TW389741B - Hydrogen cyanide process and apparatus therefor - Google Patents

Hydrogen cyanide process and apparatus therefor Download PDF

Info

Publication number
TW389741B
TW389741B TW085110881A TW85110881A TW389741B TW 389741 B TW389741 B TW 389741B TW 085110881 A TW085110881 A TW 085110881A TW 85110881 A TW85110881 A TW 85110881A TW 389741 B TW389741 B TW 389741B
Authority
TW
Taiwan
Prior art keywords
stream
oxidant
mixture
patent application
mixing
Prior art date
Application number
TW085110881A
Other languages
English (en)
Chinese (zh)
Inventor
Christopher Cowell
Ralph Doy
Original Assignee
Ici Plc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ici Plc filed Critical Ici Plc
Application granted granted Critical
Publication of TW389741B publication Critical patent/TW389741B/zh

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01CAMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C3/00Cyanogen; Compounds thereof
    • C01C3/02Preparation, separation or purification of hydrogen cyanide
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01CAMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C3/00Cyanogen; Compounds thereof
    • C01C3/02Preparation, separation or purification of hydrogen cyanide
    • C01C3/0208Preparation in gaseous phase
    • C01C3/0212Preparation in gaseous phase from hydrocarbons and ammonia in the presence of oxygen, e.g. the Andrussow-process
    • C01C3/022Apparatus therefor
    • C01C3/0225Apparatus therefor characterised by the synthesis reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006Controlling or regulating processes
    • B01J19/002Avoiding undesirable reactions or side-effects, e.g. avoiding explosions, or improving the yield by suppressing side-reactions
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • B01J19/2415Tubular reactors
    • B01J19/2425Tubular reactors in parallel
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/0285Heating or cooling the reactor
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01CAMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C3/00Cyanogen; Compounds thereof
    • C01C3/02Preparation, separation or purification of hydrogen cyanide
    • C01C3/0208Preparation in gaseous phase
    • C01C3/0212Preparation in gaseous phase from hydrocarbons and ammonia in the presence of oxygen, e.g. the Andrussow-process
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00076Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
    • B01J2219/00081Tubes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00159Controlling the temperature controlling multiple zones along the direction of flow, e.g. pre-heating and after-cooling

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
  • Hydrogen, Water And Hydrids (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Exhaust Gas Treatment By Means Of Catalyst (AREA)
TW085110881A 1995-09-01 1996-09-05 Hydrogen cyanide process and apparatus therefor TW389741B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
EP95113796 1995-09-01

Publications (1)

Publication Number Publication Date
TW389741B true TW389741B (en) 2000-05-11

Family

ID=8219571

Family Applications (1)

Application Number Title Priority Date Filing Date
TW085110881A TW389741B (en) 1995-09-01 1996-09-05 Hydrogen cyanide process and apparatus therefor

Country Status (13)

Country Link
US (2) US6491876B2 (2)
EP (1) EP0847372B1 (2)
JP (1) JP3889442B2 (2)
KR (1) KR100411692B1 (2)
CN (1) CN1095806C (2)
AT (1) ATE202541T1 (2)
AU (1) AU702825C (2)
BR (1) BR9610149A (2)
CA (1) CA2230017C (2)
DE (1) DE69613581T2 (2)
ES (1) ES2158339T3 (2)
TW (1) TW389741B (2)
WO (1) WO1997009273A1 (2)

