JPS6038440B2 - 作動液組成物 - Google Patents

作動液組成物

Info

Publication number
JPS6038440B2
JPS6038440B2 JP50013312A JP1331275A JPS6038440B2 JP S6038440 B2 JPS6038440 B2 JP S6038440B2 JP 50013312 A JP50013312 A JP 50013312A JP 1331275 A JP1331275 A JP 1331275A JP S6038440 B2 JPS6038440 B2 JP S6038440B2
Authority
JP
Japan
Prior art keywords
acid
phosphate
hydraulic fluid
phenylnaphthylamine
alkyl
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
JP50013312A
Other languages
English (en)
Other versions
JPS50115181A (ja
Inventor
フレデリツク ゲンチツト ウイリアム
アラン マロレウスキ セオドア
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Stauffer Chemical Co
Original Assignee
Stauffer Chemical Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Stauffer Chemical Co filed Critical Stauffer Chemical Co
Publication of JPS50115181A publication Critical patent/JPS50115181A/ja
Publication of JPS6038440B2 publication Critical patent/JPS6038440B2/ja
Expired legal-status Critical Current

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    • C10M169/04—Mixtures of base-materials and additives
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    • C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
    • C10M2223/08—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having phosphorus-to-nitrogen bonds
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    • C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
    • C10M2223/10—Phosphatides, e.g. lecithin, cephalin
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    • C10M2227/02—Esters of silicic acids
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    • C10M2229/02—Unspecified siloxanes; Silicones
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  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
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  • Fluid-Pressure Circuits (AREA)

