JPS5772966A - Prepataion of substituted nitrile - Google Patents
Prepataion of substituted nitrileInfo
- Publication number
- JPS5772966A JPS5772966A JP14821480A JP14821480A JPS5772966A JP S5772966 A JPS5772966 A JP S5772966A JP 14821480 A JP14821480 A JP 14821480A JP 14821480 A JP14821480 A JP 14821480A JP S5772966 A JPS5772966 A JP S5772966A
- Authority
- JP
- Japan
- Prior art keywords
- compound
- aldoxime
- reacting
- dehydrating
- dehydrating agent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Pyridine Compounds (AREA)
Abstract
PURPOSE: To prepare the titled compound useful as a raw material of pharmaceuticals, in high yield, from an aldoxime compound obtained in high yield by reacting hydroxylamine with an aldehyde derived frm a benzylpyridine compound and a formic acid ester, by dehydrating the starting compound with a dehydrating agent.
CONSTITUTION: The substituted nitrile of formula II is prepared by dehydrating an aldoxime of formulaI(R1 and R2 are H, lower alkyl, lower alkoxyl or halogen) with a dehydrating agent (pref. a strongly basic dehydrating agent such as alkali metal hydroxide and alkali metal alcoholate), pref. in an aprotic polar solvent such as dimethylformamide, dimethyl sulfoxide, etc. The aldoxime of formulaIcan be obtained by reacting a benzylpyridine compound with a formic acid ester, and then reacting the reaction product with hydroxylamine.
COPYRIGHT: (C)1982,JPO&Japio
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP14821480A JPS5772966A (en) | 1980-10-24 | 1980-10-24 | Prepataion of substituted nitrile |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP14821480A JPS5772966A (en) | 1980-10-24 | 1980-10-24 | Prepataion of substituted nitrile |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5772966A true JPS5772966A (en) | 1982-05-07 |
| JPS6328065B2 JPS6328065B2 (en) | 1988-06-07 |
Family
ID=15447816
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP14821480A Granted JPS5772966A (en) | 1980-10-24 | 1980-10-24 | Prepataion of substituted nitrile |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS5772966A (en) |
-
1980
- 1980-10-24 JP JP14821480A patent/JPS5772966A/en active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6328065B2 (en) | 1988-06-07 |
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