JPS6021928B2 - ガラス製品の製造方法 - Google Patents

ガラス製品の製造方法

Info

Publication number: JPS6021928B2
Authority: JP; Japan
Prior art keywords: dopant; glass; solvent; temperature; manufacturing
Prior art date: 1975-03-18
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

JP51029758A

Other languages

English (en)

Japanese (ja)

Other versions

JPS51126207A (en

Inventor

ペドロ・マノール・バーク・ド・メーセドー

セオドアー・アーロン・リトビツツ

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Individual

Original Assignee

Individual

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1975-03-18

Filing date

1976-03-18

Publication date

1985-05-30

1975-11-26 Priority claimed from US05/635,728 external-priority patent/US4110093A/en

1976-03-18 Application filed by Individual filed Critical Individual

1976-11-04 Publication of JPS51126207A publication Critical patent/JPS51126207A/ja

1985-05-30 Publication of JPS6021928B2 publication Critical patent/JPS6021928B2/ja

Status Expired legal-status Critical Current

Links

239000011521 glass Substances 0.000 title claims description 160
238000004519 manufacturing process Methods 0.000 title claims description 32
239000002019 doping agent Substances 0.000 claims description 196
238000000034 method Methods 0.000 claims description 138
239000002904 solvent Substances 0.000 claims description 109
239000000203 mixture Substances 0.000 claims description 78
238000010438 heat treatment Methods 0.000 claims description 51
238000002386 leaching Methods 0.000 claims description 50
239000011148 porous material Substances 0.000 claims description 48
239000005373 porous glass Substances 0.000 claims description 41
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 41
238000001035 drying Methods 0.000 claims description 34
150000001875 compounds Chemical class 0.000 claims description 32
238000009826 distribution Methods 0.000 claims description 29
230000008859 change Effects 0.000 claims description 20
238000000151 deposition Methods 0.000 claims description 18
NLSCHDZTHVNDCP-UHFFFAOYSA-N caesium nitrate Chemical compound [Cs+].[O-][N+]([O-])=O NLSCHDZTHVNDCP-UHFFFAOYSA-N 0.000 claims description 15
238000000354 decomposition reaction Methods 0.000 claims description 12
230000008021 deposition Effects 0.000 claims description 12
239000000835 fiber Substances 0.000 claims description 12
238000001704 evaporation Methods 0.000 claims description 11
239000000463 material Substances 0.000 claims description 11
239000002253 acid Substances 0.000 claims description 10
239000000126 substance Substances 0.000 claims description 10
230000009477 glass transition Effects 0.000 claims description 8
150000003839 salts Chemical class 0.000 claims description 8
230000008020 evaporation Effects 0.000 claims description 7
238000001816 cooling Methods 0.000 claims description 6
238000007654 immersion Methods 0.000 claims description 6
-1 rare earth metal ion Chemical class 0.000 claims description 6
229910052792 caesium Inorganic materials 0.000 claims description 5
239000007787 solid Substances 0.000 claims description 5
229910052723 transition metal Inorganic materials 0.000 claims description 5
RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 4
238000009835 boiling Methods 0.000 claims description 4
229910052796 boron Inorganic materials 0.000 claims description 4
238000004891 communication Methods 0.000 claims description 4
229910052700 potassium Inorganic materials 0.000 claims description 4
238000001556 precipitation Methods 0.000 claims description 4
229910052701 rubidium Inorganic materials 0.000 claims description 4
229910052708 sodium Inorganic materials 0.000 claims description 4
239000011734 sodium Substances 0.000 claims description 4
150000003624 transition metals Chemical class 0.000 claims description 4
229910052783 alkali metal Inorganic materials 0.000 claims description 3
150000001340 alkali metals Chemical class 0.000 claims description 3
229910052784 alkaline earth metal Inorganic materials 0.000 claims description 3
150000001342 alkaline earth metals Chemical class 0.000 claims description 3
TVFDJXOCXUVLDH-UHFFFAOYSA-N caesium atom Chemical compound [Cs] TVFDJXOCXUVLDH-UHFFFAOYSA-N 0.000 claims description 3
229910052500 inorganic mineral Inorganic materials 0.000 claims description 3
150000002576 ketones Chemical class 0.000 claims description 3
239000011707 mineral Substances 0.000 claims description 3
150000002823 nitrates Chemical class 0.000 claims description 3
239000003960 organic solvent Substances 0.000 claims description 3
230000001590 oxidative effect Effects 0.000 claims description 3
229910052698 phosphorus Inorganic materials 0.000 claims description 3
RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 2
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 2
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 2
229910052779 Neodymium Inorganic materials 0.000 claims description 2
229910019142 PO4 Inorganic materials 0.000 claims description 2
OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims description 2
ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 2
150000001242 acetic acid derivatives Chemical class 0.000 claims description 2
150000004649 carbonic acid derivatives Chemical class 0.000 claims description 2
229910052802 copper Inorganic materials 0.000 claims description 2
239000010949 copper Substances 0.000 claims description 2
229910052745 lead Inorganic materials 0.000 claims description 2
229910044991 metal oxide Inorganic materials 0.000 claims description 2
150000004706 metal oxides Chemical class 0.000 claims description 2
235000021317 phosphate Nutrition 0.000 claims description 2
150000003013 phosphoric acid derivatives Chemical class 0.000 claims description 2
239000011574 phosphorus Substances 0.000 claims description 2
239000011591 potassium Substances 0.000 claims description 2
230000001376 precipitating effect Effects 0.000 claims description 2
IGLNJRXAVVLDKE-UHFFFAOYSA-N rubidium atom Chemical compound [Rb] IGLNJRXAVVLDKE-UHFFFAOYSA-N 0.000 claims description 2
229910052782 aluminium Inorganic materials 0.000 claims 3
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims 2
HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims 2
229910052761 rare earth metal Inorganic materials 0.000 claims 2
229910052725 zinc Inorganic materials 0.000 claims 2
239000011701 zinc Substances 0.000 claims 2
ZSLUVFAKFWKJRC-IGMARMGPSA-N 232Th Chemical compound [232Th] ZSLUVFAKFWKJRC-IGMARMGPSA-N 0.000 claims 1
NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 claims 1
DJHGAFSJWGLOIV-UHFFFAOYSA-K Arsenate3- Chemical class [O-][As]([O-])([O-])=O DJHGAFSJWGLOIV-UHFFFAOYSA-K 0.000 claims 1
ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 claims 1
WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 claims 1
229910052776 Thorium Inorganic materials 0.000 claims 1
ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims 1
229910052770 Uranium Inorganic materials 0.000 claims 1
125000003158 alcohol group Chemical group 0.000 claims 1
239000003513 alkali Substances 0.000 claims 1
XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims 1
235000019270 ammonium chloride Nutrition 0.000 claims 1
229910052787 antimony Inorganic materials 0.000 claims 1
WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 claims 1
229910052785 arsenic Inorganic materials 0.000 claims 1
RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 claims 1
229910052788 barium Inorganic materials 0.000 claims 1
DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 claims 1
KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims 1
239000004327 boric acid Substances 0.000 claims 1
150000001642 boronic acid derivatives Chemical class 0.000 claims 1
239000005388 borosilicate glass Substances 0.000 claims 1
238000005234 chemical deposition Methods 0.000 claims 1
238000007598 dipping method Methods 0.000 claims 1
229910052732 germanium Inorganic materials 0.000 claims 1
GNPVGFCGXDBREM-UHFFFAOYSA-N germanium atom Chemical compound [Ge] GNPVGFCGXDBREM-UHFFFAOYSA-N 0.000 claims 1
229910052744 lithium Inorganic materials 0.000 claims 1
229910000510 noble metal Inorganic materials 0.000 claims 1
239000005304 optical glass Substances 0.000 claims 1
150000002910 rare earth metals Chemical class 0.000 claims 1
150000004760 silicates Chemical class 0.000 claims 1
229910052712 strontium Inorganic materials 0.000 claims 1
CIOAGBVUUVVLOB-UHFFFAOYSA-N strontium atom Chemical compound [Sr] CIOAGBVUUVVLOB-UHFFFAOYSA-N 0.000 claims 1
229910052716 thallium Inorganic materials 0.000 claims 1
BKVIYDNLLOSFOA-UHFFFAOYSA-N thallium Chemical compound [Tl] BKVIYDNLLOSFOA-UHFFFAOYSA-N 0.000 claims 1
229910052718 tin Inorganic materials 0.000 claims 1
229910001428 transition metal ion Inorganic materials 0.000 claims 1
DNYWZCXLKNTFFI-UHFFFAOYSA-N uranium Chemical compound [U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U] DNYWZCXLKNTFFI-UHFFFAOYSA-N 0.000 claims 1
239000000047 product Substances 0.000 description 86
239000000243 solution Substances 0.000 description 70
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 27
239000011159 matrix material Substances 0.000 description 27
238000011049 filling Methods 0.000 description 26
238000005191 phase separation Methods 0.000 description 26
230000008569 process Effects 0.000 description 26
XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 14
239000007789 gas Substances 0.000 description 12
230000003287 optical effect Effects 0.000 description 11
239000000377 silicon dioxide Substances 0.000 description 11
238000007711 solidification Methods 0.000 description 10
230000008023 solidification Effects 0.000 description 10
229910000272 alkali metal oxide Inorganic materials 0.000 description 8
239000007864 aqueous solution Substances 0.000 description 8
230000006378 damage Effects 0.000 description 8
230000000694 effects Effects 0.000 description 8