Description

【発明の詳細な説明】 各種の油圧システムにおける作用伝達のために各種の液
体が用いられている。
ある種の液体は航空機の油圧システムに用いられている
。航空機およびある種の工業的システムで各種のメカニ
ズムを作動させるための油圧作動システムにおいては、
用いられる作動液に関する厳しい要請が見られる。
作動液は、厳しい機能的および使用上の要請に適合しな
ければならないのみならず、防炎性の要請に適合するた
めに充分に不燃性でなければならない。
場合によっては、この種の作動液の粘度特性は、広範囲
の温度において用いられるものでなければならない。
すなわち、高温度で適切な粘度を有し、低温度で低粘度
を有し、温度による粘度変化率が低くなければならない
。また、その流動点は低く、加熱した場合の揮発性が低
くなければならない。すなわち、使用時の高温度におい
て、重要な成分の選択的揮発又は蒸発が生じてはならな
い。さらに、使用する液体に関する要請が著しく厳しい
航空機の油圧システム中に用いうるように充分に潤滑性
及び機械的安定性が高くなければならない。酸化、熱分
解等の化学的反応に対して安定でなければならす、圧力
、温度の突然の著しい変化、高灘断力、アルミニウム、
フロンズ、鋼、カドミウム、マグネシウム等のごとき各
種金属との接触に基づく所望の特性の劣化に対して、使
用状態を安定に維持するものでなければならない。
さらに、工業的又は航空機油圧システムのガスケツト及
び充填剤を劣化させたり膨潤させたりしてはならない。
漏洩の場合に、接触する物質に悪影響を与えたり、事故
によって接触する油圧システムの各部分に悪影響を与え
るものであってはならない。本発明の機能的作動液組成
物において、ェポキシシクロヘキシルカルボキシレート
及びフェニルナフチルアミンを配合する機能的液体を基
剤と称す。
基剤は、含燐系酸のェステル類等である。
客種の作動液組成物が提案されている。
適当な流動点低下剤、粘度指数向上剤、防蝕剤、防さび
剤等を配合したホスフェィトェステル類は最も好ましい
ものの一つであって、航空機作動液組成物として、広く
使用されている。
これらの作動液においては、使用中に好ましからざる酸
生成が起こる。
この酸が過剰に生じると基剤は破壊され、粘度等の所望
の物性が失なわれる。この酸は、組成物と接触する油圧
システム中の金属部分を侵蝕する。この酸侵蝕及び腐蝕
抑制剤が機能的作動液組成物中に配合される。ある種の
ェポキシドとフェニルナフチルアミンとを機能的液体に
配合すると、その酸安定性を与えることを見出した。
この種のェポキシドとアミンとの添加又は配合は、以下
に述べるように、たとえば、スラッジの生成、金属腐蝕
等のごとき特性劣化を生じさせることなく、機能的液体
の酸安定性、粘度安定性を与えるところの予期しえざる
相乗効果を示す。
本発明に用いるェポキシド類は、次の式（１）、 で表わされるェポキシシクロヘキシルカルボキシレート
であり、好ましくは３・４ーェポキシシク。
へキシルカルボキシレートであり、そして特に好ましく
は、次の式：で表わされる３・４−ェポキシシクロヘキ
シルメチルー３・４ーシクロヘキサンカルボキシレート
である。
本発明に用いるアミンは次の式（ｎ）、 （式中、Ｒ、Ｒ″及びＲ…は、同一であり又は異ってお
り、そして水素又は炭素原子数１〜１針固のアルキルで
ある、）で表わされるアルキル化されている場合がある
フェニルナフチルアミンであり、好ましくはフェニル−
Ｑーナフチルアミン、オクチル化フエニル−Ｑ−ナフチ
ルアミン（フエニルーＱーナフチルアミンを１：１〜３
：１のモル比でジィソブチレンによりアルキル化したも
の）、ジオクチルフエニル−Ｑーナフチルアミン、及び
トリオクチルフヱニルーＱーナフチルァミン等である。
作動液組成物中のェポキシシクロヘキシルカルボキシレ
ートとフェニルナフチルアミンとの濃度は、使用する特
定のシステムに適したものであり、かつ、ェポキシシク
ロヘキシルカルボキシレートとフェニルナフチルアミン
とは、組成物の醗生成を防止するに充分な量である。
組成物の特性は、異種物質の配合によって変化する。し
たがって、所望のェポキシシクロヘキシルカルボキシレ
ートとフェニルナフチルアミンとの配合童は、該組成物
の約０．１〜１０．の重量％が適当である。エポキシシ
クロヘキシルカルボキシレートとフェニルナフチルアミ
ンとの比は、約１：１０〜１０：１重量比であり、約１
：１が特に好ましい。本発明の組成物は従釆公知の方法
で製造しうる。たとえば、エポキシシクロヘキシルカル
ボキシレートとフェニルナフチルアミンをいずれかの順
序で基剤に混合し、又は共に混合し、均一な組成物が得
