LU82686A1 - Procede pour la preparation de diesterdiamides - Google Patents

Procede pour la preparation de diesterdiamides Download PDF

Info

Publication number: LU82686A1
Authority: LU; Luxembourg
Prior art keywords: salt; ester; solvent; diesterdiamide; diester
Prior art date: 1979-09-10

Application number

LU82686A

Other languages

English (en)

French (fr)

Inventor

A Mariano

F Cognigni

Original Assignee

Anic Spa

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1979-09-10

Filing date

1980-08-04

Publication date

1981-03-24

1980-08-04 Application filed by Anic Spa filed Critical Anic Spa

1981-03-24 Publication of LU82686A1 publication Critical patent/LU82686A1/fr

Links

238000000034 method Methods 0.000 title claims description 9
238000002360 preparation method Methods 0.000 title claims description 7
239000002904 solvent Substances 0.000 claims description 28
238000005406 washing Methods 0.000 claims description 18
239000003054 catalyst Substances 0.000 claims description 14
238000001914 filtration Methods 0.000 claims description 11
230000015572 biosynthetic process Effects 0.000 claims description 10
238000003786 synthesis reaction Methods 0.000 claims description 10
150000005690 diesters Chemical class 0.000 claims description 9
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 7
239000003153 chemical reaction reagent Substances 0.000 claims description 7
150000004985 diamines Chemical class 0.000 claims description 5
239000000376 reactant Substances 0.000 claims description 5
239000002244 precipitate Substances 0.000 claims description 4
239000003643 water by type Substances 0.000 claims description 4
239000012535 impurity Substances 0.000 claims description 2
238000011084 recovery Methods 0.000 claims description 2
150000003839 salts Chemical class 0.000 claims description 2
125000003158 alcohol group Chemical group 0.000 claims 1
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 39
YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 36
239000000203 mixture Substances 0.000 description 18
WOZVHXUHUFLZGK-UHFFFAOYSA-N dimethyl terephthalate Chemical compound COC(=O)C1=CC=C(C(=O)OC)C=C1 WOZVHXUHUFLZGK-UHFFFAOYSA-N 0.000 description 14
-1 diester diamides Chemical class 0.000 description 11
238000006243 chemical reaction Methods 0.000 description 7
229910052751 metal Inorganic materials 0.000 description 6
239000002184 metal Substances 0.000 description 6
VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 6
229910052757 nitrogen Inorganic materials 0.000 description 6
239000000047 product Substances 0.000 description 6
RCRBCNZJGBTYDI-UHFFFAOYSA-L dilithium;terephthalate Chemical compound [Li+].[Li+].[O-]C(=O)C1=CC=C(C([O-])=O)C=C1 RCRBCNZJGBTYDI-UHFFFAOYSA-L 0.000 description 5
229920000642 polymer Polymers 0.000 description 5
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 4
150000001298 alcohols Chemical class 0.000 description 4
229930195733 hydrocarbon Natural products 0.000 description 4
150000002430 hydrocarbons Chemical class 0.000 description 4
229910052744 lithium Inorganic materials 0.000 description 4
UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
239000006227 byproduct Substances 0.000 description 3
239000000835 fiber Substances 0.000 description 3
239000000178 monomer Substances 0.000 description 3
238000000926 separation method Methods 0.000 description 3
OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical compound NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 description 2
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 2
LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 2
IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 description 2
WQDUMFSSJAZKTM-UHFFFAOYSA-N Sodium methoxide Chemical compound [Na+].[O-]C WQDUMFSSJAZKTM-UHFFFAOYSA-N 0.000 description 2