239000010410 layer Substances 0.000 description 8
238000005336 cracking Methods 0.000 description 7
229910052742 iron Inorganic materials 0.000 description 7
239000005368 silicate glass Substances 0.000 description 7
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
230000015572 biosynthetic process Effects 0.000 description 6
238000002207 thermal evaporation Methods 0.000 description 6
230000005540 biological transmission Effects 0.000 description 5
230000007423 decrease Effects 0.000 description 5
239000012467 final product Substances 0.000 description 5
150000002500 ions Chemical class 0.000 description 5
238000000465 moulding Methods 0.000 description 5
238000012545 processing Methods 0.000 description 5
238000005406 washing Methods 0.000 description 5
229910002651 NO3 Inorganic materials 0.000 description 4
PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 4
239000013307 optical fiber Substances 0.000 description 4
238000002791 soaking Methods 0.000 description 4
GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 3
235000008331 Pinus X rigitaeda Nutrition 0.000 description 3
235000011613 Pinus brutia Nutrition 0.000 description 3
241000018646 Pinus brutia Species 0.000 description 3
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
238000010521 absorption reaction Methods 0.000 description 3
238000009825 accumulation Methods 0.000 description 3
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 3
238000004140 cleaning Methods 0.000 description 3
230000001276 controlling effect Effects 0.000 description 3
230000008014 freezing Effects 0.000 description 3
238000007710 freezing Methods 0.000 description 3
239000003365 glass fiber Substances 0.000 description 3
238000011068 loading method Methods 0.000 description 3
239000000155 melt Substances 0.000 description 3
229910017604 nitric acid Inorganic materials 0.000 description 3
MWUXSHHQAYIFBG-UHFFFAOYSA-N nitrogen oxide Inorganic materials O=[N] MWUXSHHQAYIFBG-UHFFFAOYSA-N 0.000 description 3
239000001301 oxygen Substances 0.000 description 3
229910052760 oxygen Inorganic materials 0.000 description 3
238000012856 packing Methods 0.000 description 3
238000006467 substitution reaction Methods 0.000 description 3
238000011282 treatment Methods 0.000 description 3
208000016261 weight loss Diseases 0.000 description 3
230000004580 weight loss Effects 0.000 description 3
MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 2
KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 2
206010057190 Respiratory tract infections Diseases 0.000 description 2
229910052910 alkali metal silicate Inorganic materials 0.000 description 2
239000003125 aqueous solvent Substances 0.000 description 2
230000008901 benefit Effects 0.000 description 2
230000009172 bursting Effects 0.000 description 2
239000003795 chemical substances by application Substances 0.000 description 2
210000001520 comb Anatomy 0.000 description 2
239000013078 crystal Substances 0.000 description 2
230000003247 decreasing effect Effects 0.000 description 2
239000008367 deionised water Substances 0.000 description 2
229910021641 deionized water Inorganic materials 0.000 description 2
230000001419 dependent effect Effects 0.000 description 2
238000009792 diffusion process Methods 0.000 description 2
229910001882 dioxygen Inorganic materials 0.000 description 2
238000011549 displacement method Methods 0.000 description 2
238000005530 etching Methods 0.000 description 2
230000005484 gravity Effects 0.000 description 2
239000012535 impurity Substances 0.000 description 2
238000002347 injection Methods 0.000 description 2
239000007924 injection Substances 0.000 description 2
239000007788 liquid Substances 0.000 description 2
208000020442 loss of weight Diseases 0.000 description 2
230000008018 melting Effects 0.000 description 2
238000002844 melting Methods 0.000 description 2
238000012544 monitoring process Methods 0.000 description 2
NHNBFGGVMKEFGY-UHFFFAOYSA-N nitrate group Chemical group [N+](=O)([O-])[O-] NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 2
230000000704 physical effect Effects 0.000 description 2
230000009467 reduction Effects 0.000 description 2
238000003303 reheating Methods 0.000 description 2
239000004576 sand Substances 0.000 description 2
229920006395 saturated elastomer Polymers 0.000 description 2
241000473391 Archosargus rhomboidalis Species 0.000 description 1
235000018185 Betula X alpestris Nutrition 0.000 description 1
235000018212 Betula X uliginosa Nutrition 0.000 description 1
244000241257 Cucumis melo Species 0.000 description 1
235000015510 Cucumis melo subsp melo Nutrition 0.000 description 1
WTDRDQBEARUVNC-LURJTMIESA-N L-DOPA Chemical compound OC(=O)[C@@H](N)CC1=CC=C(O)C(O)=C1 WTDRDQBEARUVNC-LURJTMIESA-N 0.000 description 1
240000002853 Nelumbo nucifera Species 0.000 description 1
235000006508 Nelumbo nucifera Nutrition 0.000 description 1
235000006510 Nelumbo pentapetala Nutrition 0.000 description 1
BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 1
241000124033 Salix Species 0.000 description 1
FJJCIZWZNKZHII-UHFFFAOYSA-N [4,6-bis(cyanoamino)-1,3,5-triazin-2-yl]cyanamide Chemical compound N#CNC1=NC(NC#N)=NC(NC#N)=N1 FJJCIZWZNKZHII-UHFFFAOYSA-N 0.000 description 1
239000002250 absorbent Substances 0.000 description 1
230000002745 absorbent Effects 0.000 description 1
230000002378 acidificating effect Effects 0.000 description 1
102000011759 adducin Human genes 0.000 description 1
108010076723 adducin Proteins 0.000 description 1
230000002411 adverse Effects 0.000 description 1
150000001298 alcohols Chemical class 0.000 description 1
150000001450 anions Chemical class 0.000 description 1
238000013459 approach Methods 0.000 description 1
238000000149 argon plasma sintering Methods 0.000 description 1
IWOUKMZUPDVPGQ-UHFFFAOYSA-N barium nitrate Inorganic materials [Ba+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O IWOUKMZUPDVPGQ-UHFFFAOYSA-N 0.000 description 1
238000004061 bleaching Methods 0.000 description 1
230000015556 catabolic process Effects 0.000 description 1
238000006243 chemical reaction Methods 0.000 description 1
239000013626 chemical specie Substances 0.000 description 1
238000005253 cladding Methods 0.000 description 1
238000009833 condensation Methods 0.000 description 1
230000005494 condensation Effects 0.000 description 1
235000009508 confectionery Nutrition 0.000 description 1
238000011109 contamination Methods 0.000 description 1
238000007796 conventional method Methods 0.000 description 1
230000007547 defect Effects 0.000 description 1
238000011161 development Methods 0.000 description 1
238000006073 displacement reaction Methods 0.000 description 1
238000001493 electron microscopy Methods 0.000 description 1
150000002170 ethers Chemical class 0.000 description 1
238000013213 extrapolation Methods 0.000 description 1
210000004709 eyebrow Anatomy 0.000 description 1
230000002349 favourable effect Effects 0.000 description 1
WDQNIWFZKXZFAY-UHFFFAOYSA-M fentin acetate Chemical compound CC([O-])=O.C1=CC=CC=C1[Sn+](C=1C=CC=CC=1)C1=CC=CC=C1 WDQNIWFZKXZFAY-UHFFFAOYSA-M 0.000 description 1
239000003337 fertilizer Substances 0.000 description 1
238000005429 filling process Methods 0.000 description 1
125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
239000005457 ice water Substances 0.000 description 1
230000000977 initiatory effect Effects 0.000 description 1
RLJMLMKIBZAXJO-UHFFFAOYSA-N lead(II) nitrate Inorganic materials [O-][N+](=O)O[Pb]O[N+]([O-])=O RLJMLMKIBZAXJO-UHFFFAOYSA-N 0.000 description 1
239000006123 lithium glass Substances 0.000 description 1
230000007774 longterm Effects 0.000 description 1
238000012423 maintenance Methods 0.000 description 1
238000005259 measurement Methods 0.000 description 1
238000001000 micrograph Methods 0.000 description 1
238000013508 migration Methods 0.000 description 1
230000005012 migration Effects 0.000 description 1
238000012986 modification Methods 0.000 description 1
230000004048 modification Effects 0.000 description 1
238000004554 molding of glass Methods 0.000 description 1
CFYGEIAZMVFFDE-UHFFFAOYSA-N neodymium(3+);trinitrate Chemical compound [Nd+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O CFYGEIAZMVFFDE-UHFFFAOYSA-N 0.000 description 1
239000012457 nonaqueous media Substances 0.000 description 1
230000003647 oxidation Effects 0.000 description 1
238000007254 oxidation reaction Methods 0.000 description 1
TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 1
230000035699 permeability Effects 0.000 description 1
235000021110 pickles Nutrition 0.000 description 1
229910052573 porcelain Inorganic materials 0.000 description 1
230000002035 prolonged effect Effects 0.000 description 1
238000007670 refining Methods 0.000 description 1
230000001105 regulatory effect Effects 0.000 description 1
238000012552 review Methods 0.000 description 1
239000012266 salt solution Substances 0.000 description 1
239000012047 saturated solution Substances 0.000 description 1
238000007493 shaping process Methods 0.000 description 1
239000000741 silica gel Substances 0.000 description 1
229910002027 silica gel Inorganic materials 0.000 description 1
NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 1
239000011343 solid material Substances 0.000 description 1
241000894007 species Species 0.000 description 1
230000003595 spectral effect Effects 0.000 description 1
239000007858 starting material Substances 0.000 description 1
230000035882 stress Effects 0.000 description 1
239000002344 surface layer Substances 0.000 description 1
230000008961 swelling Effects 0.000 description 1
230000009897 systematic effect Effects 0.000 description 1
238000012360 testing method Methods 0.000 description 1
230000008646 thermal stress Effects 0.000 description 1
238000012546 transfer Methods 0.000 description 1
230000007704 transition Effects 0.000 description 1
238000009941 weaving Methods 0.000 description 1

