PL401501A1 - Wielowarstwowy kompozyt do rewersyjnej sorpcji rtęci oraz sposób sorpcji i desorpcji rtęci z fazy gazowej - Google Patents

Wielowarstwowy kompozyt do rewersyjnej sorpcji rtęci oraz sposób sorpcji i desorpcji rtęci z fazy gazowej

Info

Publication number
PL401501A1
PL401501A1 PL401501A PL40150112A PL401501A1 PL 401501 A1 PL401501 A1 PL 401501A1 PL 401501 A PL401501 A PL 401501A PL 40150112 A PL40150112 A PL 40150112A PL 401501 A1 PL401501 A1 PL 401501A1
Authority
PL
Poland
Prior art keywords
mercury
sorption
multilayer composite
gas phase
desorption
Prior art date
Application number
PL401501A
Other languages
English (en)
Other versions
PL229084B1 (pl
Inventor
Piotr Kula
Robert Pietrasik
Małgorzata Iwona Szynkowska
Ewa LEŚNIEWSKA
Jacek Góralski
Piotr Niedzielski
Jadwiga Albińska
Sławomir Szafran
Tomasz Maniecki
Original Assignee
Politechnika Łódzka
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Politechnika Łódzka filed Critical Politechnika Łódzka
Priority to PL401501A priority Critical patent/PL229084B1/pl
Priority to PCT/PL2013/000141 priority patent/WO2014073996A1/en
Priority to EP13802461.7A priority patent/EP2916930B1/en
Priority to US14/440,905 priority patent/US9636623B2/en
Priority to ES13802461.7T priority patent/ES2665749T3/es
Publication of PL401501A1 publication Critical patent/PL401501A1/pl
Publication of PL229084B1 publication Critical patent/PL229084B1/pl

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/0407—Constructional details of adsorbing systems
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34—Chemical or biological purification of waste gases
    • B01D53/46—Removing components of defined structure
    • B01D53/64—Heavy metals or compounds thereof, e.g. mercury
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/0203—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of metals not provided for in B01J20/04
    • B01J20/0225—Compounds of Fe, Ru, Os, Co, Rh, Ir, Ni, Pd, Pt
    • B01J20/0229—Compounds of Fe
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/0203—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of metals not provided for in B01J20/04
    • B01J20/0274—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of metals not provided for in B01J20/04 characterised by the type of anion
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/0203—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of metals not provided for in B01J20/04
    • B01J20/0274—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of metals not provided for in B01J20/04 characterised by the type of anion
    • B01J20/0285—Sulfides of compounds other than those provided for in B01J20/045
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3202—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the carrier, support or substrate used for impregnation or coating
    • B01J20/3204—Inorganic carriers, supports or substrates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3231—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the coating or impregnating layer
    • B01J20/3234—Inorganic material layers
    • B01J20/3236—Inorganic material layers containing metal, other than zeolites, e.g. oxides, hydroxides, sulphides or salts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3231—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the coating or impregnating layer
    • B01J20/3289—Coatings involving more than one layer of same or different nature
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/34—Regenerating or reactivating
    • B01J20/3433—Regenerating or reactivating of sorbents or filter aids other than those covered by B01J20/3408 - B01J20/3425
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/34—Regenerating or reactivating
    • B01J20/345—Regenerating or reactivating using a particular desorbing compound or mixture
    • B01J20/3458—Regenerating or reactivating using a particular desorbing compound or mixture in the gas phase
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/34—Regenerating or reactivating
    • B01J20/3483—Regenerating or reactivating by thermal treatment not covered by groups B01J20/3441 - B01J20/3475, e.g. by heating or cooling
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2251/00—Reactants
    • B01D2251/60—Inorganic bases or salts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10—Inorganic adsorbents
    • B01D2253/112—Metals or metal compounds not provided for in B01D2253/104 or B01D2253/106
    • B01D2253/1128—Metal sulfides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2256/00—Main component in the product gas stream after treatment
    • B01D2256/10—Nitrogen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/60—Heavy metals or heavy metal compounds
    • B01D2257/602—Mercury or mercury compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2258/00—Sources of waste gases
    • B01D2258/02—Other waste gases
    • B01D2258/0283—Flue gases
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40083—Regeneration of adsorbents in processes other than pressure or temperature swing adsorption
    • B01D2259/40088—Regeneration of adsorbents in processes other than pressure or temperature swing adsorption by heating
    • B01D2259/4009—Regeneration of adsorbents in processes other than pressure or temperature swing adsorption by heating using hot gas
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34—Chemical or biological purification of waste gases
    • B01D53/96—Regeneration, reactivation or recycling of reactants