229910052784 alkaline earth metal Inorganic materials 0.000 description 2
125000004432 carbon atom Chemical group C* 0.000 description 2
238000004821 distillation Methods 0.000 description 2
150000002148 esters Chemical class 0.000 description 2
NAQMVNRVTILPCV-UHFFFAOYSA-N hexane-1,6-diamine Chemical compound NCCCCCCN NAQMVNRVTILPCV-UHFFFAOYSA-N 0.000 description 2
230000007062 hydrolysis Effects 0.000 description 2
238000006460 hydrolysis reaction Methods 0.000 description 2
XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 2
ZXEKIIBDNHEJCQ-UHFFFAOYSA-N isobutanol Chemical compound CC(C)CO ZXEKIIBDNHEJCQ-UHFFFAOYSA-N 0.000 description 2
238000004519 manufacturing process Methods 0.000 description 2
125000000956 methoxy group Chemical group [H]C([H])([H])O* 0.000 description 2
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
LQLQDKBJAIILIQ-UHFFFAOYSA-N Dibutyl terephthalate Chemical compound CCCCOC(=O)C1=CC=C(C(=O)OCCCC)C=C1 LQLQDKBJAIILIQ-UHFFFAOYSA-N 0.000 description 1
DKMROQRQHGEIOW-UHFFFAOYSA-N Diethyl succinate Chemical compound CCOC(=O)CCC(=O)OCC DKMROQRQHGEIOW-UHFFFAOYSA-N 0.000 description 1
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
125000001931 aliphatic group Chemical group 0.000 description 1
239000003513 alkali Substances 0.000 description 1
150000001342 alkaline earth metals Chemical class 0.000 description 1
125000000217 alkyl group Chemical group 0.000 description 1
125000003118 aryl group Chemical group 0.000 description 1
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
230000003197 catalytic effect Effects 0.000 description 1
238000005119 centrifugation Methods 0.000 description 1
DIOQZVSQGTUSAI-UHFFFAOYSA-N decane Chemical compound CCCCCCCCCC DIOQZVSQGTUSAI-UHFFFAOYSA-N 0.000 description 1
230000006866 deterioration Effects 0.000 description 1
ONIHPYYWNBVMID-UHFFFAOYSA-N diethyl benzene-1,4-dicarboxylate Chemical compound CCOC(=O)C1=CC=C(C(=O)OCC)C=C1 ONIHPYYWNBVMID-UHFFFAOYSA-N 0.000 description 1
VNGOYPQMJFJDLV-UHFFFAOYSA-N dimethyl benzene-1,3-dicarboxylate Chemical compound COC(=O)C1=CC=CC(C(=O)OC)=C1 VNGOYPQMJFJDLV-UHFFFAOYSA-N 0.000 description 1
GTZOYNFRVVHLDZ-UHFFFAOYSA-N dodecane-1,1-diol Chemical compound CCCCCCCCCCCC(O)O GTZOYNFRVVHLDZ-UHFFFAOYSA-N 0.000 description 1
238000001035 drying Methods 0.000 description 1
230000008030 elimination Effects 0.000 description 1
238000003379 elimination reaction Methods 0.000 description 1
244000144992 flock Species 0.000 description 1
150000002334 glycols Chemical class 0.000 description 1
125000004836 hexamethylene group Chemical group [H]C([H])([*:2])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[*:1] 0.000 description 1
ACCCMOQWYVYDOT-UHFFFAOYSA-N hexane-1,1-diol Chemical compound CCCCCC(O)O ACCCMOQWYVYDOT-UHFFFAOYSA-N 0.000 description 1
150000002642 lithium compounds Chemical class 0.000 description 1
JILPJDVXYVTZDQ-UHFFFAOYSA-N lithium methoxide Chemical compound [Li+].[O-]C JILPJDVXYVTZDQ-UHFFFAOYSA-N 0.000 description 1
239000000463 material Substances 0.000 description 1
125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
229910052760 oxygen Inorganic materials 0.000 description 1
239000001301 oxygen Substances 0.000 description 1
BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 1
238000000746 purification Methods 0.000 description 1
238000004064 recycling Methods 0.000 description 1
229910052708 sodium Inorganic materials 0.000 description 1
239000011734 sodium Substances 0.000 description 1
239000007787 solid Substances 0.000 description 1
239000011877 solvent mixture Substances 0.000 description 1
238000009987 spinning Methods 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C231/00—Preparation of carboxylic acid amides
- C07C231/02—Preparation of carboxylic acid amides from carboxylic acids or from esters, anhydrides, or halides thereof by reaction with ammonia or amines