Families Citing this family (27)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0847372B1 (en) * 1995-09-01 2001-06-27 Ineos Acrylics UK Limited Hydrogen cyanide process and apparatus therefor
DE19754988A1 (de) * 1997-12-11 1999-06-17 Degussa Herstellung von Blausäure nach dem Andrussow-Verfahren
DE19810484A1 (de) * 1998-03-11 1999-09-16 Degussa Verfahren zur Herstellung von Blausäure
US6221327B1 (en) 1998-05-15 2001-04-24 Rohm And Haas Company Catalyst system using flow-through radiation shielding and a process for producing hydrogen cyanide using the same
AU4090600A (en) * 1999-06-30 2001-01-04 Rohm And Haas Company High performance heat exchangers
US6649137B2 (en) * 2000-05-23 2003-11-18 Rohm And Haas Company Apparatus with improved safety features for high temperature industrial processes
DE10034193A1 (de) 2000-07-13 2002-03-28 Roehm Gmbh Verfahren zur Herstellung von Cyanwasserstoff
DE10034194A1 (de) 2000-07-13 2003-09-11 Roehm Gmbh Verfahren zur Herstellung von Cyanwasserstoff
EP1604947A1 (en) * 2004-06-07 2005-12-14 ETH Zürich Process and apparatus for producing hydrogen or ammonia
DE102007014586A1 (de) * 2007-03-23 2008-09-25 Evonik Röhm Gmbh Verfahren zur Herstellung von Cyanwasserstoff (HCN)
DE102007034715A1 (de) * 2007-07-23 2009-01-29 Evonik Röhm Gmbh Reaktor zur Herstellung von Cyanwasserstoff nach dem Andrussow-Verfahren
TWI390145B (zh) * 2008-03-31 2013-03-21 Rohm & Haas 用於爆燃壓力衰減之方法及設備
JP2016502969A (ja) 2012-12-18 2016-02-01 インヴィスタ テクノロジーズ エスアエルエル シアン化水素の生成および水素の回収プロセス
TWI519479B (zh) 2012-12-18 2016-02-01 英威達技術有限公司 利用轉化器製造氰化氫之方法
CN103864106B (zh) * 2012-12-18 2021-11-26 英威达纺织(英国)有限公司 安德卢梭法中氨比例的变化
TW201425277A (zh) * 2012-12-18 2014-07-01 Invista Tech Sarl 製造二胺之整合製程
CN103864109A (zh) * 2012-12-18 2014-06-18 因温斯特技术公司 用于安德卢梭法中的再循环的系统和方法
WO2014099607A1 (en) 2012-12-18 2014-06-26 Invista Technologies S.A. R. L. Integrated process for hexamethylenediamine production
TWI519480B (zh) * 2012-12-18 2016-02-01 英威達技術有限公司 使用整流器之製造氰化氫的方法
EP2935115A1 (en) * 2012-12-18 2015-10-28 Invista Technologies S.à.r.l. Operational controls for inert gas blanketing for andrussow process
US20160046498A1 (en) * 2012-12-18 2016-02-18 Invista North America S.A R.L. Process for stabilizing heat exchanger tubes in andrussow process
US20150352481A1 (en) * 2012-12-18 2015-12-10 Invista North America S.A R.L. Apparatus and method for hydrogen recovery in an andrussow process
WO2015006548A1 (en) * 2013-07-12 2015-01-15 Invista Technologies S.A R.L. Hydrogen cyanide manufacturing process with second waste heat boiler
FR3008692B1 (fr) * 2013-07-19 2016-12-23 Arkema France Installation et procede pour la preparation de cyanure d'hydrogene
FR3008626B1 (fr) * 2013-07-19 2015-08-07 Arkema France Reacteur pour preparer du cyanure d'hydrogene par le procede d'andrussow, equipement comprenant ledit reacteur et procede utilisant un tel equipement
US10323888B2 (en) * 2016-04-18 2019-06-18 Corrosion Monitoring Service Inc. System and method for installing external corrosion guards
CN120268332A (zh) * 2024-01-05 2025-07-08 中国天辰工程有限公司 一种制备氰化氢的反应器

