SU466681A3 - Способ получени карбаматных производных кетоксимов - Google Patents
Способ получени карбаматных производных кетоксимовInfo
- Publication number
- SU466681A3 SU466681A3 SU1887327A SU1887327A SU466681A3 SU 466681 A3 SU466681 A3 SU 466681A3 SU 1887327 A SU1887327 A SU 1887327A SU 1887327 A SU1887327 A SU 1887327A SU 466681 A3 SU466681 A3 SU 466681A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- lower alkyl
- general formula
- dimethyl
- preparing carbamate
- derivatives
- Prior art date
Links
- 238000000034 method Methods 0.000 title description 8
- KXDHJXZQYSOELW-UHFFFAOYSA-M Carbamate Chemical compound NC([O-])=O KXDHJXZQYSOELW-UHFFFAOYSA-M 0.000 title description 3
- 125000000217 alkyl group Chemical group 0.000 description 10
- 150000001875 compounds Chemical class 0.000 description 9
- 229910052739 hydrogen Inorganic materials 0.000 description 7
- 150000002431 hydrogen Chemical class 0.000 description 7
- 239000001257 hydrogen Substances 0.000 description 7
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 5
- 125000003342 alkenyl group Chemical group 0.000 description 5
- 239000000203 mixture Substances 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- RWRDLPDLKQPQOW-UHFFFAOYSA-N Pyrrolidine Chemical compound C1CCNC1 RWRDLPDLKQPQOW-UHFFFAOYSA-N 0.000 description 3
- 125000000304 alkynyl group Chemical group 0.000 description 3
- 229910052736 halogen Inorganic materials 0.000 description 3
- 150000002367 halogens Chemical class 0.000 description 3
- 125000000623 heterocyclic group Chemical group 0.000 description 3
- 238000002955 isolation Methods 0.000 description 3
- 238000002360 preparation method Methods 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- -1 1-bromo-3,3-dimethyl-2-methylcarbamyloxy-aminobutane Chemical compound 0.000 description 2
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- WTDHULULXKLSOZ-UHFFFAOYSA-N Hydroxylamine hydrochloride Chemical compound Cl.ON WTDHULULXKLSOZ-UHFFFAOYSA-N 0.000 description 2
- 125000002252 acyl group Chemical group 0.000 description 2
- 125000003917 carbamoyl group Chemical group [H]N([H])C(*)=O 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- VWDWKYIASSYTQR-UHFFFAOYSA-N sodium nitrate Chemical compound [Na+].[O-][N+]([O-])=O VWDWKYIASSYTQR-UHFFFAOYSA-N 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- SAIRZMWXVJEBMO-UHFFFAOYSA-N 1-bromo-3,3-dimethylbutan-2-one Chemical compound CC(C)(C)C(=O)CBr SAIRZMWXVJEBMO-UHFFFAOYSA-N 0.000 description 1
- WCXXISMIJBRDQK-UHFFFAOYSA-N 1-methylsulfanylbutane Chemical compound CCCCSC WCXXISMIJBRDQK-UHFFFAOYSA-N 0.000 description 1
- KBYOXSZORPCSGZ-UHFFFAOYSA-N 2-(n-hydroxy-c-pyrrolidin-1-ylcarbonimidoyl)-n,3,3-trimethylbutanamide Chemical compound CNC(=O)C(C(C)(C)C)C(=NO)N1CCCC1 KBYOXSZORPCSGZ-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 230000004071 biological effect Effects 0.000 description 1
- 150000004657 carbamic acid derivatives Chemical class 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 239000005457 ice water Substances 0.000 description 1
- ZBQVPNUHRRVWDF-UHFFFAOYSA-N n-(1-bromo-3,3-dimethylbutan-2-ylidene)hydroxylamine Chemical compound CC(C)(C)C(CBr)=NO ZBQVPNUHRRVWDF-UHFFFAOYSA-N 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- IBBLRJGOOANPTQ-JKVLGAQCSA-N quinapril hydrochloride Chemical compound Cl.C([C@@H](C(=O)OCC)N[C@@H](C)C(=O)N1[C@@H](CC2=CC=CC=C2C1)C(O)=O)CC1=CC=CC=C1 IBBLRJGOOANPTQ-JKVLGAQCSA-N 0.000 description 1
- 238000001953 recrystallisation Methods 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 235000010344 sodium nitrate Nutrition 0.000 description 1
- 239000004317 sodium nitrate Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000003039 volatile agent Substances 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
- C07D295/04—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms
- C07D295/12—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly or doubly bound nitrogen atoms
- C07D295/125—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly or doubly bound nitrogen atoms with the ring nitrogen atoms and the substituent nitrogen atoms attached to the same carbon chain, which is not interrupted by carbocyclic rings
- C07D295/13—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly or doubly bound nitrogen atoms with the ring nitrogen atoms and the substituent nitrogen atoms attached to the same carbon chain, which is not interrupted by carbocyclic rings to an acyclic saturated chain
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C321/00—Thiols, sulfides, hydropolysulfides or polysulfides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C323/00—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D333/00—Heterocyclic compounds containing five-membered rings having one sulfur atom as the only ring hetero atom
- C07D333/02—Heterocyclic compounds containing five-membered rings having one sulfur atom as the only ring hetero atom not condensed with other rings
- C07D333/04—Heterocyclic compounds containing five-membered rings having one sulfur atom as the only ring hetero atom not condensed with other rings not substituted on the ring sulphur atom
- C07D333/06—Heterocyclic compounds containing five-membered rings having one sulfur atom as the only ring hetero atom not condensed with other rings not substituted on the ring sulphur atom with only hydrogen atoms, hydrocarbon or substituted hydrocarbon radicals, directly attached to the ring carbon atoms
- C07D333/14—Radicals substituted by singly bound hetero atoms other than halogen
- C07D333/18—Radicals substituted by singly bound hetero atoms other than halogen by sulfur atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
- Heterocyclic Compounds Containing Sulfur Atoms (AREA)
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US13258471A | 1971-04-08 | 1971-04-08 | |
| US229207A US3875232A (en) | 1971-04-08 | 1972-02-24 | AC Ketoxime carbamates |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU466681A3 true SU466681A3 (ru) | 1975-04-05 |
Family
ID=26830521
Family Applications (3)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU1887327A SU466681A3 (ru) | 1971-04-08 | 1972-04-07 | Способ получени карбаматных производных кетоксимов |
| SU1769624A SU454735A3 (ru) | 1971-04-08 | 1972-04-07 | Способ получени карбаматных производных кетоксимов |
| SU1886513A SU466653A3 (ru) | 1971-04-08 | 1972-04-07 | Способ получени карбаматных производных кетоксимов |
Family Applications After (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU1769624A SU454735A3 (ru) | 1971-04-08 | 1972-04-07 | Способ получени карбаматных производных кетоксимов |
| SU1886513A SU466653A3 (ru) | 1971-04-08 | 1972-04-07 | Способ получени карбаматных производных кетоксимов |
Country Status (20)
| Country | Link |
|---|---|
| US (1) | US3875232A (2) |
| JP (1) | JPS5533410B1 (2) |
| AR (1) | AR192758A1 (2) |
| BE (1) | BE830594Q (2) |
| CA (1) | CA984399A (2) |
| CH (3) | CH585194A5 (2) |
| DE (1) | DE2216838C2 (2) |
| EG (1) | EG10912A (2) |
| ES (1) | ES401551A1 (2) |
| FR (1) | FR2136055A5 (2) |
| GB (1) | GB1392111A (2) |
| HU (1) | HU165184B (2) |
| IE (1) | IE36264B1 (2) |
| IL (1) | IL39157A (2) |
| IT (1) | IT954413B (2) |
| NL (1) | NL175989C (2) |
| PL (1) | PL89001B1 (2) |
| RO (3) | RO72827A (2) |
| SU (3) | SU466681A3 (2) |
| YU (3) | YU39065B (2) |
Families Citing this family (29)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4215075A (en) * | 1971-04-08 | 1980-07-29 | Diamond Shamrock Corporation | Ketoxime carbamates |
| US3932471A (en) * | 1972-02-24 | 1976-01-13 | Diamond Shamrock Corporation | Azide |