られるまで蝿拝することによって製造しうる。本発明の
実施において、基剤として用いるに通した機能的液体と
して、下記の一般式で示される含燐系酸のェステル類が
挙げられる。
〔ここに、Ｙは酸素又は硫黄であり；Ｙ，は酸素又は硫
黄であり；Ｙ２は酸素又は硫黄であり；Ｒ、Ｒ，、Ｒ２
は、それぞれ同一又は異なる炭素数１〜３０のアルキル
、ァリール、置換アリール、贋換ァルキル基であり；ａ
、ｂ、ｃはそれぞれ０又は１で、ａ十ｂ＋ｃは１〜３で
ある。
〕置換アルキル基の例としては、一般式 〔ここに、Ｈａｌはハロゲン、ｍは幼＋１と同じか小さ
い数；ｎは０〜１８；馬、Ｒ７は水素、ハロゲン又はア
ルキル基である〕で示されるハロアルキル基であり、第
１級、第２級、第３級のいずれであっても良い。
ァリール基、置換アリール基の代表例は、フェニル、ク
レジル、キシレリル、ハロゲン化フヱニル、クレジル又
はアリール、置換アリール基上の水素の一部又は全部が
ハロゲンで魔摸したもの、ｏ−、ｍ−又はｐ−トリフル
オロメチルフエニル；ｏ−、ｍ−又はｐ−２・２・２−
トリフルオロヱチルフェニル；ｏ−、ｍ一又はｐ−３・
３・３ートリフルオロプロピルフェニル及びｏ−、ｍ一
又はｐ−４・４・４ートリフルオロプチルフェニル基で
ある。
本発明の作動液組成物は、前記の含鱗系酸のェステル類
に加えて、次のような追加の基剤を含有することもでき
る。
追加の基材として適したジカルボン酸ェステル類は、一
般式〔ここに、Ｒ凶、Ｒ礎はそれぞれ、アルキル、置換
アルキル、アリール又は置換アリールであり；Ｒ２，は
、ァルキレン又は置換ァルキレンの２価の基である〕で
示されたものであり、これは、アジピン酸、アゼラィン
酸、スベリン酸、セバシン酸、ヒドロキシこはく酸、フ
マール酸、マレィン酸等のジカルボン酸類とブチルアル
コール、ヘキシルアルコール、２−エチルヘキシルアル
コール、ドデシルアルコール、２・２−ジメチルヘプタ
ノール、１−メチルシクロヘキシルメタノール等のアル
コール類とのェステル化によって製造しうる。
アルキル、アリール、置換アルキル、置換アリール基の
代表例は上記のものである。
追加の基村として用いるに適したポリエステル類は、一
般式〔ここに、Ｒ２３は水素又はアルキル基であり；Ｒ
２４、Ｒ２５はそれぞれ、アルキル、置換アルキル、ァ
リール又は置換アリール基であり；ａは１又は０：Ｚは
１又は２であり；Ｚが１の場合Ｒ２６は水素、アルキル
、アルコキシ、置換アシロキシ基であり；Ｚが２つの場
合はＲ２６が酸素である。
〕で示したものであり、ベンタヱリスリトール、ジベン
タエリストール、トリメチロールプロ／ぐン、トリメチ
ロールヱタン、ネオベンチルグリコールのごときポリア
ルコール類とプロピオン酸、らく酸、ィソら〈酸、ｎ−
バレィン酸、カプロン酸、ｎーヘフ。チル酸、カプリソ
酸、２−エチルヘクサノン酸、２・２−ジメチルヘプタ
ノン酸、ベラルゴン酸等の酸塩とのェステル化によって
製造したものである。ァルキル、置換アルキル、アリー
ル、贋換ァリール基の代表例は、上記のものである。
追加の基剤として用いるに適した他のェステル類はモノ
ェステル類である。
石油類から得た鉱物油等の炭化水素類、合成炭化水素減
額等も追加の基剤として用いうる。
鉱物油かち得られる機能的液体の物性は、システムの要
請に基づいて選択される。それ故、広範囲の粘性、揮発
性を有する鉱物油類たとえば、ナフテン系、パラフィン
系及び混合系鉱物油を基剤として用いうる。追加の基材
としての合成炭化水素油額は、ポリブタジェン等のオレ
フィンのオリゴマー化によって得られたもの、炭素数８
〜２０の高級Ｑ−オレフィンから得られたものであって
、これらは触媒としてトリアルキルアルミニウム等を用
いたオリゴマー化又は酸触媒ダイマ−化によって得られ
たものである。
上記の追加基剤の２以上の混合物を本発明の基剤に加え
ても良い。
本発明の組成物を機能的作動液組成物として用いる場合
、染料、流動点低下剤、消泡剤、粘度指数向上剤（たと
えば、ポＩＪアルキルァクリレート類、ポリアルキルメ
タクリレート類、ポリ環状重合体類、ポリウレタン類、
ポリアルキレンオキサィド類、ポリエステル類）；潤滑
剤、水等を配合しても良い。
基剤には、機能的液体の他に他の液体を配合しても良い
。
この液体は、石炭製品から得られた液体類、合成品及び
合成油類であって、たとえば、アルキレンポリマー類（
たとえば、プロピレン、ブタジェン及びその混合物のポ
リマー）、アルキレンオキサイドタイプポリマー類（た
とえば、プロピレンオキサイドポリマー）及び、水又は
エチルアルコール等のアルコールの存在下にアルキレン
オキサィドを重合することによって得たアルキレンオキ
サイドポリマー類、アルキルベンゼン類（たとえば、ド
