PE20142014A1 - Proceso nuevo en smb - Google Patents

Proceso nuevo en smb

Info

Publication number
PE20142014A1
PE20142014A1 PE2014000007A PE2014000007A PE20142014A1 PE 20142014 A1 PE20142014 A1 PE 20142014A1 PE 2014000007 A PE2014000007 A PE 2014000007A PE 2014000007 A PE2014000007 A PE 2014000007A PE 20142014 A1 PE20142014 A1 PE 20142014A1
Authority
PE
Peru
Prior art keywords
product
pufa
separation step
chromatography
separation
Prior art date
Application number
PE2014000007A
Other languages
English (en)
Inventor
Adam Kelliher
Angus Morrison
Anil Oroskar
Rema Rakesh Vikraman Nair
Abhilesh Agarwal
Original Assignee
Basf Pharma Callanish Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Pharma Callanish Ltd filed Critical Basf Pharma Callanish Ltd
Publication of PE20142014A1 publication Critical patent/PE20142014A1/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/10—Refining fats or fatty oils by adsorption
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
    • B01D15/18—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
    • B01D15/1814—Recycling of the fraction to be distributed
    • B01D15/1821—Simulated moving beds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
    • B01D15/18—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
    • B01D15/1814—Recycling of the fraction to be distributed
    • B01D15/1821—Simulated moving beds
    • B01D15/185—Simulated moving beds characterised by the components to be separated
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
    • B01D15/18—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
    • B01D15/1892—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns the sorbent material moving as a whole, e.g. continuous annular chromatography, true moving beds or centrifugal chromatography
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B7/00—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils
    • C11B7/0008—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils by differences of solubilities, e.g. by extraction, by separation from a solution by means of anti-solvents
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B7/00—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils
    • C11B7/0008—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils by differences of solubilities, e.g. by extraction, by separation from a solution by means of anti-solvents
    • C11B7/0025—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils by differences of solubilities, e.g. by extraction, by separation from a solution by means of anti-solvents in solvents containing oxygen in their molecule
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C1/00—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
    • C11C1/005—Splitting up mixtures of fatty acids into their constituents
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C1/00—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
    • C11C1/007—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids using organic solvents

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Analytical Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Microbiology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Sustainable Development (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Fats And Perfumes (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)

Abstract

REFERIDA A UN PROCESO DE SEPARACION CROMATOGRAFICA PARA LA RECUPERACION DE UN PRODUCTO DEL ACIDO POLIINSATURADO (PUFA) A PARTIR DE UNA MEZCLA DE ALIMENTACION, EL CUAL COMPRENDE i) LA PURIFICACION DE LA MEZCLA DE ALIMENTACION EN UN PRIMER PASO DE SEPARACION EN UN APARATO DE CROMATOGRAFIA EN LECHO MOVIL, REAL O SIMULADO, TENIENDO UNA PLURALIDAD DE COLUMNAS CROMATOGRAFICAS ENLAZADAS CONTENIENDO COMO ELUYENTE, UN SOLVENTE ORGANICO ACUOSO, CON EL FIN DE OBTENER UN PRODUCTO INTERMEDIARIO Y ii) LA PURIFICACION DEL PRODUCTO INTERMEDIARIO OBTENIDO EN i) EN UN SEGUNDO PASO DE SEPARACION, USANDO UN APARATO DE CROMATOGRAFIA EN LECHO MOVIL, REAL O SIMULADO, TENIENDO UNA PLURALIDAD DE COLUMNAS DE CROMATOGRAFIA ENLAZADAS CONTENIENDO, COMO ELUYENTE, UN SOLVENTE ORGANICO ACUOSO, CON EL FIN DE OBTENER UN PRODUCTO DEL PUFA, DONDE a) EL PRIMER Y SEGUNDO PASO DE SEPARACION SE REALIZAN EN FORMA SECUENCIAL EN EL MISMO APARATO DE CROMATOGRAFIA, DE MANERA QUE EL PRODUCTO DEL PUFA ES SEPARADO DE LOS DIFERENTES COMPONENTES DE LA MEZCLA DE ALIMENTACION O b) EL PRIMER Y SEGUNDO PASO DE SEPARACION SE REALIZAN EN APARATOS DE CROMATOGRAFIA SEPARADOS, SIENDO EL PRODUCTO INTERMEDIARIO OBTENIDO A PARTIR DEL PRIMER PASO DE SEPARACION INTRODUCIDO DENTRO DEL SEGUNDO APARATO DE CROMATOGRAFIA Y SIENDO EL PRODUCTO DEL PUFA SEPARADO DE LOS DIFERENTES COMPONENTES DE LA MEZCLA DE ALIMENTACION. EL PRODUCTO DEL PUFA COMPRENDE UN PUFA OMEGA-3 TALES COMO EL ACIDO EICOSAPENTAENOICO (EPA) Y EL ACIDO DOCOSAHEXAENOICO (DHA)
PE2014000007A 2011-07-06 2012-07-06 Proceso nuevo en smb PE20142014A1 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GBGB1111589.6A GB201111589D0 (en) 2011-07-06 2011-07-06 New modified process

