TW588017B - Titanium-containing materials - Google Patents

Titanium-containing materials Download PDF

Info

Publication number: TW588017B
Authority: TW; Taiwan
Prior art keywords: preparing; solution; patent application; titanium; metal
Prior art date: 2000-07-17

Application number

TW090122226A

Other languages

English (en)

Chinese (zh)

Inventor

Najeh Al-Salim

Timothy Kemmitt

Original Assignee

Ind Res Ltd

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2000-07-17

Filing date

2001-09-07

Publication date

2004-05-21

2001-09-07 Application filed by Ind Res Ltd filed Critical Ind Res Ltd

2004-05-21 Application granted granted Critical

2004-05-21 Publication of TW588017B publication Critical patent/TW588017B/zh

Links

239000010936 titanium Substances 0.000 title claims abstract description 101
229910052719 titanium Inorganic materials 0.000 title claims abstract description 92
RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 title claims abstract description 83
239000000463 material Substances 0.000 title claims description 50
MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 claims abstract description 289
238000000034 method Methods 0.000 claims abstract description 111
235000006408 oxalic acid Nutrition 0.000 claims abstract description 93
150000001875 compounds Chemical class 0.000 claims abstract description 51
239000002245 particle Substances 0.000 claims abstract description 49
-1 titanium ions Chemical class 0.000 claims abstract description 23
239000012429 reaction media Substances 0.000 claims abstract description 13
GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 289
239000000243 solution Substances 0.000 claims description 138
229910052751 metal Inorganic materials 0.000 claims description 113
239000002184 metal Substances 0.000 claims description 113
239000002243 precursor Substances 0.000 claims description 91
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 81
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 76
239000010408 film Substances 0.000 claims description 74
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 70
239000011941 photocatalyst Substances 0.000 claims description 62
238000000576 coating method Methods 0.000 claims description 53
239000000047 product Substances 0.000 claims description 51
239000011248 coating agent Substances 0.000 claims description 49
239000000758 substrate Substances 0.000 claims description 49
239000000203 mixture Substances 0.000 claims description 48
239000004408 titanium dioxide Substances 0.000 claims description 48
230000005855 radiation Effects 0.000 claims description 33
238000010438 heat treatment Methods 0.000 claims description 29
229910052763 palladium Inorganic materials 0.000 claims description 28
229910052697 platinum Inorganic materials 0.000 claims description 28
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 27
239000002253 acid Substances 0.000 claims description 27
239000000377 silicon dioxide Substances 0.000 claims description 27
OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 claims description 27
238000006243 chemical reaction Methods 0.000 claims description 25
239000011521 glass Substances 0.000 claims description 22
239000002904 solvent Substances 0.000 claims description 21
239000000499 gel Substances 0.000 claims description 20
239000004094 surface-active agent Substances 0.000 claims description 20
KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 18
239000010949 copper Substances 0.000 claims description 18
238000001879 gelation Methods 0.000 claims description 18
238000009281 ultraviolet germicidal irradiation Methods 0.000 claims description 18
JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 claims description 16
BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 claims description 16
239000008187 granular material Substances 0.000 claims description 14
230000001699 photocatalysis Effects 0.000 claims description 14
150000003839 salts Chemical class 0.000 claims description 14
229910044991 metal oxide Inorganic materials 0.000 claims description 13
150000004706 metal oxides Chemical class 0.000 claims description 13
229910052709 silver Inorganic materials 0.000 claims description 13
239000000654 additive Substances 0.000 claims description 12
229910000077 silane Inorganic materials 0.000 claims description 12
SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical compound [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 claims description 12
238000003756 stirring Methods 0.000 claims description 12
229910052802 copper Inorganic materials 0.000 claims description 11
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 10
239000008119 colloidal silica Substances 0.000 claims description 10
229910052500 inorganic mineral Inorganic materials 0.000 claims description 9
239000011707 mineral Substances 0.000 claims description 9
238000002156 mixing Methods 0.000 claims description 9
239000002002 slurry Substances 0.000 claims description 9
OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 claims description 8
235000019253 formic acid Nutrition 0.000 claims description 8
239000004310 lactic acid Substances 0.000 claims description 8
