-10-19 Priority to JP26332387A priority Critical patent/JPH01108123A/ja

1989-04-25 Publication of JPH01108123A publication Critical patent/JPH01108123A/ja

1993-09-10 Publication of JPH0563411B2 publication Critical patent/JPH0563411B2/ja

Status Granted legal-status Critical Current

Links

-1 silver halide Chemical class 0.000 title claims abstract description 215
229910052709 silver Inorganic materials 0.000 title claims abstract description 80
239000004332 silver Substances 0.000 title claims abstract description 79
239000000839 emulsion Substances 0.000 title claims abstract description 60
238000004519 manufacturing process Methods 0.000 title claims abstract description 8
108010010803 Gelatin Proteins 0.000 claims abstract description 35
239000008273 gelatin Substances 0.000 claims abstract description 35
229920000159 gelatin Polymers 0.000 claims abstract description 35
235000019322 gelatine Nutrition 0.000 claims abstract description 35
235000011852 gelatine desserts Nutrition 0.000 claims abstract description 35
239000007800 oxidant agent Substances 0.000 claims abstract description 34
238000004062 sedimentation Methods 0.000 claims abstract description 30
238000011033 desalting Methods 0.000 claims abstract description 9
239000003513 alkali Substances 0.000 claims abstract description 6
238000002360 preparation method Methods 0.000 claims abstract description 6
238000001556 precipitation Methods 0.000 claims description 10
238000005189 flocculation Methods 0.000 claims description 2
230000016615 flocculation Effects 0.000 claims description 2
238000000034 method Methods 0.000 abstract description 51
239000002245 particle Substances 0.000 abstract description 31
230000008569 process Effects 0.000 abstract description 18
MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 abstract description 8
230000001590 oxidative effect Effects 0.000 abstract description 5
KFSLWBXXFJQRDL-UHFFFAOYSA-N Peracetic acid Chemical compound CC(=O)OO KFSLWBXXFJQRDL-UHFFFAOYSA-N 0.000 abstract description 4
PCLIMKBDDGJMGD-UHFFFAOYSA-N N-bromosuccinimide Chemical compound BrN1C(=O)CCC1=O PCLIMKBDDGJMGD-UHFFFAOYSA-N 0.000 abstract description 3
238000004904 shortening Methods 0.000 abstract description 2
239000012286 potassium permanganate Substances 0.000 abstract 1
239000000463 material Substances 0.000 description 44
239000000975 dye Substances 0.000 description 28
150000001875 compounds Chemical class 0.000 description 27
125000004432 carbon atom Chemical group C* 0.000 description 21
125000000623 heterocyclic group Chemical group 0.000 description 21
239000003795 chemical substances by application Substances 0.000 description 20
125000000217 alkyl group Chemical group 0.000 description 17
238000011161 development Methods 0.000 description 17
OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical compound NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 description 15
238000012545 processing Methods 0.000 description 14
150000003839 salts Chemical class 0.000 description 14
239000010410 layer Substances 0.000 description 13
229910021607 Silver chloride Inorganic materials 0.000 description 12
HKZLPVFGJNLROG-UHFFFAOYSA-M silver monochloride Chemical compound [Cl-].[Ag+] HKZLPVFGJNLROG-UHFFFAOYSA-M 0.000 description 12
125000003118 aryl group Chemical group 0.000 description 11
230000015572 biosynthetic process Effects 0.000 description 11
230000035945 sensitivity Effects 0.000 description 11
125000001424 substituent group Chemical group 0.000 description 11
BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 10
125000001931 aliphatic group Chemical group 0.000 description 10
239000007864 aqueous solution Substances 0.000 description 10
WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 9
125000003277 amino group Chemical group 0.000 description 9
229910052799 carbon Inorganic materials 0.000 description 9
239000013078 crystal Substances 0.000 description 9
230000007423 decrease Effects 0.000 description 9
150000002429 hydrazines Chemical class 0.000 description 9
125000004435 hydrogen atom Chemical group [H]* 0.000 description 9
239000007788 liquid Substances 0.000 description 9
229910052757 nitrogen Inorganic materials 0.000 description 9
150000003283 rhodium Chemical class 0.000 description 9