Landscapes

  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Chemical & Material Sciences (AREA)
  • Thermal Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Biomedical Technology (AREA)
  • Environmental & Geological Engineering (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Treating Waste Gases (AREA)

Abstract

Wielowarstwowy kompozyt do rewersyjnej sorpcji rtęci z rdzeniem nośnym z metalu lub stopu na bazie metali przejściowych ma dwustronnie na rdzeniu osadzone warstwy izolujące z azotku metalu przejściowego oraz usytuowane zewnętrznie warstwy sorbujące, wykonane z mieszaniny siarczków i azotków metali przejściowych. Sposób sorpcji rtęci z fazy gazowej polega na tym, że podczas ekspozycji w przedziale od 0,5 do 24 godzin wielowarstwowego kompozytu na działanie wieloskładnikowych mieszanin gazowych, zawierających pary lub związki rtęci, utrzymuje się temperaturę wielowarstwowego kompozytu w granicach od 20 do 150°C.
PL401501A 2012-11-07 2012-11-07 Wielowarstwowy kompozyt do rewersyjnej sorpcji rtęci oraz sposób sorpcji i desorpcji rtęci z fazy gazowej PL229084B1 (pl)

Priority Applications (5)

Application Number Priority Date Filing Date Title
PL401501A PL229084B1 (pl) 2012-11-07 2012-11-07 Wielowarstwowy kompozyt do rewersyjnej sorpcji rtęci oraz sposób sorpcji i desorpcji rtęci z fazy gazowej
PCT/PL2013/000141 WO2014073996A1 (en) 2012-11-07 2013-11-06 Multilayer composite for reversible sorption of mercury and method for sorption and desorption of mercury from a gaseous phase
EP13802461.7A EP2916930B1 (en) 2012-11-07 2013-11-06 Multilayer composite for reversible sorption of mercury and method for sorption and desorption of mercury from a gaseous phase
US14/440,905 US9636623B2 (en) 2012-11-07 2013-11-06 Multilayer composite for reversible sorption of mercury and method for sorption and desorption of mercury from a gaseous phase
ES13802461.7T ES2665749T3 (es) 2012-11-07 2013-11-06 Material compuesto multicapa para la sorción reversible de mercurio y procedimiento para la sorción y la desorción de mercurio a partir de una fase gaseosa

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PL401501A PL229084B1 (pl) 2012-11-07 2012-11-07 Wielowarstwowy kompozyt do rewersyjnej sorpcji rtęci oraz sposób sorpcji i desorpcji rtęci z fazy gazowej

Publications (2)

Publication Number Publication Date
PL401501A1 true PL401501A1 (pl) 2014-05-12
PL229084B1 PL229084B1 (pl) 2018-06-29

Family

ID=49726849

Family Applications (1)

Application Number Title Priority Date Filing Date
PL401501A PL229084B1 (pl) 2012-11-07 2012-11-07 Wielowarstwowy kompozyt do rewersyjnej sorpcji rtęci oraz sposób sorpcji i desorpcji rtęci z fazy gazowej

Country Status (5)

Country Link
US (1) US9636623B2 (pl)
EP (1) EP2916930B1 (pl)
ES (1) ES2665749T3 (pl)
PL (1) PL229084B1 (pl)
WO (1) WO2014073996A1 (pl)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3181213A1 (en) 2015-12-14 2017-06-21 PGE Górnictwo | Energetyka Konwencjonalna S.A. Mercury capture system from flue gases generated in a power process of coal burning

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10730034B2 (en) 2017-08-28 2020-08-04 Viviron Technology LLC Iron-selenide-oxide sorbent composition for removing mercury (Hg) vapor from a gaseous stream; methods of use and methods of manufacture