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Chemical Kinetics & Catalysis (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Polyamides (AREA)
Steroid Compounds (AREA)

LU82686A 1979-09-10 1980-08-04 Procede pour la preparation de diesterdiamides LU82686A1 (fr)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
IT2557079		1979-09-10
IT25570/79A IT1123574B (it)	1979-09-10	1979-09-10	Processo per la produzione di diesterediammidi

Publications (1)

Publication Number	Publication Date
LU82686A1 true LU82686A1 (fr)	1981-03-24

Family

ID=11217125

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
LU82686A LU82686A1 (fr)	1979-09-10	1980-08-04	Procede pour la preparation de diesterdiamides

Country Status (21)

Country	Link
US (1)	US4614815A (cs)
JP (1)	JPS5640649A (cs)
AU (1)	AU536158B2 (cs)
BE (1)	BE884650A (cs)
CA (1)	CA1172650A (cs)
CH (1)	CH650769A5 (cs)
CS (1)	CS221975B2 (cs)
DD (1)	DD152336A5 (cs)
DE (1)	DE3029970C2 (cs)
DK (1)	DK158660C (cs)
FR (1)	FR2468583A1 (cs)
GB (1)	GB2058053B (cs)
HU (1)	HU191172B (cs)
IT (1)	IT1123574B (cs)
LU (1)	LU82686A1 (cs)
NL (1)	NL8004512A (cs)
NO (1)	NO151197C (cs)
SE (1)	SE439304B (cs)
SU (1)	SU1389676A3 (cs)
YU (1)	YU41446B (cs)
ZA (1)	ZA804455B (cs)

Families Citing this family (17)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US4767839A (en) *	1987-07-06	1988-08-30	Allied-Signal Inc.	Alternating aliphatic-aromatic poly(esteramide)
US5608108A (en) *	1988-11-14	1997-03-04	Sloan-Kettering Institute For Cancer Research	Potent inducers of terminal differentiation and method of use thereof
WO1990009092A2 (en) *	1988-11-14	1990-08-23	The Trustees Of Columbia University In The City Of New York	Novel potent inducers of terminal differentiation and method of use thereof
DE4024466C2 (de) *	1990-07-30	1995-04-20	Dainippon Ink & Chemicals	Thermisch härtbare Mischungen aus polyfunktionellen Formamiden und aromatischen Mono-, Di- oder Polyglycidylethern und deren Verwendung
US5700811A (en) *	1991-10-04	1997-12-23	Sloan-Kettering Institute For Cancer Research	Potent inducers of terminal differentiation and method of use thereof
USRE38506E1 (en)	1991-10-04	2004-04-20	Sloan-Kettering Institute For Cancer Research	Potent inducers of terminal differentiation and methods of use thereof
US5369108A (en) *	1991-10-04	1994-11-29	Sloan-Kettering Institute For Cancer Research	Potent inducers of terminal differentiation and methods of use thereof
WO1995035330A1 (en) *	1994-06-17	1995-12-28	Exxon Chemical Patents Inc.	Amidation of ester functionalized hydrocarbon polymers
US5852155A (en) *	1995-03-01	1998-12-22	General Electric Company	Compositions of polyesteramides
US5744068A (en) *	1996-01-24	1998-04-28	General Electric Company	Blends of polyphenylene ethers and polyesteramides
US5731389A (en) *	1996-04-24	1998-03-24	General Electric Company	Blends of polyesters and polyesteramides, optionally with polycarbonates
WO1997041166A1 (en) *	1996-04-30	1997-11-06	Toray Industries, Inc.	Polyester amide copolymer and process for the production thereof, polyester amide monomer and process for the production thereof, and polyester amide resin composition
BR0014254A (pt)	1999-09-08	2002-08-27	Sloan Kettering Inst Cancer	Nova classe de agentes de citodiferenciação e inibidores de desacetilase de histona, e métodos de uso dos mesmos
AU2004228011A1 (en) *	2003-04-01	2004-10-21	Memorial Sloan-Kettering Cancer Center	Hydroxamic acid compounds and methods of use thereof
US20150119604A1 (en) *	2012-04-11	2015-04-30	Idemitsu Kosan Co., Ltd.	Method for producing beta-alkoxypropionamide
WO2015022119A1 (en) *	2013-08-16	2015-02-19	Dsm Ip Assets B.V.	Process for producing a thermoplastic polymer containing segments of a diamide
KR101568357B1 (ko) *	2013-11-25	2015-11-12	롯데케미칼 주식회사	신규 화합물 및 이의 제조방법

