JPH0466823B2 - - Google Patents

Info

Publication number: JPH0466823B2
Authority: JP; Japan
Prior art keywords: phosphate; laser glass; gas atmosphere; general formula; glass
Prior art date: 1985-07-12
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

JP15231085A

Other languages

English (en)

Japanese (ja)

Other versions

JPS6217043A (ja

Inventor

Chemi Hata

Koichi Hara

Tetsuo Izumitani

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Hoya Corp

Original Assignee

Hoya Corp

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1985-07-12

Filing date

1985-07-12

Publication date

1992-10-26

1985-07-12 Application filed by Hoya Corp filed Critical Hoya Corp

1985-07-12 Priority to JP15231085A priority Critical patent/JPS6217043A/ja

1986-07-14 Priority to US06/884,907 priority patent/US4816049A/en

1987-01-26 Publication of JPS6217043A publication Critical patent/JPS6217043A/ja

1992-10-26 Publication of JPH0466823B2 publication Critical patent/JPH0466823B2/ja

Status Granted legal-status Critical Current

Links

239000000087 laser glass Substances 0.000 claims description 29
239000011248 coating agent Substances 0.000 claims description 24
238000000576 coating method Methods 0.000 claims description 24
229910019142 PO4 Inorganic materials 0.000 claims description 19
239000010452 phosphate Substances 0.000 claims description 19
NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims description 18
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 14
238000000034 method Methods 0.000 claims description 12
MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 claims description 7
229910001882 dioxygen Inorganic materials 0.000 claims description 7
238000010304 firing Methods 0.000 claims description 7
239000003960 organic solvent Substances 0.000 claims description 7
239000002253 acid Substances 0.000 claims description 6
239000007788 liquid Substances 0.000 claims description 6
229910052751 metal Inorganic materials 0.000 claims description 6
239000002184 metal Substances 0.000 claims description 6
239000000243 solution Substances 0.000 claims description 6
239000011261 inert gas Substances 0.000 claims description 5
150000002902 organometallic compounds Chemical class 0.000 claims description 5
239000011259 mixed solution Substances 0.000 claims description 4
238000002156 mixing Methods 0.000 claims description 4
239000000203 mixture Substances 0.000 claims description 4
230000003301 hydrolyzing effect Effects 0.000 claims description 3
125000000962 organic group Chemical group 0.000 claims description 3
125000000217 alkyl group Chemical group 0.000 claims description 2
229910052726 zirconium Inorganic materials 0.000 claims description 2
239000011521 glass Substances 0.000 description 12
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 9
230000007062 hydrolysis Effects 0.000 description 7
238000006460 hydrolysis reaction Methods 0.000 description 7
239000000126 substance Substances 0.000 description 7
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 6
238000005452 bending Methods 0.000 description 6
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 5
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 5
230000010355 oscillation Effects 0.000 description 5
239000005416 organic matter Substances 0.000 description 4
238000003756 stirring Methods 0.000 description 4
230000008646 thermal stress Effects 0.000 description 4
UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 description 3
239000002826 coolant Substances 0.000 description 3
238000005336 cracking Methods 0.000 description 3
229910001873 dinitrogen Inorganic materials 0.000 description 3
238000001035 drying Methods 0.000 description 3
238000012643 polycondensation polymerization Methods 0.000 description 3
RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 2
YRKCREAYFQTBPV-UHFFFAOYSA-N acetylacetone Chemical compound CC(=O)CC(C)=O YRKCREAYFQTBPV-UHFFFAOYSA-N 0.000 description 2
239000002131 composite material Substances 0.000 description 2
230000006866 deterioration Effects 0.000 description 2
238000007598 dipping method Methods 0.000 description 2
239000007789 gas Substances 0.000 description 2
238000010438 heat treatment Methods 0.000 description 2
230000035939 shock Effects 0.000 description 2
CPUDPFPXCZDNGI-UHFFFAOYSA-N triethoxy(methyl)silane Chemical compound CCO[Si](C)(OCC)OCC CPUDPFPXCZDNGI-UHFFFAOYSA-N 0.000 description 2
GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
230000002378 acidificating effect Effects 0.000 description 1
150000001298 alcohols Chemical class 0.000 description 1
238000006482 condensation reaction Methods 0.000 description 1
238000002845 discoloration Methods 0.000 description 1
230000000694 effects Effects 0.000 description 1
238000005516 engineering process Methods 0.000 description 1
230000005284 excitation Effects 0.000 description 1
238000007654 immersion Methods 0.000 description 1
238000005342 ion exchange Methods 0.000 description 1
BFXIKLCIZHOAAZ-UHFFFAOYSA-N methyltrimethoxysilane Chemical compound CO[Si](C)(OC)OC BFXIKLCIZHOAAZ-UHFFFAOYSA-N 0.000 description 1
229910017604 nitric acid Inorganic materials 0.000 description 1
229910052757 nitrogen Inorganic materials 0.000 description 1
239000005365 phosphate glass Substances 0.000 description 1
150000003013 phosphoric acid derivatives Chemical class 0.000 description 1
238000006116 polymerization reaction Methods 0.000 description 1
BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 1
BCWYYHBWCZYDNB-UHFFFAOYSA-N propan-2-ol;zirconium Chemical compound [Zr].CC(C)O.CC(C)O.CC(C)O.CC(C)O BCWYYHBWCZYDNB-UHFFFAOYSA-N 0.000 description 1
150000003839 salts Chemical class 0.000 description 1
239000002904 solvent Substances 0.000 description 1
230000035882 stress Effects 0.000 description 1
239000000758 substrate Substances 0.000 description 1
238000004381 surface treatment Methods 0.000 description 1
JCVQKRGIASEUKR-UHFFFAOYSA-N triethoxy(phenyl)silane Chemical compound CCO[Si](OCC)(OCC)C1=CC=CC=C1 JCVQKRGIASEUKR-UHFFFAOYSA-N 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C23/00—Other surface treatment of glass not in the form of fibres or filaments
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C15/00—Surface treatment of glass, not in the form of fibres or filaments, by etching
- C03C15/02—Surface treatment of glass, not in the form of fibres or filaments, by etching for making a smooth surface
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/22—Surface treatment of glass, not in the form of fibres or filaments, by coating with other inorganic material
- C03C17/23—Oxides
- C03C17/25—Oxides by deposition from the liquid phase
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2217/00—Coatings on glass
- C03C2217/20—Materials for coating a single layer on glass
- C03C2217/21—Oxides
- C03C2217/229—Non-specific enumeration
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2218/00—Methods for coating glass
- C03C2218/10—Deposition methods
- C03C2218/11—Deposition methods from solutions or suspensions
- C03C2218/113—Deposition methods from solutions or suspensions by sol-gel processes

