PL414510A1 - Bifunctional difenoconazole ionic liquid, method for obtaining them and application as the compounds with fungicidal and herbicidal actions - Google Patents

Bifunctional difenoconazole ionic liquid, method for obtaining them and application as the compounds with fungicidal and herbicidal actions

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Publication number
PL414510A1
PL414510A1 PL414510A PL41451015A PL414510A1 PL 414510 A1 PL414510 A1 PL 414510A1 PL 414510 A PL414510 A PL 414510A PL 41451015 A PL41451015 A PL 41451015A PL 414510 A1 PL414510 A1 PL 414510A1
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PL
Poland
Prior art keywords
diphenoconazole
application
acetic
bifunctional
difenoconazole
Prior art date
Application number
PL414510A
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Polish (pl)
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PL237289B1 (en
Inventor
Juliusz Pernak
Mariusz Kot
Agnieszka Biedziak
Katarzyna Kurkowiak
Tadeusz Praczyk
Original Assignee
Instytut Ochrony Roślin - Państwowy Instytut Badawczy
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Application filed by Instytut Ochrony Roślin - Państwowy Instytut Badawczy filed Critical Instytut Ochrony Roślin - Państwowy Instytut Badawczy
Priority to PL414510A priority Critical patent/PL237289B1/en
Publication of PL414510A1 publication Critical patent/PL414510A1/en
Publication of PL237289B1 publication Critical patent/PL237289B1/en

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Abstract

Przedmiotem zgłoszenia są dwufunkcyjne ciecze jonowe difenokonazolu oraz sposób ich otrzymywania. Dwufunkcyjne ciecze jonowe difenokonazolu przedstawia wzór ogólny 1, w którym A- oznacza: anion herbicydowy (4-chloro-2-metylofenoksy)octowy lub 2,4-dichlorofenoksy)octowy. Sposób polega na tym, że difenokonazol o wzorze ogólnym 2, rozpuszcza się w alkoholu alifatycznym o długości łańcucha węglowego od jednego do czterech atomów węgla lub ich mieszaninie, korzystnie w metanolu, dalej miesza się z alkoholowym roztworem kwasu (4-chloro-2-metylofenoksy)octowego lub (2,4-dichlorofenoksy)octowego o stężeniu co najmniej 1%, w stosunku molowym difenokonazolu do kwasu organicznego od 1 : 1 do 1 : 1,1, korzystnie 1 : 1, w temperaturze poniżej 100°C, korzystnie w 50°C, w czasie co najmniej 40 minut, po czym rozpuszczalnik usuwa się. Zgłoszenie dotyczy też zastosowania dwufunkcyjnych cieczy jonowych difenokonazolu o wzorze ogólnym 1.The subject of the application are difunctional ionic liquids of diphenoconazole and the method of their preparation. The difunctional ionic liquids of diphenoconazole are represented by general formula 1, in which A- is: herbicidal (4-chloro-2-methylphenoxy) acetic or 2,4-dichlorophenoxy) acetic anion. The method consists in the fact that diphenoconazole of general formula 2 dissolves in an aliphatic alcohol with a carbon chain length of one to four carbon atoms or a mixture thereof, preferably in methanol, further mixed with an alcoholic acid solution (4-chloro-2-methylphenoxy) ) acetic or (2,4-dichlorophenoxy) acetic at a concentration of at least 1%, in a molar ratio of diphenoconazole to organic acid from 1: 1 to 1: 1.1, preferably 1: 1, at a temperature below 100 ° C, preferably at 50 ° C for at least 40 minutes, after which the solvent is removed. The application also relates to the use of bifunctional ionic liquids of diphenoconazole of general formula 1.

PL414510A 2015-10-26 2015-10-26 Bifunctional difenoconazole ionic liquid, method for obtaining them and application as the compounds with fungicidal and herbicidal actions PL237289B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PL414510A PL237289B1 (en) 2015-10-26 2015-10-26 Bifunctional difenoconazole ionic liquid, method for obtaining them and application as the compounds with fungicidal and herbicidal actions

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PL414510A PL237289B1 (en) 2015-10-26 2015-10-26 Bifunctional difenoconazole ionic liquid, method for obtaining them and application as the compounds with fungicidal and herbicidal actions

Publications (2)

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PL414510A1 true PL414510A1 (en) 2017-05-08
PL237289B1 PL237289B1 (en) 2021-04-06

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