CH408954A - Procédé de préparation d'un catalyseur - Google Patents

Procédé de préparation d'un catalyseur

Info

Publication number: CH408954A
Authority: CH; Switzerland
Prior art keywords: catalyst; platinum; solution; phenol; activated carbon
Prior art date: 1961-08-25

Application number

CH1007062A

Other languages

English (en)

French (fr)

Inventor

D Silber Alvin

L Russel Joseph

Original Assignee

Halcon International Inc

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1961-08-25

Filing date

1962-08-24

Publication date

1966-03-15

1962-08-24 Application filed by Halcon International Inc filed Critical Halcon International Inc

1966-03-15 Publication of CH408954A publication Critical patent/CH408954A/fr

Links

239000003054 catalyst Substances 0.000 title description 26
238000004519 manufacturing process Methods 0.000 title description 4
BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 claims description 31
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 24
229910052697 platinum Inorganic materials 0.000 claims description 15
238000000034 method Methods 0.000 claims description 8
238000010992 reflux Methods 0.000 claims description 7
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
239000000203 mixture Substances 0.000 claims description 4
150000003058 platinum compounds Chemical class 0.000 claims description 4
239000007858 starting material Substances 0.000 claims description 4
QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 2
XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 claims description 2
238000006213 oxygenation reaction Methods 0.000 claims description 2
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims 2
JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 description 17
ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 14
HPXRVTGHNJAIIH-UHFFFAOYSA-N cyclohexanol Chemical compound OC1CCCCC1 HPXRVTGHNJAIIH-UHFFFAOYSA-N 0.000 description 11
238000006356 dehydrogenation reaction Methods 0.000 description 10
UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 9
229910052739 hydrogen Inorganic materials 0.000 description 9
239000001257 hydrogen Substances 0.000 description 9
239000000243 solution Substances 0.000 description 9
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 7
229910052799 carbon Inorganic materials 0.000 description 5
239000007788 liquid Substances 0.000 description 5
239000000463 material Substances 0.000 description 5
238000002360 preparation method Methods 0.000 description 5
238000006243 chemical reaction Methods 0.000 description 4
238000005470 impregnation Methods 0.000 description 4
239000000047 product Substances 0.000 description 4
125000000217 alkyl group Chemical group 0.000 description 3
238000001035 drying Methods 0.000 description 3
238000010438 heat treatment Methods 0.000 description 3
239000003039 volatile agent Substances 0.000 description 3
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
238000010521 absorption reaction Methods 0.000 description 2
239000007864 aqueous solution Substances 0.000 description 2
238000009835 boiling Methods 0.000 description 2
238000001816 cooling Methods 0.000 description 2
239000012153 distilled water Substances 0.000 description 2
230000000694 effects Effects 0.000 description 2
238000001914 filtration Methods 0.000 description 2
150000002431 hydrogen Chemical class 0.000 description 2
239000002245 particle Substances 0.000 description 2
238000006467 substitution reaction Methods 0.000 description 2
238000005406 washing Methods 0.000 description 2
VTBOTOBFGSVRMA-UHFFFAOYSA-N 1-Methylcyclohexanol Chemical class CC1(O)CCCCC1 VTBOTOBFGSVRMA-UHFFFAOYSA-N 0.000 description 1
LFSAPCRASZRSKS-UHFFFAOYSA-N 2-methylcyclohexan-1-one Chemical class CC1CCCCC1=O LFSAPCRASZRSKS-UHFFFAOYSA-N 0.000 description 1
CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 1
238000004458 analytical method Methods 0.000 description 1
238000003556 assay Methods 0.000 description 1
230000015572 biosynthetic process Effects 0.000 description 1
125000004432 carbon atom Chemical group C* 0.000 description 1
235000011089 carbon dioxide Nutrition 0.000 description 1
230000003197 catalytic effect Effects 0.000 description 1
239000003610 charcoal Substances 0.000 description 1
230000000052 comparative effect Effects 0.000 description 1
150000001896 cresols Chemical class 0.000 description 1
239000013078 crystal Substances 0.000 description 1
HPXRVTGHNJAIIH-PTQBSOBMSA-N cyclohexanol Chemical class O[13CH]1CCCCC1 HPXRVTGHNJAIIH-PTQBSOBMSA-N 0.000 description 1
JHIVVAPYMSGYDF-PTQBSOBMSA-N cyclohexanone Chemical class O=[13C]1CCCCC1 JHIVVAPYMSGYDF-PTQBSOBMSA-N 0.000 description 1
230000008021 deposition Effects 0.000 description 1
239000007789 gas Substances 0.000 description 1
239000005457 ice water Substances 0.000 description 1
239000003317 industrial substance Substances 0.000 description 1
239000002244 precipitate Substances 0.000 description 1
238000000926 separation method Methods 0.000 description 1
239000007787 solid Substances 0.000 description 1
238000003756 stirring Methods 0.000 description 1
239000012808 vapor phase Substances 0.000 description 1