| DE2408522A1 (de) * | 1974-02-22 | 1975-09-04 | Boehringer Mannheim Gmbh | Aminderivate der azidophenole und verfahren zu ihrer herstellung |
| US3932508A (en) | 1974-04-26 | 1976-01-13 | Minnesota Mining And Manufacturing Company | Polyfluoromethylthio-substituted compounds |
| US4029688A (en) * | 1974-06-27 | 1977-06-14 | Union Carbide Corporation | Carbamic pesticidal compositions |
| US4018894A (en) * | 1975-01-20 | 1977-04-19 | Stauffer Chemical Company | Oxime carbonetes as fungicidal or bactericidal agents |
| US3988357A (en) * | 1975-01-20 | 1976-10-26 | Stauffer Chemical Company | Certain oxime carbonates |
| US4009179A (en) * | 1975-10-15 | 1977-02-22 | E. I. Du Pont De Nemours And Company | Di- and tri-substituted oxazolidin-2-one oximes |
| DE2621102A1 (de) | 1976-05-10 | 1977-11-24 | Schering Ag | Propan-1,2-diondioxime, schaedlingsbekaempfungsmittel enthaltend diese verbindungen sowie verfahren zu ihrer herstellung |
| US4073930A (en) * | 1976-06-01 | 1978-02-14 | Union Carbide Corporation | Carbamoyloximes and oximes and insecticidal and miticidal compositions and methods employing them |
| US4072750A (en) * | 1976-06-01 | 1978-02-07 | Union Carbide Corporation | 1,3,5-Trithiane and 1,3,5-oxadithiane carbamoyloxime compounds and insecticidal and miticidal compositions and methods employing them |
| US4454134A (en) * | 1976-06-14 | 1984-06-12 | Union Carbide Corporation | Amide carbamates and amide oxime compounds |
| DE2631522A1 (de) * | 1976-07-14 | 1978-01-19 | Bayer Ag | Oximcarbamate fluorierter ketone, verfahren zu ihrer herstellung und ihre verwendung als insektizide, akarizide und nematizide |
| US4045491A (en) * | 1976-10-07 | 1977-08-30 | International Flavors & Fragrances Inc. | α-Oxy(oxo) sulfides and ethers |
| DE2828133A1 (de) * | 1978-06-27 | 1980-01-10 | Bayer Ag | N-sulfenylierte carbamoyloximino-1- methylthio-butane, verfahren zu ihrer herstellung und ihre verwendung als insektizide |
| CA1126278A (en) * | 1978-11-09 | 1982-06-22 | Paul Winternitz | Carbamoyloximes |
| US4264528A (en) * | 1978-12-04 | 1981-04-28 | Diamond Shamrock Corporation | Method of preparing ketoxime carbamates |
| US4234514A (en) * | 1978-12-04 | 1980-11-18 | Diamond Shamrock Corporation | Method of preparing ketoxime carbamates |
| DE2933600A1 (de) * | 1979-08-18 | 1981-04-09 | Bayer Ag, 5090 Leverkusen | Substituierte 2-carbamoyloximinobutane, verfahren zu ihrer herstellung und ihre verwendung als schaedlingsbekaempfungsmittel |
| DE3125920A1 (de) | 1981-07-01 | 1983-01-20 | Basf Ag, 6700 Ludwigshafen | "verfahren zur herstellung von sulfiden" |
| US4387053A (en) * | 1981-11-23 | 1983-06-07 | Diamond Shamrock Corporation | Stabilization of oxime carbamates with gallic acid, lower alkyl ester derivatives thereof |
| DE3204788A1 (de) * | 1982-02-11 | 1983-08-18 | Bayer Ag, 5090 Leverkusen | Verfahren zur herstellung von 5-substituierten 1-chlor-3,3-dimethylpentan-2-onen |
| US4640927A (en) * | 1984-03-30 | 1987-02-03 | Uniroyal Chemical Company, Inc. | Substituted oxime carbamates |
| US4785108A (en) * | 1984-06-04 | 1988-11-15 | Uniroyal Chemical Company, Inc. | Substituted oxime carbamates |
| US5200427A (en) * | 1984-07-27 | 1993-04-06 | The Board Of Trustees Of The Univ. Of Illinois | Porphyric insecticides |
| GB2173499A (en) * | 1985-02-04 | 1986-10-15 | Ici Plc | Fungicidal dithiolopyrrolones |
| US7842727B2 (en) * | 2001-03-27 | 2010-11-30 | Errant Gene Therapeutics, Llc | Histone deacetylase inhibitors |
| US7214831B2 (en) * | 2002-05-22 | 2007-05-08 | Errant Gene Therapeutics, Llc | Histone deacetylase inhibitors based on alpha-chalcogenmethylcarbonyl compounds |
| EP1511477A4 (en) * | 2002-05-22 | 2008-04-09 | Errant Gene Therapeutics Llc | HISTONE DEACETYLASE INHIBITORS BASED ON ALPHA-KETO-EPOXYDE COMPOUNDS |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA846786A (en) * | 1970-07-14 | R. Baker Don. | Use of certain oxime esters in controlling fungi upon cellulosic materials | |