Landscapes

Chemical & Material Sciences (AREA)
Life Sciences & Earth Sciences (AREA)
Engineering & Computer Science (AREA)
Chemical Kinetics & Catalysis (AREA)
General Chemical & Material Sciences (AREA)
Geochemistry & Mineralogy (AREA)
Materials Engineering (AREA)
Organic Chemistry (AREA)
Surface Treatment Of Glass (AREA)
Lasers (AREA)

JP15231085A 1985-07-12 1985-07-12 リン酸塩系レーザーガラスにガラス質被膜を形成させる方法 Granted JPS6217043A (ja)

Priority Applications (2)

Application Number	Priority Date	Filing Date	Title
JP15231085A JPS6217043A (ja)	1985-07-12	1985-07-12	リン酸塩系レーザーガラスにガラス質被膜を形成させる方法
US06/884,907 US4816049A (en)	1985-07-12	1986-07-14	Process of surface treating laser glass

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP15231085A JPS6217043A (ja)	1985-07-12	1985-07-12	リン酸塩系レーザーガラスにガラス質被膜を形成させる方法

Publications (2)

Publication Number	Publication Date
JPS6217043A JPS6217043A (ja)	1987-01-26
JPH0466823B2 true JPH0466823B2 (fr)	1992-10-26

Family

ID=15537729

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP15231085A Granted JPS6217043A (ja)	1985-07-12	1985-07-12	リン酸塩系レーザーガラスにガラス質被膜を形成させる方法

Country Status (1)

Country	Link
JP (1)	JPS6217043A (fr)

1985
- 1985-07-12 JP JP15231085A patent/JPS6217043A/ja active Granted

Also Published As

Publication number	Publication date
JPS6217043A (ja)	1987-01-26

Publication	Publication Date	Title
US4816049A (en)	1989-03-28	Process of surface treating laser glass
US4547402A (en)	1985-10-15	Method of increasing the thermal shock resistance of phosphate laser glass
JPS6232157A (ja)	1987-02-12	コ−テイング用組成物
JPH0466823B2 (fr)	1992-10-26
US4460654A (en)	1984-07-17	Aluminosilicate coating method, coated articles and organic substituted silicon-oxygen-aluminum oligomers
US5750203A (en)	1998-05-12	Method of preparing organically modified aluminosilcates sol-gel films
JPS63248865A (ja)	1988-10-17	ジルコニア系コ−テイング用組成物
CN107459369A (zh)	2017-12-12	一种利用非水解溶胶‑凝胶工艺在SiC基底上制备ZrSiO4薄膜的方法
US5565245A (en)	1996-10-15	Magnesium doped β-aluminum titanate thin film coating
JPS6150904B2 (fr)	1986-11-06
JPH0466827B2 (fr)	1992-10-26
CN1120865C (zh)	2003-09-10	一种用于金属基板表面涂覆的溶胶及其涂覆方法
JPH06293879A (ja)	1994-10-21	酸化物被膜形成用塗布液および酸化物被膜の製造法
JPS61192771A (ja)	1986-08-27	炭化ケイ素を主成分とするセラミツクコ−テイング剤
JPH03290483A (ja)	1991-12-20	コーティング用組成物
JPH0372609B2 (fr)	1991-11-19
US5407479A (en)	1995-04-18	Sol-gel β-aluminum titanate thin film coating
JPH05805A (ja)	1993-01-08	ゾルゲル法による薄膜の作製方法
JPS6383175A (ja)	1988-04-13	耐アルカリ性に優れたコ−テイング用組成物
JPH01297471A (ja)	1989-11-30	無機耐熱組成物
JPS6295361A (ja)	1987-05-01	コ−テイング用組成物
JPS63207869A (ja)	1988-08-29	耐熱・耐久性に優れた防食・電気絶縁膜を作るコ−テイング用組成物
JP3100704B2 (ja)	2000-10-23	無機質塗膜用封孔処理剤および無機質塗膜の封孔処理法
JPS6236044A (ja)	1987-02-17	リン酸塩ガラスの耐水性及び破壊強度を増加させる方法
JP3251755B2 (ja)	2002-01-28	アルミナ前駆体溶液、当該溶液を用いたアルミナ薄膜の形成方法及びアルミナ薄膜形成体