Classifications

- G—PHYSICS
- G02—OPTICS
- G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
- G02B6/00—Light guides; Structural details of arrangements comprising light guides and other optical elements, e.g. couplings
- G02B6/02—Optical fibres with cladding with or without a coating
- G02B6/028—Optical fibres with cladding with or without a coating with core or cladding having graded refractive index
- G02B6/0281—Graded index region forming part of the central core segment, e.g. alpha profile, triangular, trapezoidal core
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B37/00—Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
- C03B37/01—Manufacture of glass fibres or filaments
- C03B37/012—Manufacture of preforms for drawing fibres or filaments
- C03B37/014—Manufacture of preforms for drawing fibres or filaments made entirely or partially by chemical means, e.g. vapour phase deposition of bulk porous glass either by outside vapour deposition [OVD], or by outside vapour phase oxidation [OVPO] or by vapour axial deposition [VAD]
- C03B37/016—Manufacture of preforms for drawing fibres or filaments made entirely or partially by chemical means, e.g. vapour phase deposition of bulk porous glass either by outside vapour deposition [OVD], or by outside vapour phase oxidation [OVPO] or by vapour axial deposition [VAD] by a liquid phase reaction process, e.g. through a gel phase
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C11/00—Multi-cellular glass ; Porous or hollow glass or glass particles
- C03C11/005—Multi-cellular glass ; Porous or hollow glass or glass particles obtained by leaching after a phase separation step
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C13/00—Fibre or filament compositions
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C13/00—Fibre or filament compositions
- C03C13/005—Fibre or filament compositions obtained by leaching of a soluble phase and consolidation
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C13/00—Fibre or filament compositions
- C03C13/04—Fibre optics, e.g. core and clad fibre compositions
- C03C13/045—Silica-containing oxide glass compositions
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C13/00—Fibre or filament compositions
- C03C13/04—Fibre optics, e.g. core and clad fibre compositions
- C03C13/045—Silica-containing oxide glass compositions
- C03C13/046—Multicomponent glass compositions
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C15/00—Surface treatment of glass, not in the form of fibres or filaments, by etching
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C21/00—Treatment of glass, not in the form of fibres or filaments, by diffusing ions or metals in the surface
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C23/00—Other surface treatment of glass not in the form of fibres or filaments
- C03C23/0095—Solution impregnating; Solution doping; Molecular stuffing, e.g. of porous glass
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/076—Glass compositions containing silica with 40% to 90% silica, by weight
- C03C3/089—Glass compositions containing silica with 40% to 90% silica, by weight containing boron
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/076—Glass compositions containing silica with 40% to 90% silica, by weight
- C03C3/089—Glass compositions containing silica with 40% to 90% silica, by weight containing boron
- C03C3/091—Glass compositions containing silica with 40% to 90% silica, by weight containing boron containing aluminium
- G—PHYSICS
- G02—OPTICS
- G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