| NL106827C (2) * | 1957-01-21 | |||
| BE637723A (2) * | 1962-09-25 | |||
| US3400153A (en) * | 1964-09-23 | 1968-09-03 | Union Carbide Corp | Nitroalkyl carbamoyloximes |
| US3454642A (en) * | 1966-12-22 | 1969-07-08 | Upjohn Co | Alkyl 2-methylpropenyl ketoxime carbamates |
| GB1214077A (en) * | 1967-11-02 | 1970-12-02 | Usv Pharma Corp | Oximes and their carbamoyl esters and the methods of preparation thereof |
| NL6912150A (2) * | 1968-08-19 | 1970-02-23 | ||
| US3681386A (en) * | 1969-11-06 | 1972-08-01 | Minnesota Mining & Mfg | Substituted alkanal oximes |
| CH536286A (de) * | 1970-03-23 | 1973-04-30 | Agripat Sa | Verfahren zur Herstellung von neuen Carbamoyl-oximen |
| US3647861A (en) * | 1970-08-25 | 1972-03-07 | Du Pont | Substituted o-carbamylhydroxamates |
-
1972
- 1972-02-24 US US229207A patent/US3875232A/en not_active Expired - Lifetime
- 1972-03-17 CA CA137,337A patent/CA984399A/en not_active Expired
- 1972-03-27 FR FR7210622A patent/FR2136055A5/fr not_active Expired
- 1972-04-05 AR AR241311A patent/AR192758A1/es active
- 1972-04-06 EG EG138/72A patent/EG10912A/xx active
- 1972-04-07 IL IL39157A patent/IL39157A/en unknown
- 1972-04-07 RO RO7282519A patent/RO72827A/ro unknown
- 1972-04-07 CH CH436875A patent/CH585194A5/xx not_active IP Right Cessation
- 1972-04-07 SU SU1887327A patent/SU466681A3/ru active
- 1972-04-07 HU HUDI222A patent/HU165184B/hu unknown
- 1972-04-07 IE IE453/72A patent/IE36264B1/xx unknown
- 1972-04-07 JP JP3563572A patent/JPS5533410B1/ja active Pending
- 1972-04-07 DE DE2216838A patent/DE2216838C2/de not_active Expired
- 1972-04-07 RO RO7282518A patent/RO72853A/ro unknown
- 1972-04-07 ES ES401551A patent/ES401551A1/es not_active Expired
- 1972-04-07 SU SU1769624A patent/SU454735A3/ru active
- 1972-04-07 YU YU00944/72A patent/YU39065B/xx unknown
- 1972-04-07 RO RO70445A patent/RO61151A/ro unknown
- 1972-04-07 PL PL1972154659A patent/PL89001B1/pl unknown
- 1972-04-07 IT IT49465/72A patent/IT954413B/it active
- 1972-04-07 CH CH514972A patent/CH611275A5/xx not_active IP Right Cessation
- 1972-04-07 CH CH436975A patent/CH591433A5/xx not_active IP Right Cessation
- 1972-04-07 GB GB1618772A patent/GB1392111A/en not_active Expired
- 1972-04-07 SU SU1886513A patent/SU466653A3/ru active
- 1972-04-07 NL NLAANVRAGE7204698,A patent/NL175989C/xx not_active IP Right Cessation
-
1975
- 1975-06-24 BE BE157643A patent/BE830594Q/xx not_active IP Right Cessation
-
1979
- 1979-02-12 YU YU316/79A patent/YU42298B/xx unknown
- 1979-02-12 YU YU00315/79A patent/YU39102B/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| BE830594Q (fr) | 1975-10-16 |
| YU39102B (en) | 1984-04-30 |
| FR2136055A5 (2) | 1972-12-22 |
| EG10912A (en) | 1976-12-31 |
| RO61151A (2) | 1976-10-15 |
| NL175989C (nl) | 1985-02-01 |
| CH591433A5 (2) | 1977-09-15 |
| PL89001B1 (en) | 1976-10-30 |
| YU42298B (en) | 1988-08-31 |
| CA984399A (en) | 1976-02-24 |
| IE36264L (en) | 1972-10-08 |
| IL39157A0 (en) | 1972-06-28 |
| IT954413B (it) | 1973-08-30 |
| DE2216838A1 (de) | 1972-11-02 |
| ES401551A1 (es) | 1975-10-01 |
| NL175989B (nl) | 1984-09-03 |
| YU94472A (en) | 1982-05-31 |
| IE36264B1 (en) | 1976-09-29 |
| CH585194A5 (2) | 1977-02-28 |
| YU31679A (en) | 1982-05-31 |
| SU466653A3 (ru) | 1975-04-05 |
| YU31579A (en) | 1982-06-30 |
| AR192758A1 (es) | 1973-03-14 |
| HU165184B (2) | 1974-07-27 |
| DE2216838C2 (de) | 1985-05-09 |
| US3875232A (en) | 1975-04-01 |
| RO72853A (ro) | 1982-02-26 |
| CH611275A5 (2) | 1979-05-31 |
| SU454735A3 (ru) | 1974-12-25 |
| JPS5533410B1 (2) | 1980-08-30 |
| YU39065B (en) | 1984-04-30 |
| RO72827A (ro) | 1982-10-11 |
| NL7204698A (2) | 1972-10-10 |
| GB1392111A (en) | 1975-04-30 |
| IL39157A (en) | 1976-08-31 |
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