235000014655 lactic acid Nutrition 0.000 claims description 8
239000011541 reaction mixture Substances 0.000 claims description 8
VXUYXOFXAQZZMF-UHFFFAOYSA-N titanium(IV) isopropoxide Chemical compound CC(C)O[Ti](OC(C)C)(OC(C)C)OC(C)C VXUYXOFXAQZZMF-UHFFFAOYSA-N 0.000 claims description 8
BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims description 7
PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 7
238000009835 boiling Methods 0.000 claims description 7
230000015556 catabolic process Effects 0.000 claims description 7
238000006731 degradation reaction Methods 0.000 claims description 7
239000000413 hydrolysate Substances 0.000 claims description 7
238000005470 impregnation Methods 0.000 claims description 7
WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 claims description 7
150000007524 organic acids Chemical class 0.000 claims description 7
229920000642 polymer Polymers 0.000 claims description 7
230000008569 process Effects 0.000 claims description 7
239000004753 textile Substances 0.000 claims description 7
FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 claims description 6
MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 6
MXRIRQGCELJRSN-UHFFFAOYSA-N O.O.O.[Al] Chemical compound O.O.O.[Al] MXRIRQGCELJRSN-UHFFFAOYSA-N 0.000 claims description 6
FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 claims description 6
125000000217 alkyl group Chemical group 0.000 claims description 6
235000015165 citric acid Nutrition 0.000 claims description 6
OPQARKPSCNTWTJ-UHFFFAOYSA-L copper(ii) acetate Chemical compound [Cu+2].CC([O-])=O.CC([O-])=O OPQARKPSCNTWTJ-UHFFFAOYSA-L 0.000 claims description 6
239000003365 glass fiber Substances 0.000 claims description 6
239000002923 metal particle Substances 0.000 claims description 6
238000012545 processing Methods 0.000 claims description 6
230000002829 reductive effect Effects 0.000 claims description 6
229910052710 silicon Inorganic materials 0.000 claims description 6
229910001961 silver nitrate Inorganic materials 0.000 claims description 6
230000006641 stabilisation Effects 0.000 claims description 6
238000011105 stabilization Methods 0.000 claims description 6
239000011975 tartaric acid Substances 0.000 claims description 6
235000002906 tartaric acid Nutrition 0.000 claims description 6
NWZSZGALRFJKBT-KNIFDHDWSA-N (2s)-2,6-diaminohexanoic acid;(2s)-2-hydroxybutanedioic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O.NCCCC[C@H](N)C(O)=O NWZSZGALRFJKBT-KNIFDHDWSA-N 0.000 claims description 5
XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 5
XTVVROIMIGLXTD-UHFFFAOYSA-N copper(II) nitrate Chemical compound [Cu+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O XTVVROIMIGLXTD-UHFFFAOYSA-N 0.000 claims description 5
IKDUDTNKRLTJSI-UHFFFAOYSA-N hydrazine monohydrate Substances O.NN IKDUDTNKRLTJSI-UHFFFAOYSA-N 0.000 claims description 5
230000001678 irradiating effect Effects 0.000 claims description 5
150000002576 ketones Chemical class 0.000 claims description 5
125000000962 organic group Chemical group 0.000 claims description 5
239000011368 organic material Substances 0.000 claims description 5
239000010703 silicon Substances 0.000 claims description 5
CQLFBEKRDQMJLZ-UHFFFAOYSA-M silver acetate Chemical compound [Ag+].CC([O-])=O CQLFBEKRDQMJLZ-UHFFFAOYSA-M 0.000 claims description 5
229940071536 silver acetate Drugs 0.000 claims description 5
DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 claims description 4
230000000996 additive effect Effects 0.000 claims description 4
239000004566 building material Substances 0.000 claims description 4
YHWCPXVTRSHPNY-UHFFFAOYSA-N butan-1-olate;titanium(4+) Chemical compound [Ti+4].CCCC[O-].CCCC[O-].CCCC[O-].CCCC[O-] YHWCPXVTRSHPNY-UHFFFAOYSA-N 0.000 claims description 4
229910052799 carbon Inorganic materials 0.000 claims description 4
239000000919 ceramic Substances 0.000 claims description 4
230000008859 change Effects 0.000 claims description 4
229910000365 copper sulfate Inorganic materials 0.000 claims description 4
ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 claims description 4
238000011161 development Methods 0.000 claims description 4
150000002894 organic compounds Chemical class 0.000 claims description 4
239000011241 protective layer Substances 0.000 claims description 4
239000010453 quartz Substances 0.000 claims description 4
150000004756 silanes Chemical class 0.000 claims description 4
230000009466 transformation Effects 0.000 claims description 4
239000002023 wood Substances 0.000 claims description 4
239000004698 Polyethylene Substances 0.000 claims description 3
239000003929 acidic solution Substances 0.000 claims description 3
DIZPMCHEQGEION-UHFFFAOYSA-H aluminium sulfate (anhydrous) Chemical compound [Al+3].[Al+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O DIZPMCHEQGEION-UHFFFAOYSA-H 0.000 claims description 3
BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical group N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 claims description 3
229910052921 ammonium sulfate Inorganic materials 0.000 claims description 3
235000011130 ammonium sulphate Nutrition 0.000 claims description 3