- G02B6/00—Light guides; Structural details of arrangements comprising light guides and other optical elements, e.g. couplings
- G02B6/02—Optical fibres with cladding with or without a coating
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B2201/00—Type of glass produced
- C03B2201/06—Doped silica-based glasses
- C03B2201/08—Doped silica-based glasses doped with boron or fluorine or other refractive index decreasing dopant
- C03B2201/10—Doped silica-based glasses doped with boron or fluorine or other refractive index decreasing dopant doped with boron
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B2201/00—Type of glass produced
- C03B2201/06—Doped silica-based glasses
- C03B2201/30—Doped silica-based glasses doped with metals, e.g. Ga, Sn, Sb, Pb or Bi
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B2201/00—Type of glass produced
- C03B2201/06—Doped silica-based glasses
- C03B2201/30—Doped silica-based glasses doped with metals, e.g. Ga, Sn, Sb, Pb or Bi
- C03B2201/32—Doped silica-based glasses doped with metals, e.g. Ga, Sn, Sb, Pb or Bi doped with aluminium
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B2201/00—Type of glass produced
- C03B2201/06—Doped silica-based glasses
- C03B2201/30—Doped silica-based glasses doped with metals, e.g. Ga, Sn, Sb, Pb or Bi
- C03B2201/34—Doped silica-based glasses doped with metals, e.g. Ga, Sn, Sb, Pb or Bi doped with rare earth metals, i.e. with Sc, Y or lanthanides, e.g. for laser-amplifiers
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B2201/00—Type of glass produced
- C03B2201/06—Doped silica-based glasses
- C03B2201/30—Doped silica-based glasses doped with metals, e.g. Ga, Sn, Sb, Pb or Bi
- C03B2201/50—Doped silica-based glasses doped with metals, e.g. Ga, Sn, Sb, Pb or Bi doped with alkali metals
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B2201/00—Type of glass produced
- C03B2201/06—Doped silica-based glasses
- C03B2201/30—Doped silica-based glasses doped with metals, e.g. Ga, Sn, Sb, Pb or Bi
- C03B2201/54—Doped silica-based glasses doped with metals, e.g. Ga, Sn, Sb, Pb or Bi doped with beryllium, magnesium or alkaline earth metals
- G—PHYSICS
- G02—OPTICS
- G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
- G02B6/00—Light guides; Structural details of arrangements comprising light guides and other optical elements, e.g. couplings
- G02B6/02—Optical fibres with cladding with or without a coating
- G02B6/036—Optical fibres with cladding with or without a coating core or cladding comprising multiple layers
- G02B6/03605—Highest refractive index not on central axis
- G02B6/03611—Highest index adjacent to central axis region, e.g. annular core, coaxial ring, centreline depression affecting waveguiding
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/50—Glass production, e.g. reusing waste heat during processing or shaping
- Y02P40/57—Improving the yield, e-g- reduction of reject rates

Landscapes

Chemical & Material Sciences (AREA)
Chemical Kinetics & Catalysis (AREA)
Engineering & Computer Science (AREA)
Geochemistry & Mineralogy (AREA)
Organic Chemistry (AREA)
Life Sciences & Earth Sciences (AREA)
Materials Engineering (AREA)
General Chemical & Material Sciences (AREA)
Physics & Mathematics (AREA)
Optics & Photonics (AREA)
General Physics & Mathematics (AREA)
Dispersion Chemistry (AREA)
General Life Sciences & Earth Sciences (AREA)
Manufacturing & Machinery (AREA)
Surface Treatment Of Glass (AREA)
Glass Melting And Manufacturing (AREA)
Glass Compositions (AREA)
Manufacture, Treatment Of Glass Fibers (AREA)
Optical Fibers, Optical Fiber Cores, And Optical Fiber Bundles (AREA)