Classifications

- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
- B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
- B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
- B01J23/42—Platinum
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
- C07C37/06—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by conversion of non-aromatic six-membered rings or of such rings formed in situ into aromatic six-membered rings, e.g. by dehydrogenation
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
- C07C37/06—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by conversion of non-aromatic six-membered rings or of such rings formed in situ into aromatic six-membered rings, e.g. by dehydrogenation
- C07C37/07—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by conversion of non-aromatic six-membered rings or of such rings formed in situ into aromatic six-membered rings, e.g. by dehydrogenation with simultaneous reduction of C=O group in that ring
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
- B01J21/18—Carbon
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Engineering & Computer Science (AREA)
Materials Engineering (AREA)
Chemical Kinetics & Catalysis (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Catalysts (AREA)

CH1007062A 1961-08-25 1962-08-24 Procédé de préparation d'un catalyseur CH408954A (fr)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
US13377461A	1961-08-25	1961-08-25

Publications (1)

Publication Number	Publication Date
CH408954A true CH408954A (fr)	1966-03-15

Family

ID=22460244

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CH1007062A CH408954A (fr)	1961-08-25	1962-08-24	Procédé de préparation d'un catalyseur

Country Status (4)

Country	Link
CH (1)	CH408954A (es)
ES (1)	ES280295A1 (es)
GB (1)	GB1013715A (es)
LU (1)	LU42227A1 (es)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
KR20130081294A (ko)	2008-08-29	2013-07-16	엑손모빌 케미칼 패턴츠 인코포레이티드	페놀 제조 방법
CN102753505A (zh)	2010-02-05	2012-10-24	埃克森美孚化学专利公司	环己酮脱氢催化剂和方法
US9242227B2 (en)	2010-02-05	2016-01-26	Exxonmobil Chemical Patents Inc.	Dehydrogenation catalyst and process
SG10201503888PA (en)	2010-06-25	2015-06-29	Exxonmobil Chem Patents Inc	Dehydrogenation process

1962
- 1962-08-08 GB GB30370/62A patent/GB1013715A/en not_active Expired
- 1962-08-16 LU LU42227D patent/LU42227A1/xx unknown
- 1962-08-24 CH CH1007062A patent/CH408954A/fr unknown
- 1962-08-25 ES ES280295A patent/ES280295A1/es not_active Expired

Also Published As

Publication number	Publication date
ES280295A1 (es)	1963-02-01
LU42227A1 (es)	1964-02-16
GB1013715A (en)	1965-12-22

Publication	Publication Date	Title
FR2489816A1 (fr)	1982-03-12	Procede d'hydroxylation des hydrocarbures aromatiques
Feuer et al.	1956	The Nitration of Cyclic Ketones with Alkyl Nitrates1
Kohler et al.	1923	The catalytic reduction of nitro compounds. i. α, β-unsaturated nitro compounds
US3968163A (en)	1976-07-06	Preparation of 4 and 5-methylindanes
FR2510991A1 (fr)	1983-02-11	Procede pour la preparation de methacrylamides et d'acrylamides n-substitues
EP0025383B1 (fr)	1982-09-22	Nouveaux dérivés substitués du cyclopropène, leur préparation et leur application dans la synthèse de précurseurs de l'acide dl cis chrysanthémique
FR2467837A1 (fr)	1981-04-30	Nouveaux composes acetyleniques, obtention et application en vue de la preparation de cetones alicycliques, telles que la b-damascenone
EP0301925B1 (fr)	1991-10-23	Nouveau procédé de préparation énantiospécifique du (S) éthylamino-2 (trifluorométhyl-3 phényl)-1 propane
BE623725A (es)
FR2525590A1 (fr)	1983-10-28	Preparation en phase liquide d'esters d'acides delta-cetocarboxyliques utilisant un catalyseur insoluble dans la phase liquide
CH417562A (fr)	1966-07-31	Procédé de préparation d'un acide dibasique
FR1464505A (fr)	1966-12-30	Procédé pour la préparation du 1, 3-cyclohexadiényl-carbonitrile
US1576544A (en)	1926-03-16	Proces for the production of butyric aldehyde
CH443340A (fr)	1967-09-15	Procédé de préparation d'hydroxybenzènes
BAILEY et al.	1958	Pyrolysis of Esters. XIV. Synthesis of 1, 3-Dimethylenecyclohexane1
MC896A1 (fr)	1972-06-22	Procédé de préparation de 1-alkyl-2-aminomethylpyrrolidines
CH285943A (fr)	1952-09-30	Procédé de synthèse de la vitamine A.
CH637104A5 (fr)	1983-07-15	Procede de synthese de dinitro-2,4 t-butyl-6 methyl-3 anisole.
CH174870A (fr)	1935-01-31	Procédé de fabrication d'alcool éthylique.
CH406190A (fr)	1966-01-31	Procédé de préparation de l'acide hydroxy-10 décène-2 oïque trans
US2675391A (en)	1954-04-13	Preparation of alkyl isodehydroacetates from alkyl acetoacetates using hci in ethyl sulfuric acid as condensing agent
JPS6240346B2 (es)	1987-08-27
BE477693A (es)
BE621338A (es)
CH439269A (fr)	1967-07-15	Procédé de préparation d'une cycloalcanone