SE439304B - Forfarande for framstellning av diesterdiamider - Google Patents

Forfarande for framstellning av diesterdiamider

Info

Publication number: SE439304B
Authority: SE; Sweden
Prior art keywords: diester; ester salt; solvent; diamide; catalyst
Prior art date: 1979-09-10

Application number

SE8005346A

Other languages

English (en)

Swedish (sv)

Other versions

SE8005346L (sv

Inventor

F Cognigni

A Mariano

Original Assignee

Anic Spa

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1979-09-10

Filing date

1980-07-23

Publication date

1985-06-10

1980-07-23 Application filed by Anic Spa filed Critical Anic Spa

1981-03-11 Publication of SE8005346L publication Critical patent/SE8005346L/xx

1985-06-10 Publication of SE439304B publication Critical patent/SE439304B/sv

Links

238000000034 method Methods 0.000 title claims description 4
238000002360 preparation method Methods 0.000 title claims 2
YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims description 42
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 39
WOZVHXUHUFLZGK-UHFFFAOYSA-N dimethyl terephthalate Chemical compound COC(=O)C1=CC=C(C(=O)OC)C=C1 WOZVHXUHUFLZGK-UHFFFAOYSA-N 0.000 claims description 26
239000002904 solvent Substances 0.000 claims description 26
-1 ester salt Chemical class 0.000 claims description 25
150000005690 diesters Chemical class 0.000 claims description 19
239000000203 mixture Substances 0.000 claims description 19
238000005406 washing Methods 0.000 claims description 17
OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical compound NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 claims description 16
239000003054 catalyst Substances 0.000 claims description 13
238000001914 filtration Methods 0.000 claims description 11
230000015572 biosynthetic process Effects 0.000 claims description 9
238000003786 synthesis reaction Methods 0.000 claims description 9
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 8
JILPJDVXYVTZDQ-UHFFFAOYSA-N lithium methoxide Chemical compound [Li+].[O-]C JILPJDVXYVTZDQ-UHFFFAOYSA-N 0.000 claims description 8
239000000376 reactant Substances 0.000 claims description 8
239000007788 liquid Substances 0.000 claims description 6
239000010413 mother solution Substances 0.000 claims description 5
239000000243 solution Substances 0.000 claims description 5
229910052751 metal Inorganic materials 0.000 claims description 4
239000002184 metal Substances 0.000 claims description 4
150000004985 diamines Chemical class 0.000 claims description 2
150000002148 esters Chemical class 0.000 claims description 2
230000007062 hydrolysis Effects 0.000 claims description 2
238000006460 hydrolysis reaction Methods 0.000 claims description 2
XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 claims description 2
239000012535 impurity Substances 0.000 claims description 2
239000000047 product Substances 0.000 description 6
RCRBCNZJGBTYDI-UHFFFAOYSA-L dilithium;terephthalate Chemical compound [Li+].[Li+].[O-]C(=O)C1=CC=C(C([O-])=O)C=C1 RCRBCNZJGBTYDI-UHFFFAOYSA-L 0.000 description 5
NAQMVNRVTILPCV-UHFFFAOYSA-N hexane-1,6-diamine Chemical compound NCCCCCCN NAQMVNRVTILPCV-UHFFFAOYSA-N 0.000 description 4
229910052744 lithium Inorganic materials 0.000 description 4
UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
238000006243 chemical reaction Methods 0.000 description 3
239000000178 monomer Substances 0.000 description 3
VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
229920000642 polymer Polymers 0.000 description 3
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 2
WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 2
LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 2
IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 description 2
239000003513 alkali Substances 0.000 description 2
229910052784 alkaline earth metal Inorganic materials 0.000 description 2
239000006227 byproduct Substances 0.000 description 2
230000006866 deterioration Effects 0.000 description 2
238000005755 formation reaction Methods 0.000 description 2
229930195733 hydrocarbon Natural products 0.000 description 2
150000002430 hydrocarbons Chemical class 0.000 description 2
ZXEKIIBDNHEJCQ-UHFFFAOYSA-N isobutanol Chemical compound CC(C)CO ZXEKIIBDNHEJCQ-UHFFFAOYSA-N 0.000 description 2
238000004519 manufacturing process Methods 0.000 description 2
238000000926 separation method Methods 0.000 description 2
238000009987 spinning Methods 0.000 description 2
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 1
DKMROQRQHGEIOW-UHFFFAOYSA-N Diethyl succinate Chemical compound CCOC(=O)CCC(=O)OCC DKMROQRQHGEIOW-UHFFFAOYSA-N 0.000 description 1
WQDUMFSSJAZKTM-UHFFFAOYSA-N Sodium methoxide Chemical compound [Na+].[O-]C WQDUMFSSJAZKTM-UHFFFAOYSA-N 0.000 description 1
150000001298 alcohols Chemical class 0.000 description 1
150000001342 alkaline earth metals Chemical class 0.000 description 1
230000000903 blocking effect Effects 0.000 description 1
230000003197 catalytic effect Effects 0.000 description 1
238000005119 centrifugation Methods 0.000 description 1
239000003153 chemical reaction reagent Substances 0.000 description 1
238000010908 decantation Methods 0.000 description 1
ONIHPYYWNBVMID-UHFFFAOYSA-N diethyl benzene-1,4-dicarboxylate Chemical compound CCOC(=O)C1=CC=C(C(=O)OCC)C=C1 ONIHPYYWNBVMID-UHFFFAOYSA-N 0.000 description 1
VNGOYPQMJFJDLV-UHFFFAOYSA-N dimethyl benzene-1,3-dicarboxylate Chemical compound COC(=O)C1=CC=CC(C(=O)OC)=C1 VNGOYPQMJFJDLV-UHFFFAOYSA-N 0.000 description 1
VIQSRHWJEKERKR-UHFFFAOYSA-L disodium;terephthalate Chemical compound [Na+].[Na+].[O-]C(=O)C1=CC=C(C([O-])=O)C=C1 VIQSRHWJEKERKR-UHFFFAOYSA-L 0.000 description 1
238000004821 distillation Methods 0.000 description 1
238000001035 drying Methods 0.000 description 1
239000000835 fiber Substances 0.000 description 1
BBCLUPOZFBVMPB-UHFFFAOYSA-M lithium 4-methoxycarbonylbenzoate Chemical compound C(C1=CC=C(C(=O)[O-])C=C1)(=O)OC.[Li+] BBCLUPOZFBVMPB-UHFFFAOYSA-M 0.000 description 1
150000002642 lithium compounds Chemical class 0.000 description 1
AZVCGYPLLBEUNV-UHFFFAOYSA-N lithium;ethanolate Chemical compound [Li+].CC[O-] AZVCGYPLLBEUNV-UHFFFAOYSA-N 0.000 description 1
239000000463 material Substances 0.000 description 1
238000002844 melting Methods 0.000 description 1
230000008018 melting Effects 0.000 description 1
239000012452 mother liquor Substances 0.000 description 1
239000002244 precipitate Substances 0.000 description 1
BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 1
238000000746 purification Methods 0.000 description 1
238000004064 recycling Methods 0.000 description 1
229910052708 sodium Inorganic materials 0.000 description 1
239000011734 sodium Substances 0.000 description 1
QDRKDTQENPPHOJ-UHFFFAOYSA-N sodium ethoxide Chemical compound [Na+].CC[O-] QDRKDTQENPPHOJ-UHFFFAOYSA-N 0.000 description 1
239000011877 solvent mixture Substances 0.000 description 1
239000007858 starting material Substances 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C231/00—Preparation of carboxylic acid amides
- C07C231/02—Preparation of carboxylic acid amides from carboxylic acids or from esters, anhydrides, or halides thereof by reaction with ammonia or amines