デシルベンゼン、テトラデシルベンゼン等のモノアルキ
ルベンゼン）、ジアルキルベンゼン類（たとえば、ｎー
ノニル２−エチルヘキシルベンゼン）及びポリフェノー
ル類（たとえば、ビフェニル類、ターフェニル類）等で
ある。本発明においては、ェポキシシクロヘキシルカル
ボキシレート及びフェニルナフチルアミンを燐酸系機能
的液体基剤に配合する。この基剤は、トリアルキルホス
フェイト類５０〜９５重量％、好ましくは６０〜９０重
量％を配合したものが特に好ましい。最良の効果を与え
るトリアルキルホスフェィト類の各アルキル基は炭素数
１〜２ｕ好ましくは３〜１２、特に好ましくは４〜９の
ものである。
該アルキル基は直鎖状のものが好ましい。各トリアルキ
ルホスフェィトは３つの位置のアルキル基が同一又は異
なるものである。各種のトリアルキルホスフェイト類の
混合物を用いることもできる。基剤として用いるに通し
たトリアルキルホスフェィト類は、トリプロピルホスフ
ェィト類、トリブチルホスフエイト、トリへキシルホス
フエイト類、トリオクチルホスフェイト、ジプロピルオ
クチルホスフエイト、ジブチルオクチルホスフエイト、
ジプロピルヘキシルホスフエイト、ジヘキシルオクチル
ホスフエイト、ジヘキシルプロピルホスフェイト及びプ
ロピルブチルオクチルホスフヱィト等である。トリアル
キルホスフェイト類は、トリアリールホスフェィト類と
配合しても良い。
好ましいトリアリールホスフェィト類は、クレジルジフ
ェニルホスフエイト、トリクレジルホスフエイト、トリ
キシレニルホスフエイト、ターシヤリブチルフエニルフ
エニルホスフエイト、エチルフエニルジクレジルホスフ
エイト、イソプロピルフエニルジフエニルホスフエイト
、フエニルービス（４一Ｑ−メチルベンジルフェニル）
ホスフェィト等である。好ましい態様において、第１級
トリキシレニルホスフエイトを配合した基剤が用いられ
る。
トリアリールホスフェイト類は、トリアルキルホスフェ
ィト類の増粘剤としての作用を有する。しかして、トリ
アリールホスフェイトの配合革は約０〜３５重量％であ
る。トリアリールホスフェイトの好ましい配合量は約５
〜３の重量％である。公知の重合体増粘剤又は粘度指数
向上剤をトリアルキルホスフエイトとトリアリ−ルホス
フエイトとの混合物に配合して、所望の粘度を達成しう
る。使用される代表的な増粘剤は、ポリァクリレ−ト類
、ボリメタクリレート類、ポリエチレンオキサィド類、
ポリプロピレンオキサイド類、ポリエステル額等である
。
好ましくは、アゼライン酸とジオールとのポリエステル
を０．３〜２の重量％粘度指数向上剤として用いる。
ペンゾトリアゾール、キニザリン等の防蝕剤を上記の混
合物に対して０．００１〜０．５重量％配合して充分に
混和する。
上記組成物に対し、百万分の５〜２の部の濃度の染料を
添加し、公知の方法で混和しうる。有効量のシリコン消
泡剤を上記組成物に配合しうる。
最も好ましい配合量は百万分の５〜５の部である。本発
明の機能的作動液組成物は、約１重量％以下の水分を含
有しうる。
しかしながら、好ましくは０．館重量％以下、特に好ま
しくは０．箱重量％以下の水分とする。上記の好ましい
機能的液体組成物に適当な割合のエポキシシクロヘキシ
ルカルボキシレートとフヱニルナフチルアミンとを配合
した場合に、その特性は公知の作動液組成物に比して著
しくすぐれたものとなる。本発明を実施例によって、さ
らに説明する。
実施例中、部、％は特に規定しない限り、重量部、重量
％である。実施例約６８％のトリブチルホスフェイトと
１９％の混合クレジル及びキシレニルホスフェイト類で
シーボルトユニバーサルセコンド（ＳＵＳ）が約１５０
のものと、１２％のポリブチルメタクリレート粘度指数
向上剤と０．５％の水と、０．０２％のペンゾトリアゾ
ール金属不活性化剤とアルキルこはく酸防蝕剤とからな
る基剤組成物に、ＦＩ％の３・４−ヱポキシシクロヘキ
シルメチル／‘３・４−エポキシシクロヘキサンカルボ
キシレートと１％の下記の酸化防止剤とを配合し、全酸
価を試験した。
これらの試験結果は、ェポキシシクロヘキシルカルボキ
シレートにフヱニルーＱーナフチルアミン類を配合した
場合著しく安定性が良いことを示している。
約７９％のトリブチルホスフェイトと１０％のクレジル
ホスフェイトとキシレニルホスフヱィト混合物と９％の
ァゼラン酸の低分子ポリエチレングリコールポリエステ
ルと１％のフエニルーＱーナフチルアミンと０．０２％
のペンゾトリアゾールと０．２５％の水とを配合してな
る組成物に、１．０％の各種のェポキサィドアシッドア
クセプターを配合して、同様の試験をおこなった。
この結果は下記の通りである。これらの両実験結果は、
フェニル。