239000002585 base Substances 0.000 claims description 3
239000011449 brick Substances 0.000 claims description 3
239000004567 concrete Substances 0.000 claims description 3
238000010297 mechanical methods and process Methods 0.000 claims description 3
239000003960 organic solvent Substances 0.000 claims description 3
230000010355 oscillation Effects 0.000 claims description 3
229920000728 polyester Polymers 0.000 claims description 3
229920000573 polyethylene Polymers 0.000 claims description 3
238000005245 sintering Methods 0.000 claims description 3
239000003513 alkali Substances 0.000 claims description 2
230000000087 stabilizing effect Effects 0.000 claims description 2
230000007704 transition Effects 0.000 claims description 2
DKGAVHZHDRPRBM-UHFFFAOYSA-N Tert-Butanol Chemical compound CC(C)(C)O DKGAVHZHDRPRBM-UHFFFAOYSA-N 0.000 claims 1
239000003125 aqueous solvent Substances 0.000 claims 1
125000005843 halogen group Chemical group 0.000 claims 1
230000007062 hydrolysis Effects 0.000 claims 1
238000006460 hydrolysis reaction Methods 0.000 claims 1
125000004043 oxo group Chemical group O=* 0.000 claims 1
239000004575 stone Substances 0.000 claims 1
229910052861 titanite Inorganic materials 0.000 claims 1
230000003019 stabilising effect Effects 0.000 abstract 1
239000000084 colloidal system Substances 0.000 description 29
239000000843 powder Substances 0.000 description 23
239000004744 fabric Substances 0.000 description 22
238000002360 preparation method Methods 0.000 description 21
VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 15
239000005977 Ethylene Substances 0.000 description 15
YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 15
239000007789 gas Substances 0.000 description 15
IKHGUXGNUITLKF-UHFFFAOYSA-N Acetaldehyde Chemical compound CC=O IKHGUXGNUITLKF-UHFFFAOYSA-N 0.000 description 14
230000000694 effects Effects 0.000 description 14
239000003054 catalyst Substances 0.000 description 13
KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 11
238000001704 evaporation Methods 0.000 description 11
OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical compound NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 description 10
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 9
HZAXFHJVJLSVMW-UHFFFAOYSA-N 2-Aminoethan-1-ol Chemical compound NCCO HZAXFHJVJLSVMW-UHFFFAOYSA-N 0.000 description 8
QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 8
CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 8
239000008188 pellet Substances 0.000 description 7
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 6
LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 6
WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 6
ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 6
OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 6
239000002131 composite material Substances 0.000 description 6
239000013078 crystal Substances 0.000 description 6
239000011148 porous material Substances 0.000 description 6
LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 5
238000000354 decomposition reaction Methods 0.000 description 5
239000012528 membrane Substances 0.000 description 5
QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 5
229910052753 mercury Inorganic materials 0.000 description 5
238000000059 patterning Methods 0.000 description 5
235000012239 silicon dioxide Nutrition 0.000 description 5
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
QYOVMAREBTZLBT-KTKRTIGZSA-N CCCCCCCC\C=C/CCCCCCCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCO Chemical compound CCCCCCCC\C=C/CCCCCCCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCO QYOVMAREBTZLBT-KTKRTIGZSA-N 0.000 description 4
CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 4
238000005299 abrasion Methods 0.000 description 4
239000012670 alkaline solution Substances 0.000 description 4
125000003545 alkoxy group Chemical group 0.000 description 4
229910021529 ammonia Inorganic materials 0.000 description 4
WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 4
230000015572 biosynthetic process Effects 0.000 description 4
239000003344 environmental pollutant Substances 0.000 description 4
230000003301 hydrolyzing effect Effects 0.000 description 4
239000010410 layer Substances 0.000 description 4
238000004519 manufacturing process Methods 0.000 description 4
GEVPUGOOGXGPIO-UHFFFAOYSA-N oxalic acid;dihydrate Chemical compound O.O.OC(=O)C(O)=O GEVPUGOOGXGPIO-UHFFFAOYSA-N 0.000 description 4
238000001782 photodegradation Methods 0.000 description 4
231100000719 pollutant Toxicity 0.000 description 4
229920005862 polyol Polymers 0.000 description 4
150000003077 polyols Chemical class 0.000 description 4
229910000029 sodium carbonate Inorganic materials 0.000 description 4
238000001179 sorption measurement Methods 0.000 description 4
238000012360 testing method Methods 0.000 description 4
150000005622 tetraalkylammonium hydroxides Chemical class 0.000 description 4
229910000906 Bronze Inorganic materials 0.000 description 3
PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 3
GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 3
BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 3