125000002252 acyl group Chemical group 0.000 description 8
125000003545 alkoxy group Chemical group 0.000 description 8
239000000084 colloidal system Substances 0.000 description 8
125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 8
230000001965 increasing effect Effects 0.000 description 7
230000005070 ripening Effects 0.000 description 7
229910052717 sulfur Inorganic materials 0.000 description 7
CDAWCLOXVUBKRW-UHFFFAOYSA-N 2-aminophenol Chemical class NC1=CC=CC=C1O CDAWCLOXVUBKRW-UHFFFAOYSA-N 0.000 description 6
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 6
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 6
QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 6
239000002202 Polyethylene glycol Substances 0.000 description 6
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
239000002253 acid Substances 0.000 description 6
125000003342 alkenyl group Chemical group 0.000 description 6
125000003236 benzoyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C(*)=O 0.000 description 6
125000003917 carbamoyl group Chemical group [H]N([H])C(*)=O 0.000 description 6
229910052736 halogen Inorganic materials 0.000 description 6
229920001223 polyethylene glycol Polymers 0.000 description 6
ANRHNWWPFJCPAZ-UHFFFAOYSA-M thionine Chemical compound [Cl-].C1=CC(N)=CC2=[S+]C3=CC(N)=CC=C3N=C21 ANRHNWWPFJCPAZ-UHFFFAOYSA-M 0.000 description 6
125000002777 acetyl group Chemical group [H]C([H])([H])C(*)=O 0.000 description 5
229910052783 alkali metal Inorganic materials 0.000 description 5
150000001412 amines Chemical class 0.000 description 5
125000004397 aminosulfonyl group Chemical group NS(=O)(=O)* 0.000 description 5
IOJUPLGTWVMSFF-UHFFFAOYSA-N benzothiazole Chemical group C1=CC=C2SC=NC2=C1 IOJUPLGTWVMSFF-UHFFFAOYSA-N 0.000 description 5
125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 5
125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 5
150000002367 halogens Chemical class 0.000 description 5
125000002887 hydroxy group Chemical group [H]O* 0.000 description 5
239000003112 inhibitor Substances 0.000 description 5
125000005647 linker group Chemical group 0.000 description 5
125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 5
238000002156 mixing Methods 0.000 description 5
239000000203 mixture Substances 0.000 description 5
125000004433 nitrogen atom Chemical group N* 0.000 description 5
239000000243 solution Substances 0.000 description 5
125000000565 sulfonamide group Chemical group 0.000 description 5
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
JKFYKCYQEWQPTM-UHFFFAOYSA-N 2-azaniumyl-2-(4-fluorophenyl)acetate Chemical compound OC(=O)C(N)C1=CC=C(F)C=C1 JKFYKCYQEWQPTM-UHFFFAOYSA-N 0.000 description 4
QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 4
QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 4
229910019142 PO4 Inorganic materials 0.000 description 4
229910021612 Silver iodide Inorganic materials 0.000 description 4
FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 4
NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 4
239000000654 additive Substances 0.000 description 4
150000001340 alkali metals Chemical group 0.000 description 4
125000003710 aryl alkyl group Chemical group 0.000 description 4
150000001565 benzotriazoles Chemical class 0.000 description 4
125000001951 carbamoylamino group Chemical group C(N)(=O)N* 0.000 description 4
125000005521 carbonamide group Chemical group 0.000 description 4
230000000694 effects Effects 0.000 description 4
125000002485 formyl group Chemical group [H]C(*)=O 0.000 description 4
125000005843 halogen group Chemical group 0.000 description 4
DZVCFNFOPIZQKX-LTHRDKTGSA-M merocyanine Chemical compound [Na+].O=C1N(CCCC)C(=O)N(CCCC)C(=O)C1=C\C=C\C=C/1N(CCCS([O-])(=O)=O)C2=CC=CC=C2O\1 DZVCFNFOPIZQKX-LTHRDKTGSA-M 0.000 description 4
125000002950 monocyclic group Chemical group 0.000 description 4
230000003647 oxidation Effects 0.000 description 4
238000007254 oxidation reaction Methods 0.000 description 4
235000021317 phosphate Nutrition 0.000 description 4
IOLCXVTUBQKXJR-UHFFFAOYSA-M potassium bromide Chemical compound [K+].[Br-] IOLCXVTUBQKXJR-UHFFFAOYSA-M 0.000 description 4
NDGRWYRVNANFNB-UHFFFAOYSA-N pyrazolidin-3-one Chemical class O=C1CCNN1 NDGRWYRVNANFNB-UHFFFAOYSA-N 0.000 description 4