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US2848439A (en) *	1955-04-26	1958-08-19	Eastman Kodak Co	Linear polyesters of bis (nu-p-carboxyphenyl) alkylene diamides and manufacture thereof
US2861055A (en) *	1955-04-26	1958-11-18	Eastman Kodak Co	Copolyesters of a glycol and an alkylene diamine dicarboxylate containing isophthalate modifier and their preparation
US2851443A (en) *	1955-04-26	1958-09-09	Eastman Kodak Co	Quenchable copolyesters of a glycol, terephthalic acid and an alkylene diamine dicarboxylate and their preparation
US2839508A (en) *	1955-04-26	1958-06-17	Eastman Kodak Co	Copolyesters of a glycol, an alkylene diamine dicarboxylate and a sulfone ester
US2925405A (en) *	1955-04-26	1960-02-16	Eastman Kodak Co	Linear polyesters containing an alkylene diamine group and manufacture thereof
US2856385A (en) *	1956-05-10	1958-10-14	Eastman Kodak Co	Polyester-amides of n,n'-bis-(p-carboxybenzoyl) alkylenediamines, glycols and diamines
SU1069623A3 (ru) *	1970-10-13	1984-01-23	Снам Прогетти С.П.А. (Фирма)	Способ получени диамидодиэфиров

1979
- 1979-09-10 IT IT25570/79A patent/IT1123574B/it active
1980
- 1980-07-17 CH CH5485/80A patent/CH650769A5/it not_active IP Right Cessation
- 1980-07-21 DK DK313380A patent/DK158660C/da not_active IP Right Cessation
- 1980-07-22 AU AU60686/80A patent/AU536158B2/en not_active Ceased
- 1980-07-22 NO NO802196A patent/NO151197C/no unknown
- 1980-07-23 SE SE8005346A patent/SE439304B/sv not_active IP Right Cessation
- 1980-07-23 ZA ZA00804455A patent/ZA804455B/xx unknown
- 1980-07-24 GB GB8024330A patent/GB2058053B/en not_active Expired
- 1980-07-24 CA CA000356970A patent/CA1172650A/en not_active Expired
- 1980-07-30 YU YU1925/80A patent/YU41446B/xx unknown
- 1980-08-04 LU LU82686A patent/LU82686A1/fr unknown
- 1980-08-05 FR FR8017294A patent/FR2468583A1/fr active Granted
- 1980-08-06 HU HU801956A patent/HU191172B/hu not_active IP Right Cessation
- 1980-08-06 CS CS805438A patent/CS221975B2/cs unknown
- 1980-08-06 BE BE0/201664A patent/BE884650A/fr not_active IP Right Cessation
- 1980-08-06 JP JP10724780A patent/JPS5640649A/ja active Granted
- 1980-08-06 DD DD80223155A patent/DD152336A5/de unknown
- 1980-08-06 SU SU802957756A patent/SU1389676A3/ru active
- 1980-08-07 NL NL8004512A patent/NL8004512A/nl not_active Application Discontinuation
- 1980-08-07 DE DE3029970A patent/DE3029970C2/de not_active Expired
1982
- 1982-06-07 US US06/385,529 patent/US4614815A/en not_active Expired - Fee Related