LCKIEQZJEYYRIY-UHFFFAOYSA-N Titanium ion Chemical compound [Ti+4] LCKIEQZJEYYRIY-UHFFFAOYSA-N 0.000 description 3
238000002441 X-ray diffraction Methods 0.000 description 3
238000004458 analytical method Methods 0.000 description 3
239000010974 bronze Substances 0.000 description 3
229910052681 coesite Inorganic materials 0.000 description 3
KUNSUQLRTQLHQQ-UHFFFAOYSA-N copper tin Chemical compound [Cu].[Sn] KUNSUQLRTQLHQQ-UHFFFAOYSA-N 0.000 description 3
229910052906 cristobalite Inorganic materials 0.000 description 3
230000003247 decreasing effect Effects 0.000 description 3
150000002009 diols Chemical class 0.000 description 3
239000012153 distilled water Substances 0.000 description 3
238000004043 dyeing Methods 0.000 description 3
239000003349 gelling agent Substances 0.000 description 3
150000004820 halides Chemical class 0.000 description 3
238000002329 infrared spectrum Methods 0.000 description 3
229910017604 nitric acid Inorganic materials 0.000 description 3
238000001935 peptisation Methods 0.000 description 3
238000006303 photolysis reaction Methods 0.000 description 3
229920001983 poloxamer Polymers 0.000 description 3
ONQDVAFWWYYXHM-UHFFFAOYSA-M potassium lauryl sulfate Chemical compound [K+].CCCCCCCCCCCCOS([O-])(=O)=O ONQDVAFWWYYXHM-UHFFFAOYSA-M 0.000 description 3
238000000634 powder X-ray diffraction Methods 0.000 description 3
BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 3
230000035484 reaction time Effects 0.000 description 3
238000006722 reduction reaction Methods 0.000 description 3
238000001878 scanning electron micrograph Methods 0.000 description 3
239000004332 silver Substances 0.000 description 3
238000005507 spraying Methods 0.000 description 3
229910052682 stishovite Inorganic materials 0.000 description 3
239000010409 thin film Substances 0.000 description 3
229910052905 tridymite Inorganic materials 0.000 description 3
GPRLSGONYQIRFK-MNYXATJNSA-N triton Chemical class [3H+] GPRLSGONYQIRFK-MNYXATJNSA-N 0.000 description 3
229910052724 xenon Inorganic materials 0.000 description 3
FHNFHKCVQCLJFQ-UHFFFAOYSA-N xenon atom Chemical compound [Xe] FHNFHKCVQCLJFQ-UHFFFAOYSA-N 0.000 description 3
WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 2
JKXYOQDLERSFPT-UHFFFAOYSA-N 2-[2-[2-[2-[2-[2-[2-[2-[2-[2-[2-[2-[2-[2-[2-[2-[2-[2-[2-(2-octadecoxyethoxy)ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethanol Chemical compound CCCCCCCCCCCCCCCCCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCO JKXYOQDLERSFPT-UHFFFAOYSA-N 0.000 description 2
LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 2
QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 2
238000004438 BET method Methods 0.000 description 2
239000005711 Benzoic acid Substances 0.000 description 2
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical group [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
239000012691 Cu precursor Substances 0.000 description 2
KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 description 2
241000196324 Embryophyta Species 0.000 description 2
238000004566 IR spectroscopy Methods 0.000 description 2
239000005642 Oleic acid Substances 0.000 description 2
ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 2
239000002202 Polyethylene glycol Substances 0.000 description 2
239000004372 Polyvinyl alcohol Substances 0.000 description 2
QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 2
GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 description 2
235000011054 acetic acid Nutrition 0.000 description 2
125000001931 aliphatic group Chemical group 0.000 description 2
235000010233 benzoic acid Nutrition 0.000 description 2
229910002092 carbon dioxide Inorganic materials 0.000 description 2
125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 2
YCIMNLLNPGFGHC-UHFFFAOYSA-N catechol Chemical compound OC1=CC=CC=C1O YCIMNLLNPGFGHC-UHFFFAOYSA-N 0.000 description 2
239000003795 chemical substances by application Substances 0.000 description 2
230000001186 cumulative effect Effects 0.000 description 2
239000003599 detergent Substances 0.000 description 2
ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 description 2
238000003618 dip coating Methods 0.000 description 2
235000013399 edible fruits Nutrition 0.000 description 2
238000011067 equilibration Methods 0.000 description 2
230000008020 evaporation Effects 0.000 description 2
239000011152 fibreglass Substances 0.000 description 2
150000004676 glycans Chemical class 0.000 description 2
230000005660 hydrophilic surface Effects 0.000 description 2
125000002887 hydroxy group Chemical group [H]O* 0.000 description 2
238000011065 in-situ storage Methods 0.000 description 2
QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 2
239000007788 liquid Substances 0.000 description 2
VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 description 2
239000011976 maleic acid Substances 0.000 description 2
BJEPYKJPYRNKOW-UHFFFAOYSA-N malic acid Chemical compound OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 description 2
238000005259 measurement Methods 0.000 description 2
150000002736 metal compounds Chemical class 0.000 description 2
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Classifications