ADZWSOLPGZMUMY-UHFFFAOYSA-M silver bromide Chemical compound [Ag]Br ADZWSOLPGZMUMY-UHFFFAOYSA-M 0.000 description 4
229940045105 silver iodide Drugs 0.000 description 4
SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical compound [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 description 4
238000003860 storage Methods 0.000 description 4
239000011593 sulfur Substances 0.000 description 4
239000006228 supernatant Substances 0.000 description 4
150000003852 triazoles Chemical group 0.000 description 4
238000005406 washing Methods 0.000 description 4
KJCVRFUGPWSIIH-UHFFFAOYSA-N 1-naphthol Chemical compound C1=CC=C2C(O)=CC=CC2=C1 KJCVRFUGPWSIIH-UHFFFAOYSA-N 0.000 description 3
125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 description 3
QDHHCQZDFGDHMP-UHFFFAOYSA-N Chloramine Chemical compound ClN QDHHCQZDFGDHMP-UHFFFAOYSA-N 0.000 description 3
229940090898 Desensitizer Drugs 0.000 description 3
229920003171 Poly (ethylene oxide) Chemical class 0.000 description 3
KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
206010070834 Sensitisation Diseases 0.000 description 3
SJOOOZPMQAWAOP-UHFFFAOYSA-N [Ag].BrCl Chemical compound [Ag].BrCl SJOOOZPMQAWAOP-UHFFFAOYSA-N 0.000 description 3
125000004390 alkyl sulfonyl group Chemical group 0.000 description 3
125000003785 benzimidazolyl group Chemical group N1=C(NC2=C1C=CC=C2)* 0.000 description 3
125000001797 benzyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])* 0.000 description 3
125000002619 bicyclic group Chemical group 0.000 description 3
230000008859 change Effects 0.000 description 3
239000011248 coating agent Substances 0.000 description 3
238000000576 coating method Methods 0.000 description 3
125000000113 cyclohexyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C([H])([H])C1([H])[H] 0.000 description 3
150000005205 dihydroxybenzenes Chemical class 0.000 description 3
239000010419 fine particle Substances 0.000 description 3
239000007789 gas Substances 0.000 description 3
RAXXELZNTBOGNW-UHFFFAOYSA-N imidazole Natural products C1=CNC=N1 RAXXELZNTBOGNW-UHFFFAOYSA-N 0.000 description 3
150000002460 imidazoles Chemical class 0.000 description 3
125000002883 imidazolyl group Chemical group 0.000 description 3
230000006872 improvement Effects 0.000 description 3
239000002184 metal Chemical class 0.000 description 3
229910052751 metal Inorganic materials 0.000 description 3
125000000956 methoxy group Chemical group [H]C([H])([H])O* 0.000 description 3
125000001160 methoxycarbonyl group Chemical group [H]C([H])([H])OC(*)=O 0.000 description 3
125000004170 methylsulfonyl group Chemical group [H]C([H])([H])S(*)(=O)=O 0.000 description 3
230000006911 nucleation Effects 0.000 description 3
238000010899 nucleation Methods 0.000 description 3
230000036961 partial effect Effects 0.000 description 3
125000006678 phenoxycarbonyl group Chemical group 0.000 description 3
125000001501 propionyl group Chemical group O=C([*])C([H])([H])C([H])([H])[H] 0.000 description 3
125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 3
230000001681 protective effect Effects 0.000 description 3
238000011160 research Methods 0.000 description 3
239000010948 rhodium Substances 0.000 description 3
229920006395 saturated elastomer Polymers 0.000 description 3
230000008313 sensitization Effects 0.000 description 3
ZUNKMNLKJXRCDM-UHFFFAOYSA-N silver bromoiodide Chemical compound [Ag].IBr ZUNKMNLKJXRCDM-UHFFFAOYSA-N 0.000 description 3
229910052708 sodium Inorganic materials 0.000 description 3
239000011734 sodium Substances 0.000 description 3
239000000126 substance Substances 0.000 description 3
125000000020 sulfo group Chemical group O=S(=O)([*])O[H] 0.000 description 3
125000004434 sulfur atom Chemical group 0.000 description 3
150000003536 tetrazoles Chemical class 0.000 description 3
238000012546 transfer Methods 0.000 description 3
229910052724 xenon Inorganic materials 0.000 description 3
FHNFHKCVQCLJFQ-UHFFFAOYSA-N xenon atom Chemical compound [Xe] FHNFHKCVQCLJFQ-UHFFFAOYSA-N 0.000 description 3
150000005208 1,4-dihydroxybenzenes Chemical class 0.000 description 2
125000001731 2-cyanoethyl group Chemical group [H]C([H])(*)C([H])([H])C#N 0.000 description 2
125000000094 2-phenylethyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])C([H])([H])* 0.000 description 2