JP51029758A 1975-03-18 1976-03-18 ガラス製品の製造方法 Expired JPS6021928B2 (ja)

Applications Claiming Priority (4)

Application Number	Priority Date	Filing Date	Title
US55951275A	1975-03-18	1975-03-18
US559512		1975-03-18
US635728		1975-11-26
US05/635,728 US4110093A (en)	1974-04-22	1975-11-26	Method for producing an impregnated waveguide

Publications (2)

Publication Number	Publication Date
JPS51126207A JPS51126207A (en)	1976-11-04
JPS6021928B2 true JPS6021928B2 (ja)	1985-05-30

Family

ID=27072087

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP51029758A Expired JPS6021928B2 (ja)	1975-03-18	1976-03-18	ガラス製品の製造方法

Country Status (14)

Country	Link
JP (1)	JPS6021928B2 (da)
AU (1)	AU499877B2 (da)
BR (1)	BR7601603A (da)
CA (1)	CA1063352A (da)
CH (1)	CH613049A5 (da)
DE (1)	DE2611496A1 (da)
DK (1)	DK118976A (da)
FR (1)	FR2304579A1 (da)
GB (1)	GB1527436A (da)
IE (1)	IE44144B1 (da)
IT (1)	IT1057427B (da)
LU (1)	LU74597A1 (da)
NL (1)	NL7602765A (da)
SE (1)	SE7603367L (da)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS61271437A (ja) *	1985-05-28	1986-12-01	Sumitomo Metal Ind Ltd	搬送原料のサンプリング方法

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
GB2002342B (en) *	1977-07-27	1982-06-30	Sumitomo Electric Industries	Process for producing a glass member
GB2033372B (en) *	1978-09-28	1983-01-19	Sumitomo Electric Industries	Method of producing an optical waveguide
US4302231A (en) *	1979-01-29	1981-11-24	Pedro Manoel Buarque De Macedo	Method of producing a glass article having a graded refractive index profile of a parabolic nature
JPS5829260B2 (ja) *	1979-08-02	1983-06-21	日本電信電話株式会社	光通信用光学ガラス
ZA81161B (en) *	1980-01-28	1982-08-25	Pilkington Brothers Ltd	Optical glass fibres and methods of forming such fibres
JPS56117209A (en) *	1980-02-22	1981-09-14	Sumitomo Electric Ind Ltd	Manufacture of optical circuit
JPS56164026A (en) *	1980-05-16	1981-12-16	Nippon Telegr & Teleph Corp <Ntt>	Production of basic material for glass for laser
JPS58199747A (ja) *	1982-05-14	1983-11-21	Hoya Corp	屈折率勾配を有するガラス体の製造法
JPS59119739U (ja) *	1983-01-28	1984-08-13	富士電機株式会社	電力用変圧器の差動保護装置
JPS59152238A (ja) *	1983-02-18	1984-08-30	Hoya Corp	屈折率勾配を有するガラス体の製造法
JPS6016730U (ja) *	1983-07-12	1985-02-04	日立電線株式会社	耐放射線性光ファイバ
JPS6088915A (ja) *	1983-10-22	1985-05-18	Hoya Corp	光軸方向に屈折率分布を有するレンズの製造法
JPS6177629A (ja) *	1984-09-21	1986-04-21	Hoya Corp	屈折率分布を有する球レンズの製造法
DE3741393A1 (de) *	1987-12-07	1989-06-15	Siemens Ag	Verfahren zum herstellen von aus hochreinem sio(pfeil abwaerts)2(pfeil abwaerts) bestehenden formkoerpern
JP2545313Y2 (ja) *	1991-11-08	1997-08-25	日新電機株式会社	計器用変圧器

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US2106744A (en) *	1934-03-19	1938-02-01	Corning Glass Works	Treated borosilicate glass
US2522524A (en) *	1946-06-24	1950-09-19	Corning Glass Works	Method of making sealing glasses
CA1020752A (en) *	1973-04-27	1977-11-15	Pedro B. Macedo	Method of producing optical wave guide fibers
US3859073A (en) *	1973-10-19	1975-01-07	Corning Glass Works	Method of producing glass by flame hydrolysis