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Chemical Kinetics & Catalysis (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Polyamides (AREA)
Steroid Compounds (AREA)

SE8005346A 1979-09-10 1980-07-23 Forfarande for framstellning av diesterdiamider SE439304B (sv)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
IT25570/79A IT1123574B (it)	1979-09-10	1979-09-10	Processo per la produzione di diesterediammidi

Publications (2)

Publication Number	Publication Date
SE8005346L SE8005346L (sv)	1981-03-11
SE439304B true SE439304B (sv)	1985-06-10

Family

ID=11217125

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
SE8005346A SE439304B (sv)	1979-09-10	1980-07-23	Forfarande for framstellning av diesterdiamider

Country Status (21)

Country	Link
US (1)	US4614815A (cs)
JP (1)	JPS5640649A (cs)
AU (1)	AU536158B2 (cs)
BE (1)	BE884650A (cs)
CA (1)	CA1172650A (cs)
CH (1)	CH650769A5 (cs)
CS (1)	CS221975B2 (cs)
DD (1)	DD152336A5 (cs)
DE (1)	DE3029970C2 (cs)
DK (1)	DK158660C (cs)
FR (1)	FR2468583A1 (cs)
GB (1)	GB2058053B (cs)
HU (1)	HU191172B (cs)
IT (1)	IT1123574B (cs)
LU (1)	LU82686A1 (cs)
NL (1)	NL8004512A (cs)
NO (1)	NO151197C (cs)
SE (1)	SE439304B (cs)
SU (1)	SU1389676A3 (cs)
YU (1)	YU41446B (cs)
ZA (1)	ZA804455B (cs)

Families Citing this family (17)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US4767839A (en) *	1987-07-06	1988-08-30	Allied-Signal Inc.	Alternating aliphatic-aromatic poly(esteramide)
US5608108A (en) *	1988-11-14	1997-03-04	Sloan-Kettering Institute For Cancer Research	Potent inducers of terminal differentiation and method of use thereof
CA2002853A1 (en) *	1988-11-14	1990-05-14	Ronald Breslow	Potent inducers of terminal differentiation and method of use thereof
DE4024466C2 (de) *	1990-07-30	1995-04-20	Dainippon Ink & Chemicals	Thermisch härtbare Mischungen aus polyfunktionellen Formamiden und aromatischen Mono-, Di- oder Polyglycidylethern und deren Verwendung
USRE38506E1 (en)	1991-10-04	2004-04-20	Sloan-Kettering Institute For Cancer Research	Potent inducers of terminal differentiation and methods of use thereof
US5700811A (en) *	1991-10-04	1997-12-23	Sloan-Kettering Institute For Cancer Research	Potent inducers of terminal differentiation and method of use thereof
US5369108A (en) *	1991-10-04	1994-11-29	Sloan-Kettering Institute For Cancer Research	Potent inducers of terminal differentiation and methods of use thereof
WO1995035330A1 (en) *	1994-06-17	1995-12-28	Exxon Chemical Patents Inc.	Amidation of ester functionalized hydrocarbon polymers
US5852155A (en) *	1995-03-01	1998-12-22	General Electric Company	Compositions of polyesteramides
US5744068A (en) *	1996-01-24	1998-04-28	General Electric Company	Blends of polyphenylene ethers and polyesteramides
US5731389A (en) *	1996-04-24	1998-03-24	General Electric Company	Blends of polyesters and polyesteramides, optionally with polycarbonates
CA2225792A1 (en) *	1996-04-30	1997-11-06	Toshihide Inoue	Polyester amide copolymer and method of producing the same, polyester amide monomer and method of producing the same, and polyester amide resin composition
KR20020059393A (ko) *	1999-09-08	2002-07-12	제임스 에스. 쿼크	새로운 부류의 세포분화제 및 히스톤 데아세틸라아제, 및이의 사용 방법
JP2006523693A (ja) *	2003-04-01	2006-10-19	メモリアルスローン−ケタリングキャンサーセンター	ヒドロキサム酸化合物およびその使用方法
US20150119604A1 (en) *	2012-04-11	2015-04-30	Idemitsu Kosan Co., Ltd.	Method for producing beta-alkoxypropionamide
US10040904B2 (en)	2013-08-16	2018-08-07	Dsm Ip Assets B.V.	Process for producing a thermoplastic polymer containing segments of a diamide
KR101568357B1 (ko) *	2013-11-25	2015-11-12	롯데케미칼 주식회사	신규 화합물 및 이의 제조방법