OWIRCRREDNEXTA-UHFFFAOYSA-N 3-nitro-1h-indazole Chemical class C1=CC=C2C([N+](=O)[O-])=NNC2=C1 OWIRCRREDNEXTA-UHFFFAOYSA-N 0.000 description 2
LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 2
WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical group [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 2
MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 2
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 2
ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 2
NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
239000004372 Polyvinyl alcohol Substances 0.000 description 2
JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical group C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 2
QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 2
LSNNMFCWUKXFEE-UHFFFAOYSA-N Sulfurous acid Chemical compound OS(O)=O LSNNMFCWUKXFEE-UHFFFAOYSA-N 0.000 description 2
FZWLAAWBMGSTSO-UHFFFAOYSA-N Thiazole Chemical group C1=CSC=N1 FZWLAAWBMGSTSO-UHFFFAOYSA-N 0.000 description 2
125000003668 acetyloxy group Chemical group [H]C([H])([H])C(=O)O[*] 0.000 description 2
230000002378 acidificating effect Effects 0.000 description 2
150000007513 acids Chemical class 0.000 description 2
230000009471 action Effects 0.000 description 2
125000004442 acylamino group Chemical group 0.000 description 2
125000004423 acyloxy group Chemical group 0.000 description 2
229910052784 alkaline earth metal Inorganic materials 0.000 description 2
150000001342 alkaline earth metals Chemical class 0.000 description 2
125000004453 alkoxycarbonyl group Chemical group 0.000 description 2
125000005138 alkoxysulfonyl group Chemical group 0.000 description 2
150000005215 alkyl ethers Chemical class 0.000 description 2
125000004414 alkyl thio group Chemical group 0.000 description 2
125000002947 alkylene group Chemical group 0.000 description 2
229910021529 ammonia Inorganic materials 0.000 description 2
229920006318 anionic polymer Polymers 0.000 description 2
125000004391 aryl sulfonyl group Chemical group 0.000 description 2
125000004429 atom Chemical group 0.000 description 2
JEHKKBHWRAXMCH-UHFFFAOYSA-N benzenesulfinic acid Chemical compound O[S@@](=O)C1=CC=CC=C1 JEHKKBHWRAXMCH-UHFFFAOYSA-N 0.000 description 2
125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 2
150000001721 carbon Chemical group 0.000 description 2
239000001913 cellulose Substances 0.000 description 2
229920002678 cellulose Polymers 0.000 description 2
235000010980 cellulose Nutrition 0.000 description 2
229910052801 chlorine Inorganic materials 0.000 description 2
125000001309 chloro group Chemical group Cl* 0.000 description 2
239000011651 chromium Substances 0.000 description 2
229920001577 copolymer Polymers 0.000 description 2
238000005859 coupling reaction Methods 0.000 description 2
125000004093 cyano group Chemical group *C#N 0.000 description 2
125000006165 cyclic alkyl group Chemical group 0.000 description 2
125000004122 cyclic group Chemical group 0.000 description 2
239000006185 dispersion Substances 0.000 description 2
238000004945 emulsification Methods 0.000 description 2
230000002708 enhancing effect Effects 0.000 description 2
125000001301 ethoxy group Chemical group [H]C([H])([H])C([H])([H])O* 0.000 description 2
230000001747 exhibiting effect Effects 0.000 description 2
229910052731 fluorine Inorganic materials 0.000 description 2
LNTHITQWFMADLM-UHFFFAOYSA-N gallic acid Chemical class OC(=O)C1=CC(O)=C(O)C(O)=C1 LNTHITQWFMADLM-UHFFFAOYSA-N 0.000 description 2
LEQAOMBKQFMDFZ-UHFFFAOYSA-N glyoxal Chemical compound O=CC=O LEQAOMBKQFMDFZ-UHFFFAOYSA-N 0.000 description 2
125000001072 heteroaryl group Chemical group 0.000 description 2
125000005842 heteroatom Chemical group 0.000 description 2
125000004836 hexamethylene group Chemical group [H]C([H])([*:2])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[*:1] 0.000 description 2
150000007857 hydrazones Chemical class 0.000 description 2
208000015181 infectious disease Diseases 0.000 description 2
230000002458 infectious effect Effects 0.000 description 2
125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 2
229910052744 lithium Inorganic materials 0.000 description 2
125000004573 morpholin-4-yl group Chemical group N1(CCOCC1)* 0.000 description 2