Publications (1)

Publication Number Publication Date
PE20142014A1 true PE20142014A1 (es) 2014-12-24

Family

ID=44544336

Family Applications (1)

Application Number Title Priority Date Filing Date
PE2014000007A PE20142014A1 (es) 2011-07-06 2012-07-06 Proceso nuevo en smb

Country Status (17)

Country Link
US (1) US9260677B2 (es)
EP (1) EP2613862B1 (es)
JP (1) JP5990580B2 (es)
KR (1) KR101603448B1 (es)
CN (1) CN103796724B (es)
AU (1) AU2012279993B2 (es)
BR (1) BR112014000152B1 (es)
CA (1) CA2815301C (es)
CL (1) CL2013003799A1 (es)
DK (1) DK2613862T3 (es)
ES (1) ES2710652T3 (es)
GB (1) GB201111589D0 (es)
HU (1) HUE043139T2 (es)
PE (1) PE20142014A1 (es)
PL (1) PL2613862T3 (es)
TR (1) TR201819866T4 (es)
WO (1) WO2013005051A1 (es)

Families Citing this family (19)

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US9321715B2 (en) 2009-12-30 2016-04-26 Basf Pharma (Callanish) Limited Simulated moving bed chromatographic separation process
GB201111594D0 (en) 2011-07-06 2011-08-24 Equateq Ltd New improved process
GB201111595D0 (en) 2011-07-06 2011-08-24 Equateq Ltd Improved process
GB201111589D0 (en) 2011-07-06 2011-08-24 Equateq Ltd New modified process
GB201111591D0 (en) 2011-07-06 2011-08-24 Equateq Ltd Further new process
GB201111601D0 (en) 2011-07-06 2011-08-24 Equateq Ltd New process
GB201300354D0 (en) * 2013-01-09 2013-02-20 Basf Pharma Callanish Ltd Multi-step separation process
EP2801604B1 (en) 2013-05-07 2017-04-12 Groupe Novasep Chromatographic process for the production of highly purified polyunsaturated fatty acids
US9428711B2 (en) 2013-05-07 2016-08-30 Groupe Novasep Chromatographic process for the production of highly purified polyunsaturated fatty acids
EP2994523B1 (en) * 2013-05-07 2024-02-21 Groupe Novasep Chromatographic process for the production of highly purified polyunsaturated fatty acids
FR3014436B1 (fr) 2013-12-11 2016-10-21 Novasep Process Procede de purification chromatographique d'un acide gras
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JP6303017B2 (ja) 2014-01-07 2018-03-28 ノヴァセプ プロセスＮｏｖａｓｅｐ Ｐｒｏｃｅｓｓ 芳香族アミノ酸を精製する方法
US9163198B2 (en) * 2014-01-17 2015-10-20 Orochem Technologies, Inc. Process for purification of EPA (eicosapentanoic acid) ethyl ester from fish oil
US9546125B2 (en) * 2015-02-11 2017-01-17 Orochem Technologies, Inc. Continuous process for extraction of unsaturated triglycerides from fish oil
TWI648258B (zh) * 2017-07-10 2019-01-21 喬璞科技有限公司 純化不飽和脂肪酸以及二十碳五烯酸的方法
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WO2023111317A1 (en) 2021-12-17 2023-06-22 Basf Se Chromatographic separation process for efficient purification of polyunsaturated fatty acids

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CA2815301C (en) 2015-09-29
KR101603448B1 (ko) 2016-03-14
HUE043139T2 (hu) 2019-07-29
PL2613862T3 (pl) 2019-05-31
JP2014523944A (ja) 2014-09-18
BR112014000152B1 (pt) 2020-10-27
CA2815301A1 (en) 2013-01-10
JP5990580B2 (ja) 2016-09-14
BR112014000152A2 (pt) 2017-02-14
CN103796724B (zh) 2015-07-15
EP2613862B1 (en) 2018-12-19
CN103796724A (zh) 2014-05-14
DK2613862T3 (en) 2019-03-11
TR201819866T4 (tr) 2019-01-21
US9260677B2 (en) 2016-02-16
ES2710652T3 (es) 2019-04-26
US20140128627A1 (en) 2014-05-08
CL2013003799A1 (es) 2014-07-04
WO2013005051A1 (en) 2013-01-10
GB201111589D0 (en) 2011-08-24
EP2613862A1 (en) 2013-07-17
AU2012279993A1 (en) 2013-05-02

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