Family Cites Families (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1934838A (en) 1930-04-14 1933-11-14 Ig Farbenindustrie Ag Production of hydrocyanic acid
DE1005049B (de) 1951-12-06 1957-03-28 Goodrich Co B F Verfahren zur Erzeugung von Cyanwasserstoff
US2803522A (en) * 1953-04-15 1957-08-20 Du Pont Manufacture of hydrogen cyanide
US3112177A (en) * 1959-11-11 1963-11-26 Toyo Koatsu Ind Inc Method of separating ammonia from hydrogen cyanide
US3104945A (en) * 1961-07-19 1963-09-24 Du Pont Method of producing hydrogen cyanide
DE1161870B (de) 1961-09-19 1964-01-30 Hans J Zimmer Verfahrenstechni Verfahren zur Herstellung von Cyanwasserstoff
US3215495A (en) 1962-01-23 1965-11-02 Du Pont Apparatus and process for preparing hydrogen cyanide
DE1190445B (de) 1962-09-29 1965-04-08 Hans J Zimmer Verfahrenstechni Verfahren zur Herstellung von Cyanwasserstoff und Nitrilen
NL6604519A (2) * 1965-04-14 1966-10-17
US3376500A (en) 1966-04-25 1968-04-02 Varian Associates Direct reading magnetic field intensity indicating apparatus
US4107278A (en) 1976-08-16 1978-08-15 E. I. Du Pont De Nemours And Company Process for making HCN
US4128622A (en) 1976-08-27 1978-12-05 E. I. Du Pont De Nemours And Company Process for producing hydrogen cyanide
PL109343B1 (en) 1978-06-19 1981-11-30 Politechnika Wroclawska Method of producing hydrogen cyanide
US5266291A (en) * 1992-05-05 1993-11-30 Praxair Technology, Inc. Packed bed arrangement for oxidation reaction system
US5360603A (en) * 1993-08-23 1994-11-01 Praxair Technology, Inc. Packed bed arrangement useful for mixing and/or oxidation
EP0847372B1 (en) * 1995-09-01 2001-06-27 Ineos Acrylics UK Limited Hydrogen cyanide process and apparatus therefor

Also Published As

Publication number Publication date
AU6879996A (en) 1997-03-27
EP0847372B1 (en) 2001-06-27
DE69613581D1 (de) 2001-08-02
AU702825C (en) 2002-09-19
CN1200102A (zh) 1998-11-25
US20020039553A1 (en) 2002-04-04
BR9610149A (pt) 1999-02-02
CA2230017A1 (en) 1997-03-13
ATE202541T1 (de) 2001-07-15
WO1997009273A1 (en) 1997-03-13
JPH11512070A (ja) 1999-10-19
JP3889442B2 (ja) 2007-03-07
US6491876B2 (en) 2002-12-10
US20020182137A1 (en) 2002-12-05
ES2158339T3 (es) 2001-09-01
US6656442B2 (en) 2003-12-02
EP0847372A1 (en) 1998-06-17
MX9801546A (es) 1998-05-31
CN1095806C (zh) 2002-12-11
DE69613581T2 (de) 2002-04-25
KR19990044326A (ko) 1999-06-25
CA2230017C (en) 2006-06-20
KR100411692B1 (ko) 2004-02-18
AU702825B2 (en) 1999-03-04

Similar Documents

Publication Publication Date Title
TW389741B (en) Hydrogen cyanide process and apparatus therefor
US6524356B2 (en) Method and apparatus for producing reformed gases
US5980596A (en) Multi-injector autothermal reforming process and apparatus for producing synthesis gas (law 565).
EP2299090A2 (en) Combustion turbine system with integrated ion transport membrane
US6267912B1 (en) Distributed injection catalytic partial oxidation process and apparatus for producing synthesis gas
US5785774A (en) Process for producing heat treatment atmospheres
CN105879786B (zh) 用于催化气相反应的装置和方法以及其用途
CN108862194A (zh) 用于生产合成气的燃烧器和方法
JPS63282410A (ja) 触媒式燃焼による高温加圧ガス流の生成方法
EP2492358B1 (en) Method and apparatus for heating a blast furnace stove
US6244860B1 (en) Apparatus and process for producing perlite
JPH09508346A (ja) N▲下2▼oからのnoの製造
US10850242B2 (en) Two stage gas-gas mixer
US4230278A (en) Apparatus for reducing hydrocarbon fuel requirement for Haber ammonia synthesis
EP1136443A1 (en) Gas and oxygen reactor and method for the production of reducing elements
KR20090111775A (ko) 고상 연료 연소 방법 및 고상 연료 연소용 장치
MXPA98001546A (en) Procedure for hydrogen cyanide and apparatus
RU2841537C1 (ru) Способ получения конвертированного газа и топливно-кислородный реактор для его осуществления
JPS63176303A (ja) 炭化珪素粉末の製造方法
MXPA00002273A (es) Proceso reformador de refuerzo de oxigeno-combustible y aparato

Legal Events

Date Code Title Description
GD4A Issue of patent certificate for granted invention patent