125000004108 n-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 2
125000001624 naphthyl group Chemical group 0.000 description 2
229910000510 noble metal Inorganic materials 0.000 description 2
125000005740 oxycarbonyl group Chemical group [*:1]OC([*:2])=O 0.000 description 2
229910052760 oxygen Inorganic materials 0.000 description 2
239000001301 oxygen Substances 0.000 description 2
125000004430 oxygen atom Chemical group O* 0.000 description 2
239000012071 phase Substances 0.000 description 2
125000000951 phenoxy group Chemical group [H]C1=C([H])C([H])=C(O*)C([H])=C1[H] 0.000 description 2
125000003170 phenylsulfonyl group Chemical group C1(=CC=CC=C1)S(=O)(=O)* 0.000 description 2
150000004714 phosphonium salts Chemical group 0.000 description 2
229920000233 poly(alkylene oxides) Polymers 0.000 description 2
229920000728 polyester Polymers 0.000 description 2
239000004848 polyfunctional curative Substances 0.000 description 2
229920000642 polymer Polymers 0.000 description 2
229920002451 polyvinyl alcohol Polymers 0.000 description 2
230000001376 precipitating effect Effects 0.000 description 2
239000003755 preservative agent Substances 0.000 description 2
230000002335 preservative effect Effects 0.000 description 2
230000002265 prevention Effects 0.000 description 2
230000001737 promoting effect Effects 0.000 description 2
125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 2
150000003242 quaternary ammonium salts Chemical class 0.000 description 2
230000009467 reduction Effects 0.000 description 2
SONJTKJMTWTJCT-UHFFFAOYSA-K rhodium(iii) chloride Chemical compound [Cl-].[Cl-].[Cl-].[Rh+3] SONJTKJMTWTJCT-UHFFFAOYSA-K 0.000 description 2
230000001235 sensitizing effect Effects 0.000 description 2
229910001961 silver nitrate Inorganic materials 0.000 description 2
239000011780 sodium chloride Substances 0.000 description 2
HIEHAIZHJZLEPQ-UHFFFAOYSA-M sodium;naphthalene-1-sulfonate Chemical compound [Na+].C1=CC=C2C(S(=O)(=O)[O-])=CC=CC2=C1 HIEHAIZHJZLEPQ-UHFFFAOYSA-M 0.000 description 2
239000002904 solvent Substances 0.000 description 2
238000001179 sorption measurement Methods 0.000 description 2
125000005504 styryl group Chemical group 0.000 description 2
BUUPQKDIAURBJP-UHFFFAOYSA-N sulfinic acid Chemical compound OS=O BUUPQKDIAURBJP-UHFFFAOYSA-N 0.000 description 2
LSNNMFCWUKXFEE-UHFFFAOYSA-L sulfite Chemical compound [O-]S([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-L 0.000 description 2
239000004094 surface-active agent Substances 0.000 description 2
125000000999 tert-butyl group Chemical group [H]C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 description 2
125000000383 tetramethylene group Chemical group [H]C([H])([*:1])C([H])([H])C([H])([H])C([H])([H])[*:2] 0.000 description 2
VLLMWSRANPNYQX-UHFFFAOYSA-N thiadiazole Chemical compound C1=CSN=N1.C1=CSN=N1 VLLMWSRANPNYQX-UHFFFAOYSA-N 0.000 description 2
125000003441 thioacyl group Chemical group 0.000 description 2
125000005323 thioketone group Chemical group 0.000 description 2
150000004764 thiosulfuric acid derivatives Chemical class 0.000 description 2
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ZAKLKBFCSHJIRI-UHFFFAOYSA-N mucochloric acid Natural products OC1OC(=O)C(Cl)=C1Cl ZAKLKBFCSHJIRI-UHFFFAOYSA-N 0.000 description 1
125000004123 n-propyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
PSZYNBSKGUBXEH-UHFFFAOYSA-N naphthalene-1-sulfonic acid Chemical compound C1=CC=C2C(S(=O)(=O)O)=CC=CC2=C1 PSZYNBSKGUBXEH-UHFFFAOYSA-N 0.000 description 1
125000004957 naphthylene group Chemical group 0.000 description 1
230000007935 neutral effect Effects 0.000 description 1
125000000449 nitro group Chemical group [O-][N+](*)=O 0.000 description 1
239000002736 nonionic surfactant Substances 0.000 description 1
125000003261 o-tolyl group Chemical group [H]C1=C([H])C(*)=C(C([H])=C1[H])C([H])([H])[H] 0.000 description 1
239000003921 oil Substances 0.000 description 1
230000003287 optical effect Effects 0.000 description 1
150000001451 organic peroxides Chemical class 0.000 description 1
150000002898 organic sulfur compounds Chemical class 0.000 description 1
WCPAKWJPBJAGKN-UHFFFAOYSA-N oxadiazole Chemical compound C1=CON=N1 WCPAKWJPBJAGKN-UHFFFAOYSA-N 0.000 description 1