Also Published As

Publication number	Publication date
CH650769A5 (it)	1985-08-15
ZA804455B (en)	1981-07-29
YU192580A (en)	1984-02-29
AU536158B2 (en)	1984-04-19
DK158660B (da)	1990-07-02
YU41446B (en)	1987-06-30
AU6068680A (en)	1981-03-19
IT1123574B (it)	1986-04-30
NO151197B (no)	1984-11-19
CA1172650A (en)	1984-08-14
NL8004512A (nl)	1981-03-12
CS221975B2 (en)	1983-04-29
SU1389676A3 (ru)	1988-04-15
JPS5640649A (en)	1981-04-16
BE884650A (fr)	1981-02-06
US4614815A (en)	1986-09-30
JPH021136B2 (cs)	1990-01-10
FR2468583B1 (cs)	1984-02-17
HU191172B (en)	1987-01-28
GB2058053A (en)	1981-04-08
DE3029970A1 (de)	1981-03-12
SE8005346L (sv)	1981-03-11
NO802196L (no)	1981-03-11
GB2058053B (en)	1983-10-05
NO151197C (no)	1985-02-27
DE3029970C2 (de)	1984-10-04
IT7925570A0 (it)	1979-09-10
FR2468583A1 (fr)	1981-05-08
SE439304B (sv)	1985-06-10
DK313380A (da)	1981-03-11
DD152336A5 (de)	1981-11-25
DK158660C (da)	1991-01-21

Publication	Publication Date	Title
FR2468583A1 (fr)	1981-05-08	Procede pour la preparation de diesterdiamides
JP2862796B2 (ja)	1999-03-03	ジアリールカーボネートの精製法
FR2501673A1 (fr)	1982-09-17	Procede continu de production d'acide terephtalique
EP0461096B1 (fr)	1997-02-05	Procédé de fabrication de N-phénylmaléimide
EP0237446A1 (fr)	1987-09-16	Procédé de préparation d'acides perhalogénométhanesulfiniques et sulfoniques et de leurs sels
US5182392A (en)	1993-01-26	Process for producing bistrimellitic imide
CN116178182B (zh)	2023-09-19	一种2-甲基-4-甲氧基二苯胺的制备方法
EP0102297B1 (fr)	1985-10-23	Procédé de décomposition d'un complexe d'acide ortho-benzoyl-benzoique, de fluorure d'hydrogène et de trifluorure de bore
EP0478428B1 (fr)	1995-03-08	Procédé de préparation d'oxyde borique par hydrolyse du borate de méthyle et sa mise en oeuvre dans l'oxydation d'hydrocarbures saturées en alcools
EP0169107B1 (fr)	1987-09-02	Procédé de purification du mercaptobenzothiazole
EP0296990B1 (fr)	1991-12-04	Procédé de fabrication de polybutadiène hydroxylé
EP0035759B1 (en)	1985-07-10	Process for producing dithionites
BE1000127A3 (fr)	1988-04-12	Composants de catalyseurs pour catalyseurs de polymerisation d'alpha-olefines, et procede pour les fabriquer.
WO2002046096A1 (fr)	2002-06-13	Procede de fabrication d'hydrazine en solution aqueuse
KR100228736B1 (ko)	1999-11-01	말론산에스터 폐액으로부터 말론산디알킬에스터의 제조방법
JP4240565B2 (ja)	2009-03-18	アクリル酸エステルの製造法
FR2583040A1 (fr)	1986-12-12	Procede pour la production de 2,6-naphtalenediol et de 2,6-diacetoxynaphtalene
FR2588859A1 (fr)	1987-04-24	Procede pour la production du di(hydroxy-2 propyl-2)-2,6 naphtalene
FR2634196A1 (fr)	1990-01-19	Procede de preparation de l'acide methoxyacetique
KR20000033754A (ko)	2000-06-15	말론산디알킬에스터의 회수방법
BE546930A (cs)
BE589404A (cs)
BE534731A (cs)
JPS589046B2 (ja)	1983-02-18	硫酸ヒドラジンの製法
FR2795720A1 (fr)	2001-01-05	Procede de cristallisation d'acide carboxylique et procede de fabrication d'acide carboxylique cristallise