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- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
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- C04B35/46—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates
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- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3231—Refractory metal oxides, their mixed metal oxides, or oxide-forming salts thereof
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- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
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TW090122226A 2000-07-17 2001-09-07 Titanium-containing materials TW588017B (en)

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NZ505774A NZ505774A (en)	2000-07-17	2000-07-17	Oxalate stabilised titania solutions and coating compositions and catalysts formed therefrom

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EP (1)	EP1324950A4 (fr)
JP (1)	JP2004507421A (fr)
AU (2)	AU8271101A (fr)
CA (1)	CA2415951A1 (fr)
NZ (1)	NZ505774A (fr)
TW (1)	TW588017B (fr)
WO (1)	WO2002006159A1 (fr)

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2000
- 2000-07-17 NZ NZ505774A patent/NZ505774A/xx unknown
2001
- 2001-07-17 JP JP2002512067A patent/JP2004507421A/ja active Pending
- 2001-07-17 AU AU8271101A patent/AU8271101A/xx active Pending
- 2001-07-17 AU AU2001282711A patent/AU2001282711B2/en not_active Ceased
- 2001-07-17 EP EP01961449A patent/EP1324950A4/fr not_active Withdrawn
- 2001-07-17 US US10/312,577 patent/US20030167878A1/en not_active Abandoned
- 2001-07-17 WO PCT/NZ2001/000144 patent/WO2002006159A1/fr not_active Ceased
- 2001-07-17 CA CA002415951A patent/CA2415951A1/fr not_active Abandoned
- 2001-09-07 TW TW090122226A patent/TW588017B/zh not_active IP Right Cessation

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Publication number	Publication date
NZ505774A (en)	2002-12-20
WO2002006159A1 (fr)	2002-01-24
EP1324950A4 (fr)	2005-04-06
EP1324950A1 (fr)	2003-07-09
AU2001282711B2 (en)	2005-01-06
JP2004507421A (ja)	2004-03-11
CA2415951A1 (fr)	2002-01-24
US20030167878A1 (en)	2003-09-11
AU8271101A (en)	2002-01-30

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Date	Code	Title	Description
2007-07-11	MM4A	Annulment or lapse of patent due to non-payment of fees

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