150000002916 oxazoles Chemical class 0.000 description 1
238000005691 oxidative coupling reaction Methods 0.000 description 1
QUBQYFYWUJJAAK-UHFFFAOYSA-N oxymethurea Chemical compound OCNC(=O)NCO QUBQYFYWUJJAAK-UHFFFAOYSA-N 0.000 description 1
229950005308 oxymethurea Drugs 0.000 description 1
239000006179 pH buffering agent Substances 0.000 description 1
229910052763 palladium Inorganic materials 0.000 description 1
VLTRZXGMWDSKGL-UHFFFAOYSA-M perchlorate Inorganic materials [O-]Cl(=O)(=O)=O VLTRZXGMWDSKGL-UHFFFAOYSA-M 0.000 description 1
VLTRZXGMWDSKGL-UHFFFAOYSA-N perchloric acid Chemical compound OCl(=O)(=O)=O VLTRZXGMWDSKGL-UHFFFAOYSA-N 0.000 description 1
230000000737 periodic effect Effects 0.000 description 1
125000000864 peroxy group Chemical group O(O*)* 0.000 description 1
CMCWWLVWPDLCRM-UHFFFAOYSA-N phenidone Chemical compound N1C(=O)CCN1C1=CC=CC=C1 CMCWWLVWPDLCRM-UHFFFAOYSA-N 0.000 description 1
125000000843 phenylene group Chemical group C1(=C(C=CC=C1)*)* 0.000 description 1
150000004986 phenylenediamines Chemical class 0.000 description 1
125000003356 phenylsulfanyl group Chemical group [*]SC1=C([H])C([H])=C([H])C([H])=C1[H] 0.000 description 1
239000010452 phosphate Substances 0.000 description 1
XYFCBTPGUUZFHI-UHFFFAOYSA-O phosphonium Chemical compound [PH4+] XYFCBTPGUUZFHI-UHFFFAOYSA-O 0.000 description 1
150000003013 phosphoric acid derivatives Chemical class 0.000 description 1
150000003014 phosphoric acid esters Chemical class 0.000 description 1
238000000206 photolithography Methods 0.000 description 1
125000005936 piperidyl group Chemical group 0.000 description 1
239000004014 plasticizer Substances 0.000 description 1
229920000191 poly(N-vinyl pyrrolidone) Polymers 0.000 description 1
229920002006 poly(N-vinylimidazole) polymer Polymers 0.000 description 1
229920000172 poly(styrenesulfonic acid) Polymers 0.000 description 1
229920002401 polyacrylamide Polymers 0.000 description 1
239000004584 polyacrylic acid Substances 0.000 description 1
229920001515 polyalkylene glycol Polymers 0.000 description 1
229920000120 polyethyl acrylate Polymers 0.000 description 1
229920001451 polypropylene glycol Polymers 0.000 description 1
229920001296 polysiloxane Polymers 0.000 description 1
229920002223 polystyrene Polymers 0.000 description 1
229940005642 polystyrene sulfonic acid Drugs 0.000 description 1
238000012805 post-processing Methods 0.000 description 1
XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 description 1
BHZRJJOHZFYXTO-UHFFFAOYSA-L potassium sulfite Chemical compound [K+].[K+].[O-]S([O-])=O BHZRJJOHZFYXTO-UHFFFAOYSA-L 0.000 description 1
235000019252 potassium sulphite Nutrition 0.000 description 1
239000002243 precursor Substances 0.000 description 1
230000003449 preventive effect Effects 0.000 description 1
239000000047 product Substances 0.000 description 1
125000004368 propenyl group Chemical group C(=CC)* 0.000 description 1
MWWATHDPGQKSAR-UHFFFAOYSA-N propyne Chemical group CC#C MWWATHDPGQKSAR-UHFFFAOYSA-N 0.000 description 1
239000011241 protective layer Substances 0.000 description 1
235000018102 proteins Nutrition 0.000 description 1
108090000623 proteins and genes Proteins 0.000 description 1
102000004169 proteins and genes Human genes 0.000 description 1
150000003217 pyrazoles Chemical class 0.000 description 1
125000003226 pyrazolyl group Chemical group 0.000 description 1
150000003222 pyridines Chemical class 0.000 description 1
JUJWROOIHBZHMG-UHFFFAOYSA-O pyridinium Chemical compound C1=CC=[NH+]C=C1 JUJWROOIHBZHMG-UHFFFAOYSA-O 0.000 description 1
125000004076 pyridyl group Chemical group 0.000 description 1
HBCQSNAFLVXVAY-UHFFFAOYSA-N pyrimidine-2-thiol Chemical class SC1=NC=CC=N1 HBCQSNAFLVXVAY-UHFFFAOYSA-N 0.000 description 1
150000003230 pyrimidines Chemical class 0.000 description 1
125000000714 pyrimidinyl group Chemical group 0.000 description 1
125000001308 pyruvoyl group Chemical group O=C([*])C(=O)C([H])([H])[H] 0.000 description 1
150000003248 quinolines Chemical class 0.000 description 1
125000002943 quinolinyl group Chemical group N1=C(C=CC2=CC=CC=C12)* 0.000 description 1
230000002829 reductive effect Effects 0.000 description 1
KIWUVOGUEXMXSV-UHFFFAOYSA-N rhodanine Chemical compound O=C1CSC(=S)N1 KIWUVOGUEXMXSV-UHFFFAOYSA-N 0.000 description 1