1976
- 1976-03-10 CA CA000247545A patent/CA1063352A/en not_active Expired
- 1976-03-15 AU AU11988/76A patent/AU499877B2/en not_active Expired
- 1976-03-16 FR FR7607444A patent/FR2304579A1/fr active Granted
- 1976-03-17 BR BR7601603A patent/BR7601603A/pt unknown
- 1976-03-17 NL NL7602765A patent/NL7602765A/xx active Search and Examination
- 1976-03-17 CH CH332676A patent/CH613049A5/xx not_active IP Right Cessation
- 1976-03-17 SE SE7603367A patent/SE7603367L/ unknown
- 1976-03-17 IT IT48616/76A patent/IT1057427B/it active
- 1976-03-18 DE DE19762611496 patent/DE2611496A1/de not_active Ceased
- 1976-03-18 LU LU74597A patent/LU74597A1/xx unknown
- 1976-03-18 JP JP51029758A patent/JPS6021928B2/ja not_active Expired
- 1976-03-18 GB GB10935/76A patent/GB1527436A/en not_active Expired
- 1976-03-18 DK DK118976A patent/DK118976A/da not_active Application Discontinuation
- 1976-03-18 IE IE571/76A patent/IE44144B1/en unknown

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS61271437A (ja) *	1985-05-28	1986-12-01	Sumitomo Metal Ind Ltd	搬送原料のサンプリング方法

Also Published As

Publication number	Publication date
JPS51126207A (en)	1976-11-04
DK118976A (da)	1976-09-19
IT1057427B (it)	1982-03-10
IE44144L (en)	1976-09-18
SE7603367L (sv)	1976-09-19
IE44144B1 (en)	1981-08-26
AU1198876A (en)	1977-09-22
BR7601603A (pt)	1976-09-14
AU499877B2 (en)	1979-05-03
CA1063352A (en)	1979-10-02
DE2611496A1 (de)	1976-10-14
NL7602765A (nl)	1976-09-21
GB1527436A (en)	1978-10-04
FR2304579A1 (fr)	1976-10-15
LU74597A1 (da)	1976-09-01
FR2304579B1 (da)	1982-12-03
CH613049A5 (en)	1979-08-31

Publication	Publication Date	Title
US4110093A (en)	1978-08-29	Method for producing an impregnated waveguide
US4110096A (en)	1978-08-29	Method of precipitation of a dopant in a porous silicate glass
US4225330A (en)	1980-09-30	Process for producing glass member
AU652351B2 (en)	1994-08-25	Quartz glass doped with rare earth element and production thereof
JPS6021928B2 (ja)	1985-05-30	ガラス製品の製造方法
EP0443781A1 (en)	1991-08-28	Method for doping optical fibers
US5151117A (en)	1992-09-29	Solution doping of porous preforms
JPH01239032A (ja)	1989-09-25	光ファイバ製造方法
JPH0121099B2 (da)	1989-04-19
JPS58145634A (ja)	1983-08-30	ド−プされたガラス状シリカの製造方法
CN104876434B (zh)	2018-05-04	一种均匀掺杂石英玻璃棒的制备方法
US4236930A (en)	1980-12-02	Optical waveguide and method and compositions for producing same
US4188198A (en)	1980-02-12	Joint doping of porous glasses to produce materials with high modifier concentrations
CA1160845A (en)	1984-01-24	Method of producing optical waveguide
US4313748A (en)	1982-02-02	Method for producing a strengthened glass structural member
US4319905A (en)	1982-03-16	Method of leaching glass preforms
US4220682A (en)	1980-09-02	Strengthened glass structural member
JPS6021931B2 (ja)	1985-05-30	強化ガラス製品
US20030213268A1 (en)	2003-11-20	Process for solution-doping of optical fiber preforms
JPS6152089B2 (da)	1986-11-12
JPH03265537A (ja)	1991-11-26	希土類元素ドープガラスの製造方法
JP2677871B2 (ja)	1997-11-17	石英系ドープトガラスの製造方法
JPS62858B2 (da)	1987-01-09
KR100341544B1 (ko)	2002-06-21	금속이온-도핑된 광소자 제조방법
JPH07507035A (ja)	1995-08-03	光伝送デバイスおよびその製造方法

JPS6021928B2 - ガラス製品の製造方法 - Google Patents

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Landscapes

Applications Claiming Priority (4)

Publications (2)

Family

ID=27072087

Family Applications (1)

Country Status (14)

Cited By (1)

Families Citing this family (15)

Family Cites Families (4)

Cited By (1)

Also Published As

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