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US2925405A (en) *	1955-04-26	1960-02-16	Eastman Kodak Co	Linear polyesters containing an alkylene diamine group and manufacture thereof
US2839508A (en) *	1955-04-26	1958-06-17	Eastman Kodak Co	Copolyesters of a glycol, an alkylene diamine dicarboxylate and a sulfone ester
US2851443A (en) *	1955-04-26	1958-09-09	Eastman Kodak Co	Quenchable copolyesters of a glycol, terephthalic acid and an alkylene diamine dicarboxylate and their preparation
US2861055A (en) *	1955-04-26	1958-11-18	Eastman Kodak Co	Copolyesters of a glycol and an alkylene diamine dicarboxylate containing isophthalate modifier and their preparation
US2848439A (en) *	1955-04-26	1958-08-19	Eastman Kodak Co	Linear polyesters of bis (nu-p-carboxyphenyl) alkylene diamides and manufacture thereof
US2856385A (en) *	1956-05-10	1958-10-14	Eastman Kodak Co	Polyester-amides of n,n'-bis-(p-carboxybenzoyl) alkylenediamines, glycols and diamines
SU1069623A3 (ru) *	1970-10-13	1984-01-23	Снам Прогетти С.П.А. (Фирма)	Способ получени диамидодиэфиров

1979
- 1979-09-10 IT IT25570/79A patent/IT1123574B/it active
1980
- 1980-07-17 CH CH5485/80A patent/CH650769A5/it not_active IP Right Cessation
- 1980-07-21 DK DK313380A patent/DK158660C/da not_active IP Right Cessation
- 1980-07-22 AU AU60686/80A patent/AU536158B2/en not_active Ceased
- 1980-07-22 NO NO802196A patent/NO151197C/no unknown
- 1980-07-23 ZA ZA00804455A patent/ZA804455B/xx unknown
- 1980-07-23 SE SE8005346A patent/SE439304B/sv not_active IP Right Cessation
- 1980-07-24 GB GB8024330A patent/GB2058053B/en not_active Expired
- 1980-07-24 CA CA000356970A patent/CA1172650A/en not_active Expired
- 1980-07-30 YU YU1925/80A patent/YU41446B/xx unknown
- 1980-08-04 LU LU82686A patent/LU82686A1/fr unknown
- 1980-08-05 FR FR8017294A patent/FR2468583A1/fr active Granted
- 1980-08-06 BE BE0/201664A patent/BE884650A/fr not_active IP Right Cessation
- 1980-08-06 SU SU802957756A patent/SU1389676A3/ru active
- 1980-08-06 JP JP10724780A patent/JPS5640649A/ja active Granted
- 1980-08-06 CS CS805438A patent/CS221975B2/cs unknown
- 1980-08-06 DD DD80223155A patent/DD152336A5/de unknown
- 1980-08-06 HU HU801956A patent/HU191172B/hu not_active IP Right Cessation
- 1980-08-07 NL NL8004512A patent/NL8004512A/nl not_active Application Discontinuation
- 1980-08-07 DE DE3029970A patent/DE3029970C2/de not_active Expired
1982
- 1982-06-07 US US06/385,529 patent/US4614815A/en not_active Expired - Fee Related