BALRIWPTGHDDFF-UHFFFAOYSA-N rhodium Chemical compound [Rh].[Rh] BALRIWPTGHDDFF-UHFFFAOYSA-N 0.000 description 1
229910052703 rhodium Inorganic materials 0.000 description 1
229930182490 saponin Natural products 0.000 description 1
150000007949 saponins Chemical class 0.000 description 1
235000017709 saponins Nutrition 0.000 description 1
239000004065 semiconductor Substances 0.000 description 1
229910000077 silane Inorganic materials 0.000 description 1
239000000661 sodium alginate Substances 0.000 description 1
235000010413 sodium alginate Nutrition 0.000 description 1
229940005550 sodium alginate Drugs 0.000 description 1
125000004436 sodium atom Chemical group 0.000 description 1
SUKJFIGYRHOWBL-UHFFFAOYSA-N sodium hypochlorite Chemical compound [Na+].Cl[O-] SUKJFIGYRHOWBL-UHFFFAOYSA-N 0.000 description 1
159000000000 sodium salts Chemical class 0.000 description 1
XMVONEAAOPAGAO-UHFFFAOYSA-N sodium tungstate Chemical class [Na+].[Na+].[O-][W]([O-])(=O)=O XMVONEAAOPAGAO-UHFFFAOYSA-N 0.000 description 1
GGCZERPQGJTIQP-UHFFFAOYSA-N sodium;9,10-dioxoanthracene-2-sulfonic acid Chemical compound [Na+].C1=CC=C2C(=O)C3=CC(S(=O)(=O)O)=CC=C3C(=O)C2=C1 GGCZERPQGJTIQP-UHFFFAOYSA-N 0.000 description 1
239000007787 solid Substances 0.000 description 1
230000003595 spectral effect Effects 0.000 description 1
239000003381 stabilizer Substances 0.000 description 1
230000000087 stabilizing effect Effects 0.000 description 1
150000003431 steroids Chemical class 0.000 description 1
150000005846 sugar alcohols Polymers 0.000 description 1
125000004964 sulfoalkyl group Chemical group 0.000 description 1
BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 1
150000003871 sulfonates Chemical class 0.000 description 1
125000001174 sulfone group Chemical group 0.000 description 1
125000000542 sulfonic acid group Chemical group 0.000 description 1
125000000472 sulfonyl group Chemical group *S(*)(=O)=O 0.000 description 1
150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
125000003718 tetrahydrofuranyl group Chemical group 0.000 description 1
125000005958 tetrahydrothienyl group Chemical group 0.000 description 1
125000003831 tetrazolyl group Chemical group 0.000 description 1
150000003475 thallium Chemical class 0.000 description 1
JJJPTTANZGDADF-UHFFFAOYSA-N thiadiazole-4-thiol Chemical class SC1=CSN=N1 JJJPTTANZGDADF-UHFFFAOYSA-N 0.000 description 1
150000003557 thiazoles Chemical class 0.000 description 1
125000000335 thiazolyl group Chemical group 0.000 description 1
125000001391 thioamide group Chemical group 0.000 description 1
150000003567 thiocyanates Chemical class 0.000 description 1
150000003568 thioethers Chemical class 0.000 description 1
125000003396 thiol group Chemical group [H]S* 0.000 description 1
150000004886 thiomorpholines Chemical class 0.000 description 1
UMGDCJDMYOKAJW-UHFFFAOYSA-N thiourea group Chemical group NC(=S)N UMGDCJDMYOKAJW-UHFFFAOYSA-N 0.000 description 1
150000003585 thioureas Chemical class 0.000 description 1
JOXIMZWYDAKGHI-UHFFFAOYSA-M toluene-4-sulfonate Chemical compound CC1=CC=C(S([O-])(=O)=O)C=C1 JOXIMZWYDAKGHI-UHFFFAOYSA-M 0.000 description 1
JOXIMZWYDAKGHI-UHFFFAOYSA-N toluene-4-sulfonic acid Chemical compound CC1=CC=C(S(O)(=O)=O)C=C1 JOXIMZWYDAKGHI-UHFFFAOYSA-N 0.000 description 1
VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
150000003918 triazines Chemical class 0.000 description 1
ITMCEJHCFYSIIV-UHFFFAOYSA-M triflate Chemical compound [O-]S(=O)(=O)C(F)(F)F ITMCEJHCFYSIIV-UHFFFAOYSA-M 0.000 description 1
125000004044 trifluoroacetyl group Chemical group FC(C(=O)*)(F)F 0.000 description 1
GETQZCLCWQTVFV-UHFFFAOYSA-N trimethylamine Chemical group CN(C)C GETQZCLCWQTVFV-UHFFFAOYSA-N 0.000 description 1
WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 1
229910052721 tungsten Inorganic materials 0.000 description 1
239000010937 tungsten Substances 0.000 description 1
239000006097 ultraviolet radiation absorber Substances 0.000 description 1
150000003672 ureas Chemical class 0.000 description 1
150000003673 urethanes Chemical class 0.000 description 1
125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 1
239000002023 wood Substances 0.000 description 1
229910052727 yttrium Inorganic materials 0.000 description 1
150000003751 zinc Chemical class 0.000 description 1