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US2012A (en) 1841-03-18 Machine foe
DE2453143C3 (de) 1973-11-09 1979-09-13 Nippon Mining Co., Ltd., Tokio Verfahren zum Entfernen von Quecksilber aus einem Schwefeldioxyd enthaltenden Gas
DE2656803C2 (de) 1975-12-18 1986-12-18 Institut Français du Pétrole, Rueil-Malmaison, Hauts-de-Seine Verfahren zur Entfernung von in einem Gas oder in einer Flüssigkeit vorhandenem Quecksilber
US5401393A (en) 1993-09-14 1995-03-28 Mobil Oil Corporation Reactive adsorbent and method for removing mercury from hydrocarbon fluids
US6248217B1 (en) * 1997-04-10 2001-06-19 The University Of Cincinnati Process for the enhanced capture of heavy metal emissions
US6328939B1 (en) 1999-03-31 2001-12-11 Mcdermott Technology, Inc. Mercury removal in utility wet scrubber using a chelating agent
US6576092B2 (en) 2001-09-13 2003-06-10 The United States Of America As Represented By The U.S. Department Of Energy Method for removal of mercury from various gas streams
US6713519B2 (en) * 2001-12-21 2004-03-30 Battelle Memorial Institute Carbon nanotube-containing catalysts, methods of making, and reactions catalyzed over nanotube catalysts
US7435286B2 (en) 2004-08-30 2008-10-14 Energy & Environmental Research Center Foundation Sorbents for the oxidation and removal of mercury
US7220390B2 (en) * 2003-05-16 2007-05-22 Velocys, Inc. Microchannel with internal fin support for catalyst or sorption medium
EP1861192A1 (en) * 2005-03-11 2007-12-05 The Regents of the University of Minnesota Air pollutant removal using magnetic sorbent particles
US20060205591A1 (en) 2005-03-11 2006-09-14 Do-Hee Lee Adsorbent for removing mercury using sulfided iron compounds containing oxygen and method of producing same
CA2851742C (en) 2005-03-17 2017-07-11 Nox Ii, Ltd. Reducing mercury emissions from the burning of coal
US7858061B2 (en) 2005-12-15 2010-12-28 The United States Of America As Represented By The Administrator Of The United States Environmental Protection Agency Compositions and methods for removing mercury from mercury-containing fluids
US8236185B2 (en) 2006-03-23 2012-08-07 J.I. Enterprises, Inc. Methods for using sulfidized red mud
US8110163B2 (en) 2007-12-07 2012-02-07 Nalco Company Complexation and removal of heavy metals from flue gas desulfurization systems
US8025160B2 (en) 2007-06-05 2011-09-27 Amcol International Corporation Sulfur-impregnated organoclay mercury and/or arsenic ion removal media
CA2673686A1 (en) 2008-07-23 2010-01-23 Srivats Srinivasachar Method for capturing mercury from flue gas
EP2365856A1 (en) 2008-11-25 2011-09-21 Johnson Matthey PLC Reduced copper sulphide sorbent for removing heavy metals
GB0900965D0 (en) * 2009-01-21 2009-03-04 Johnson Matthey Plc Sorbents
PL218635B1 (pl) 2009-01-26 2015-01-30 Innowacyjne Przedsiębiorstwo Wielobranżowe Polin Spółka Z Ograniczoną Odpowi Sposób usuwania ze spalin tlenków azotu i rtęci
US20120135214A1 (en) * 2010-11-30 2012-05-31 Steven Bruce Dawes Sorbent For Removal Of A Contaminant From A Fluid

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3181213A1 (en) 2015-12-14 2017-06-21 PGE Górnictwo | Energetyka Konwencjonalna S.A. Mercury capture system from flue gases generated in a power process of coal burning

Also Published As

Publication number Publication date
ES2665749T3 (es) 2018-04-27
EP2916930B1 (en) 2018-01-31
US9636623B2 (en) 2017-05-02
US20150283496A1 (en) 2015-10-08
EP2916930A1 (en) 2015-09-16
WO2014073996A1 (en) 2014-05-15
PL229084B1 (pl) 2018-06-29

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