Also Published As

Publication number	Publication date
CA1172650A (en)	1984-08-14
SU1389676A3 (ru)	1988-04-15
YU192580A (en)	1984-02-29
AU6068680A (en)	1981-03-19
AU536158B2 (en)	1984-04-19
JPS5640649A (en)	1981-04-16
GB2058053A (en)	1981-04-08
ZA804455B (en)	1981-07-29
IT1123574B (it)	1986-04-30
DK158660C (da)	1991-01-21
DK313380A (da)	1981-03-11
FR2468583B1 (cs)	1984-02-17
SE8005346L (sv)	1981-03-11
CS221975B2 (en)	1983-04-29
DD152336A5 (de)	1981-11-25
FR2468583A1 (fr)	1981-05-08
LU82686A1 (fr)	1981-03-24
NO802196L (no)	1981-03-11
BE884650A (fr)	1981-02-06
NL8004512A (nl)	1981-03-12
JPH021136B2 (cs)	1990-01-10
DK158660B (da)	1990-07-02
IT7925570A0 (it)	1979-09-10
DE3029970A1 (de)	1981-03-12
US4614815A (en)	1986-09-30
YU41446B (en)	1987-06-30
CH650769A5 (it)	1985-08-15
NO151197C (no)	1985-02-27
HU191172B (en)	1987-01-28
DE3029970C2 (de)	1984-10-04
NO151197B (no)	1984-11-19
GB2058053B (en)	1983-10-05

Legal Events

Date

Code

Title

Description

1995-01-31

NUG

Patent has lapsed

Ref document number: 8005346-5

Effective date: 19920210

Format of ref document f/p: F

Publication	Publication Date	Title
SE439304B (sv)	1985-06-10	Forfarande for framstellning av diesterdiamider
GB2061941A (en)	1981-05-20	Process for recovery of polyol fatty acid polyesters
ITBO950017A1 (it)	1996-07-24	Processo per la preparazione di bis (2-idrossietil) teraftalato
EP3848357B1 (en)	2023-01-18	Reactive benzotriazole uv absorber and use thereof
CN108997424B (zh)	2020-11-13	一种简捷制备磷霉素氨丁三醇的方法
US5182392A (en)	1993-01-26	Process for producing bistrimellitic imide
US2494133A (en)	1950-01-10	Method of neutralizing and completely removing salts before distilling crude high-boiling esters
CN119684373A (zh)	2025-03-25	三（二甲胺基）环戊二烯基铪及其制备工艺
EP0022816B1 (en)	1983-07-13	The preparation of antioxidant amides
CN223430308U (zh)	2025-10-14	一种bdp酸洗、碱洗、水洗系统
CN1075510C (zh)	2001-11-28	一种制备乙二醇锑的方法
DE69116507T2 (de)	1996-05-30	Verfahren zur Gewinnung von hochreiner Zimtsäure
US2083870A (en)	1937-06-15	Preparation of sodium hydrosulphite
CN115974767B (zh)	2026-03-27	一种三丙酮胺精馏过程中连续除盐的方法及系统装置
EP0035759B1 (en)	1985-07-10	Process for producing dithionites
US5011965A (en)	1991-04-30	Process for production of methylene bisxanthates
US2102016A (en)	1937-12-14	Method of separating an organic acid ester of cellulose from its reaction mixture
CN108314621A (zh)	2018-07-24	一种制造长链二酸单酯的方法
JPS611680A (ja)	1986-01-07	アルケニル無水コハク酸の製造方法
JPS62106052A (ja)	1987-05-16	アクリル酸エステル類の製造法
SU332716A1 (ru)	1976-02-15	Способ выделени уксусной кислоты из кубового остатка производства винилацетата
US6646119B1 (en)	2003-11-11	Acetylated pyroxylin
CN119588269A (zh)	2025-03-11	一种bdp酸洗、碱洗、水洗系统及洗涤工艺
US3646124A (en)	1972-02-29	Process for purification of terephthalic acid or its salt
JPH02237974A (ja)	1990-09-20	ビス（２・２・６・６―テトラメチル―４―ピペリジル）セバケートの新規製造法