Classifications

- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C1/00—Photosensitive materials
- G03C1/005—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein
- G03C1/04—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein with macromolecular additives; with layer-forming substances
- G03C1/047—Proteins, e.g. gelatine derivatives; Hydrolysis or extraction products of proteins

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Physics & Mathematics (AREA)
Chemical & Material Sciences (AREA)
Spectroscopy & Molecular Physics (AREA)
Chemical Kinetics & Catalysis (AREA)
Engineering & Computer Science (AREA)
Materials Engineering (AREA)
General Physics & Mathematics (AREA)

JP26332387A 1987-10-19 1987-10-19 ハロゲン化銀乳剤の製造方法 Granted JPH01108123A (ja)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
JP26332387A JPH01108123A (ja)	1987-10-19	1987-10-19	ハロゲン化銀乳剤の製造方法

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP26332387A JPH01108123A (ja)	1987-10-19	1987-10-19	ハロゲン化銀乳剤の製造方法

Publications (2)

Publication Number	Publication Date
JPH01108123A true JPH01108123A (ja)	1989-04-25
JPH0563411B2 JPH0563411B2 (2)	1993-09-10

Family

ID=17387878

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP26332387A Granted JPH01108123A (ja)	1987-10-19	1987-10-19	ハロゲン化銀乳剤の製造方法

Country Status (1)

Country	Link
JP (1)	JPH01108123A (2)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPH06130554A (ja) *	1992-10-22	1994-05-13	Fuji Photo Film Co Ltd	ハロゲン化銀写真感光材料およびその処理方法
EP1280005A1 (en) *	2001-07-24	2003-01-29	Fuji Photo Film B.V.	Silver halide emulsion, process for producing silver halide emulsion, and silver halide photographic material

1987
- 1987-10-19 JP JP26332387A patent/JPH01108123A/ja active Granted

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPH06130554A (ja) *	1992-10-22	1994-05-13	Fuji Photo Film Co Ltd	ハロゲン化銀写真感光材料およびその処理方法
EP1280005A1 (en) *	2001-07-24	2003-01-29	Fuji Photo Film B.V.	Silver halide emulsion, process for producing silver halide emulsion, and silver halide photographic material

Also Published As

Publication number	Publication date
JPH0563411B2 (2)	1993-09-10

Legal Events

Date	Code	Title	Description
2004-08-24	R250	Receipt of annual fees	Free format text: JAPANESE INTERMEDIATE CODE: R250
2005-08-23	R250	Receipt of annual fees	Free format text: JAPANESE INTERMEDIATE CODE: R250
2006-08-22	R250	Receipt of annual fees	Free format text: JAPANESE INTERMEDIATE CODE: R250
2007-09-10	LAPS	Cancellation because of no payment of annual fees

Publication	Publication Date	Title
CA1245502A (en)	1988-11-29	Process for producing silver halide emulsion and silver halide photographic light-sensitive material containing the same
US4713321A (en)	1987-12-15	Process for preparing silver halide emulsion utilizing a photographically useful additive capable of being deactivated and a deactivating agent therefor and silver halide photographic material prepared by the process
US4665017A (en)	1987-05-12	Process for preparing silver halide emulsion and silver halide photographic light-sensitive material
JPH028833A (ja)	1990-01-12	ハロゲン化銀写真感光材料
JPS613136A (ja)	1986-01-09	ハロゲン化銀乳剤の製造方法及びハロゲン化銀乳剤
JPS60163042A (ja)	1985-08-24	写真感光材料
JPH0327097B2 (2)	1991-04-12
JPH0518091B2 (2)	1993-03-11
JPH0731381B2 (ja)	1995-04-10	超硬調ネガ型ハロゲン化銀写真感光材料
JPH0215051B2 (2)	1990-04-10
JPS60222843A (ja)	1985-11-07	ハロゲン化銀乳剤の製造方法及びハロゲン化銀写真感光材料
JPS61122642A (ja)	1986-06-10	ハロゲン化銀写真感光材料
JPH0363056B2 (2)	1991-09-27
JPS6258237A (ja)	1987-03-13	ハロゲン化銀乳剤とその製造方法及び該ハロゲン化銀乳剤を用いたハロゲン化銀感光材料
JPH01108123A (ja)	1989-04-25	ハロゲン化銀乳剤の製造方法
JP2709647B2 (ja)	1998-02-04	画像形成方法
JPH0419647A (ja)	1992-01-23	ハロゲン化銀写真感光材料
JPH02293736A (ja)	1990-12-04	ハロゲン化銀写真感光材料
JPS61282834A (ja)	1986-12-13	ハロゲン化銀写真感光材料
JPH03276152A (ja)	1991-12-06	耐圧性が改良されたハロゲン化銀写真感光材料及び処理方法
JPH02124561A (ja)	1990-05-11	ハロゲン化銀写真乳剤
JPH021835A (ja)	1990-01-08	ハロゲン化銀写真感光材料
JPH0545767A (ja)	1993-02-26	ハロゲン化銀写真感光材料
JPH03119348A (ja)	1991-05-21	ハロゲン化銀写真感光材料
JPH03153238A (ja)	1991-07-01	ハロゲン化銀写真感光材料

JPH01108123A - ハロゲン化銀乳剤の製造方法 - Google Patents

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Links

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Priority Applications (1)

Applications Claiming Priority (1)

Publications (2)

Family

ID=17387878

Family Applications (1)

Country Status (1)

Cited By (2)

Cited By (2)

Also Published As

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