Claims (1)

  1. 【特許請求の範囲】 １ 含燐系酸のエステル類を主体とする基剤、並びに次
    の式（I）、▲数式、化学式、表等があります▼ で表わされるエポキシシクロヘキシルカルボキシレート
    、及び次の式（II）、▲数式、化学式、表等があります
    ▼ （式中Ｒ′、Ｒ″、及びＲ′″は、同一であり又は異り
    、そして水素又は炭素原子数１〜１６個のアルキル基で
    ある、）で表わされるフエニルナフチルアミンを含んで
    成り、前記エポキシシクロヘキシルカルボキシレートと
    前記フエニルナフチルアミンとの合計量が組成物全体に
    対して０．１〜１０重量％であり、そして前記エポキシ
    シクロヘキシルカルボキシレートと前記フエニルナフチ
    ルアミンとの重量比が１：１０〜１０：１であることを
    特徴とする作動液組成分。
JP50013312A 1974-02-11 1975-01-31 作動液組成物 Expired JPS6038440B2 (ja)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US441697 1974-02-11
US05/441,697 US3941708A (en) 1974-02-11 1974-02-11 Hydraulic fluid antioxidant system

Publications (2)

Publication Number Publication Date
JPS50115181A JPS50115181A (ja) 1975-09-09
JPS6038440B2 true JPS6038440B2 (ja) 1985-08-31

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US (1) US3941708A (ja)
JP (1) JPS6038440B2 (ja)
BE (1) BE825339A (ja)
CA (1) CA1048011A (ja)
CH (1) CH616957A5 (ja)
DE (1) DE2505116C2 (ja)
DK (1) DK144380C (ja)
FR (1) FR2260616B1 (ja)
GB (1) GB1506197A (ja)
IL (1) IL46500A (ja)
IN (1) IN142709B (ja)
IT (1) IT1029650B (ja)
NL (1) NL7501425A (ja)
NO (1) NO140677C (ja)
SE (1) SE410006B (ja)
SU (1) SU652900A3 (ja)
ZA (1) ZA75841B (ja)

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Also Published As

Publication number Publication date
US3941708A (en) 1976-03-02
DK144380B (da) 1982-03-01
IT1029650B (it) 1979-03-20
IL46500A0 (en) 1975-04-25
JPS50115181A (ja) 1975-09-09
NO140677C (no) 1979-10-17
SE7501452L (ja) 1975-08-12
GB1506197A (en) 1978-04-05
DK144380C (da) 1982-08-02
NO140677B (no) 1979-07-09
AU7759875A (en) 1976-07-29
BE825339A (nl) 1975-08-07
NO750422L (ja) 1975-08-12
ZA75841B (en) 1976-01-28
SU652900A3 (ru) 1979-03-15
DE2505116A1 (de) 1975-08-14
DE2505116C2 (de) 1985-06-20
FR2260616B1 (ja) 1982-04-23
SE410006B (sv) 1979-09-17
DK39175A (ja) 1975-10-06
CA1048011A (en) 1979-02-06
IL46500A (en) 1977-06-30
IN142709B (ja) 1977-08-20
NL7501425A (nl) 1975-08-13
FR2260616A1 (ja) 1975-09-05
CH616957A5 (ja) 1980-04-30

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